AR023309A1 - Procedimiento y dispositivo para la preparacion continua de polimerizados. - Google Patents
Procedimiento y dispositivo para la preparacion continua de polimerizados.Info
- Publication number
- AR023309A1 AR023309A1 ARP990101789A ARP990101789A AR023309A1 AR 023309 A1 AR023309 A1 AR 023309A1 AR P990101789 A ARP990101789 A AR P990101789A AR P990101789 A ARP990101789 A AR P990101789A AR 023309 A1 AR023309 A1 AR 023309A1
- Authority
- AR
- Argentina
- Prior art keywords
- polymerized
- procedure
- educts
- mixer
- micro
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/30—Micromixers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/30—Injector mixers
- B01F25/31—Injector mixers in conduits or tubes through which the main component flows
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2415—Tubular reactors
- B01J19/242—Tubular reactors in series
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F2025/91—Direction of flow or arrangement of feed and discharge openings
- B01F2025/917—Laminar or parallel flow, i.e. every point of the flow moves in layers which do not intermix
- B01F2025/9171—Parallel flow, i.e. every point of the flow moves in parallel layers where intermixing can occur by diffusion or which do not intermix; Focusing, i.e. compressing parallel layers without intermixing them
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F2035/99—Heating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/2805—Mixing plastics, polymer material ingredients, monomers or oligomers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00889—Mixing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
- B29K2105/0002—Condition, form or state of moulded material or of the material to be shaped monomers or prepolymers
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Polymerisation Methods In General (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
Abstract
Se procede a almacenar dos componentes reactivos (eductos) en recipientes separados (2, 3, 4 y 5) y mediante los dispositivos de regulacion y dosificacion6, 7, que pueden ser bombas dosificadoras, se los introduce por sobre presion en una micro-mezcladora 18, pasando por los intercambiadores de calorprecalentados, 11, 12. En los intercambiadores de calor 11, 12, cada uno de los eductos es calentados por separado en un grado tal que en el proceso delmezclado en la micro-mezcladora 18 se llega deinmediato a la temperatura requerida para la reaccion. La polimerizacion tiene lugar en un reactor tubular 20situado corriente abajo, consistente en tubos 21, 22, 23, conectados en serie (fig. 1).
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19816886A DE19816886C2 (de) | 1998-04-17 | 1998-04-17 | Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polymerisaten |
Publications (1)
Publication Number | Publication Date |
---|---|
AR023309A1 true AR023309A1 (es) | 2002-09-04 |
Family
ID=7864727
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ARP990101789A AR023309A1 (es) | 1998-04-17 | 1999-04-16 | Procedimiento y dispositivo para la preparacion continua de polimerizados. |
Country Status (10)
Country | Link |
---|---|
US (1) | US6555629B1 (es) |
EP (1) | EP1086143B1 (es) |
JP (1) | JP4410416B2 (es) |
KR (1) | KR100526914B1 (es) |
AR (1) | AR023309A1 (es) |
AT (1) | ATE302796T1 (es) |
AU (1) | AU3413599A (es) |
DE (2) | DE19816886C2 (es) |
ES (1) | ES2248994T3 (es) |
WO (1) | WO1999054362A1 (es) |
Families Citing this family (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19960389B4 (de) * | 1999-12-15 | 2009-01-15 | Basf Coatings Ag | Verfahren zur Polymerisation olefinisch ungesättigter Monomere mittels eines Taylorreaktors |
DE10001317A1 (de) * | 2000-01-14 | 2001-07-19 | Merck Patent Gmbh | Reaktion von Carbonylverbindungen mit metallorganischen Reagenzien |
DE10041823C2 (de) | 2000-08-25 | 2002-12-19 | Inst Mikrotechnik Mainz Gmbh | Verfahren und statischer Mikrovermischer zum Mischen mindestens zweier Fluide |
DE10154045A1 (de) * | 2001-11-02 | 2003-05-22 | Basf Coatings Ag | Verfahren zur Herstellung von (Co)Polymerisaten von olefinisch ungesättigten Monomeren |
DE10301874A1 (de) * | 2003-01-17 | 2004-07-29 | Celanese Emulsions Gmbh | Verfahren und Vorrichtung zur Herstellung von Emulsionspolymerisaten |
CN100413891C (zh) * | 2003-07-25 | 2008-08-27 | 出光兴产株式会社 | 自由基聚合物的制造方法及微细化学反应装置 |
EP1650228A4 (en) * | 2003-07-25 | 2008-02-27 | Idemitsu Kosan Co | PROCESS FOR PREPARING A RADICAL POLYMER AND MICROPROPERTATE FOR CHEMICAL REACTIONS |
