ZA201202132B - Method for producing a crystalline solid from glycine-n,n-diacetic acid derivatives - Google Patents
Method for producing a crystalline solid from glycine-n,n-diacetic acid derivativesInfo
- Publication number
- ZA201202132B ZA201202132B ZA2012/02132A ZA201202132A ZA201202132B ZA 201202132 B ZA201202132 B ZA 201202132B ZA 2012/02132 A ZA2012/02132 A ZA 2012/02132A ZA 201202132 A ZA201202132 A ZA 201202132A ZA 201202132 B ZA201202132 B ZA 201202132B
- Authority
- ZA
- South Africa
- Prior art keywords
- glycine
- producing
- acid derivatives
- crystalline solid
- diacetic acid
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000007787 solid Substances 0.000 title 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
- C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
- C07C229/10—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
- C07C229/16—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of hydrocarbon radicals substituted by amino or carboxyl groups, e.g. ethylenediamine-tetra-acetic acid, iminodiacetic acids
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
- C05D9/02—Other inorganic fertilisers containing trace elements
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/40—Separation; Purification
- C07C227/42—Crystallisation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
- C11D7/3245—Aminoacids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/13—Crystalline forms, e.g. polymorphs
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2602/00—Systems containing two condensed rings
- C07C2602/02—Systems containing two condensed rings the rings having only two atoms in common
- C07C2602/04—One of the condensed rings being a six-membered aromatic ring
- C07C2602/12—One of the condensed rings being a six-membered aromatic ring the other ring being at least seven-membered
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102009038951A DE102009038951A1 (de) | 2009-08-26 | 2009-08-26 | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| PCT/EP2010/005219 WO2011023382A2 (de) | 2009-08-26 | 2010-08-25 | Verfahren zur herstellung eines kristallinen feststoffes aus glycin-n, n-diessigsäure-derivaten mit hinreichend geringer hygroskopizität |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ZA201202132B true ZA201202132B (en) | 2013-05-29 |
Family
ID=43500504
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ZA2012/02132A ZA201202132B (en) | 2009-08-26 | 2012-03-22 | Method for producing a crystalline solid from glycine-n,n-diacetic acid derivatives |
Country Status (17)
| Country | Link |
|---|---|
| US (2) | US9376649B2 (enExample) |
| EP (1) | EP2470496B2 (enExample) |
| JP (1) | JP5756107B2 (enExample) |
| KR (1) | KR101755736B1 (enExample) |
| CN (1) | CN102574775B (enExample) |
| AU (1) | AU2010288872A1 (enExample) |
| BR (1) | BR112012004179B1 (enExample) |
| CA (1) | CA2771916C (enExample) |
| DE (1) | DE102009038951A1 (enExample) |
| ES (1) | ES2563323T5 (enExample) |
| MX (1) | MX2012002244A (enExample) |
| MY (1) | MY158464A (enExample) |
| PL (1) | PL2470496T5 (enExample) |
| RU (1) | RU2551851C2 (enExample) |
| SG (1) | SG178352A1 (enExample) |
| WO (1) | WO2011023382A2 (enExample) |
| ZA (1) | ZA201202132B (enExample) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102009038951A1 (de) * | 2009-08-26 | 2011-03-03 | Inprotec Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| WO2011045266A1 (de) | 2009-10-12 | 2011-04-21 | Basf Se | Verfahren zur herstellung eines pulvers enthaltend eines oder mehrere komplexbildnersalze |
| DE102009060814A1 (de) | 2009-12-30 | 2011-07-07 | inprotec AG, 79423 | Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält |
| ES2547417T3 (es) * | 2010-09-27 | 2015-10-06 | Basf Se | Procedimiento para la producción de un granulado que contiene una o varias sales de agentes complejantes |
| US9227915B2 (en) * | 2011-05-03 | 2016-01-05 | Basf Se | Process for the preparation of a crystalline L-MGDA trialkali metal salt |
| GB2491619B (en) | 2011-06-09 | 2014-10-01 | Pq Silicas Bv | Builder granules and process for their preparation |
| EP2931699A1 (en) | 2012-12-14 | 2015-10-21 | Akzo Nobel Chemicals International B.V. | Crystalline particles of glutamic acid n,n-diacetic acid |
| WO2014090943A1 (en) | 2012-12-14 | 2014-06-19 | Akzo Nobel Chemicals International B.V. | Crystalline particles of salts of glutamic acid n,n-diacetic acid |
| WO2015173157A2 (en) * | 2014-05-13 | 2015-11-19 | Akzo Nobel Chemicals International B.V. | Process to crystallize chelating agents |
| JP2019507671A (ja) | 2015-12-11 | 2019-03-22 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | 顆粒の製造方法 |
| RU2742268C2 (ru) * | 2016-06-20 | 2021-02-04 | Басф Се | Порошки и гранулы и способ получения таких порошков и гранул |
| BR112019017127A2 (pt) | 2017-02-24 | 2020-04-14 | Basf Se | processo para produção de sal de metal alcalino de diacetato de metilglicina sólido, partículas sólidas de sal de metal alcalino de diacetato de metilglici-na, e, uso de partículas sólidas |
| US10836709B2 (en) | 2017-07-07 | 2020-11-17 | Nouryon Chemicals International B.V. | Process to prepare a solid composition of an amino acid diacetic acid |
| CN112166102A (zh) | 2018-05-30 | 2021-01-01 | 巴斯夫欧洲公司 | 制造固体甲基甘氨酸二乙酸(mgda)碱金属盐的方法和固体颗粒 |
| US12263299B2 (en) | 2018-06-26 | 2025-04-01 | Juul Labs, Inc. | Devices and methods for cessation of nicotine addiction |
| EP3898575B1 (en) | 2018-12-21 | 2023-02-15 | Nouryon Chemicals International B.V. | Crumbly phase composition of methylglycine n,n diacetic acid |
| KR102771094B1 (ko) | 2019-11-21 | 2025-02-24 | (주)아모레퍼시픽 | 고함량의 락테이트 금속염 및 실리콘계 오일의 혼합물을 포함하는 w/s형 화장료 조성물 |
| WO2021255525A1 (en) | 2020-06-19 | 2021-12-23 | Nouryon Chemicals International B.V. | Process to prepare a co granule of methylglycine n,n diacetic acid salts employing a crumbly phase composition of methylglycine n,n diacetic acid salts |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3932316A (en) | 1974-11-13 | 1976-01-13 | The Procter & Gamble Company | Free flowing detergent compositions containing benzoate salts |
| JPH0678225B2 (ja) | 1985-11-27 | 1994-10-05 | 株式会社林原生物化学研究所 | 脱水医薬品とその製造方法 |
| DE4319935A1 (de) * | 1993-06-16 | 1994-12-22 | Basf Ag | Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen |
| JP4711471B2 (ja) | 1996-07-05 | 2011-06-29 | 三菱商事フードテック株式会社 | 結晶マルチトール及びそれを含有する含蜜結晶の製造方法 |
| DE19649681A1 (de) | 1996-11-29 | 1998-06-04 | Basf Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| RU2305604C2 (ru) * | 2001-04-13 | 2007-09-10 | Уреа Касале С.А. | Гранулятор с псевдоожиженным слоем и используемый в нем распылитель |
| DE102004032320A1 (de) * | 2004-07-02 | 2006-01-19 | Basf Ag | Mischpulver oder Mischgranulat auf Basis von