CN1984709A (zh) * | 2004-03-02 | 2007-06-20 | 维洛塞斯公司 | 微通道聚合反应器 |
JP4603371B2 (ja) * | 2005-01-19 | 2010-12-22 | 出光興産株式会社 | ラジカル重合体の製造方法及び微細化学反応装置 |
US7795359B2 (en) * | 2005-03-04 | 2010-09-14 | Novartis Ag | Continuous process for production of polymeric materials |
DE102005015433A1 (de) * | 2005-04-05 | 2006-10-12 | Forschungszentrum Karlsruhe Gmbh | Mischersystem, Reaktor und Reaktorsystem |
DE102005055866A1 (de) * | 2005-11-23 | 2007-05-24 | Hte Ag The High Throughput Experimentation Company | Verfahren zur Herstellung von Aryl-Aryl gekoppelter Verbindungen |
JP2009067999A (ja) * | 2007-08-21 | 2009-04-02 | Kyoto Univ | Mw/Mnが1.25以下であるポリマーの製造方法 |
WO2009133187A1 (en) * | 2008-05-02 | 2009-11-05 | Basf Se | Process and apparatus for continuously polymerizing cationically polymerizable monomers |
JP5623387B2 (ja) * | 2008-05-02 | 2014-11-12 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | ラジカル重合によってポリマーを連続的に製造するための方法及び装置 |
DE102009019470A1 (de) | 2008-05-02 | 2009-11-05 | Basf Se | Verfahren und Vorrichtung zur kontinuierlichen Polymerisation von kationisch polymerisierbaren Monomeren |
WO2010059000A2 (ko) * | 2008-11-21 | 2010-05-27 | (주)Lg화학 | 고분자 입자의 제조 장치 및 제조 방법 |
KR101783494B1 (ko) * | 2009-11-04 | 2017-09-29 | 바스프 에스이 | 폴리아크릴산 수용액의 제조 방법 |
ES2522842T3 (es) | 2010-04-01 | 2014-11-18 | Dsm Ip Assets B.V. | Proceso para polimerización continua en emulsión |
JP2014505753A (ja) | 2010-12-17 | 2014-03-06 | ビーエーエスエフ ソシエタス・ヨーロピア | 安定なポリアクリル酸、その製造およびその使用 |
JP5776318B2 (ja) * | 2011-05-12 | 2015-09-09 | Dic株式会社 | 乳化分散体及びその製造方法 |
EP2570180A1 (en) | 2011-09-15 | 2013-03-20 | Bayer MaterialScience AG | Method for a continuous radical polymerization using microreactors |
CA2865460A1 (en) * | 2012-03-09 | 2013-09-12 | Basf Se | Continuous process for the synthesis of graft polymers based on polyethers |
US9481742B2 (en) | 2013-04-16 | 2016-11-01 | Basf Se | Continuous process for the manufacture of highly-branched polymers |
EP2915581B1 (de) | 2014-03-06 | 2017-07-12 | Fluitec Invest AG | Statischer Mischer |
US10442873B2 (en) | 2014-08-29 | 2019-10-15 | Japan Agency For Marine-Earth Science And Technology | Radical polymerization method and polymerization reaction apparatus |
CN109925975B (zh) * | 2019-04-03 | 2020-09-01 | 中山华明泰科技股份有限公司 | 一种固体丙烯酸树脂管式自动反应装置 |
CN110681326B (zh) * | 2019-08-09 | 2021-09-10 | 中国科学院大连化学物理研究所 | 一种橡胶防焦剂ctp合成的微反应系统及方法 |
CN110681327B (zh) * | 2019-08-09 | 2021-07-23 | 中国科学院大连化学物理研究所 | 一种橡胶防焦剂ctp连续合成的微反应系统及方法 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2940043A1 (de) * | 1979-10-03 | 1981-04-16 | Henkel KGaA, 4000 Düsseldorf | Verfahren zur herstellung von polymerisaten von acryl- und methacrylsaeureestern, sowie deren verwendung |
FR2735480B1 (fr) * | 1995-06-15 | 1997-07-18 | Atochem Elf Sa | Procede de polymerisation anionique en continu d'au moins un monomere (meth)acrylique pour l'obtention de polymeres a haut taux de solide |
-
1998
- 1998-04-17 DE DE19816886A patent/DE19816886C2/de not_active Expired - Fee Related
-
1999
- 1999-03-17 AT AT99915632T patent/ATE302796T1/de active
- 1999-03-17 WO PCT/EP1999/001734 patent/WO1999054362A1/de active IP Right Grant
- 1999-03-17 US US09/673,156 patent/US6555629B1/en not_active Expired - Fee Related
- 1999-03-17 KR KR10-2000-7011498A patent/KR100526914B1/ko not_active IP Right Cessation
- 1999-03-17 EP EP99915632A patent/EP1086143B1/de not_active Expired - Lifetime
- 1999-03-17 ES ES99915632T patent/ES2248994T3/es not_active Expired - Lifetime
- 1999-03-17 AU AU34135/99A patent/AU3413599A/en not_active Abandoned
- 1999-03-17 DE DE59912468T patent/DE59912468D1/de not_active Expired - Lifetime
- 1999-03-17 JP JP2000544700A patent/JP4410416B2/ja not_active Expired - Fee Related
- 1999-04-16 AR ARP990101789A patent/AR023309A1/es unknown
Also Published As
Publication number | Publication date |
---|---|
DE19816886A1 (de) | 1999-10-21 |
EP1086143B1 (de) | 2005-08-24 |
AU3413599A (en) | 1999-11-08 |
JP2002512272A (ja) | 2002-04-23 |
DE19816886C2 (de) | 2001-06-07 |
WO1999054362A1 (de) | 1999-10-28 |
KR20010042764A (ko) | 2001-05-25 |
EP1086143A1 (de) | 2001-03-28 |
ATE302796T1 (de) | 2005-09-15 |
ES2248994T3 (es) | 2006-03-16 |
KR100526914B1 (ko) | 2005-11-09 |
JP4410416B2 (ja) | 2010-02-03 |
US6555629B1 (en) | 2003-04-29 |
DE59912468D1 (de) | 2005-09-29 |
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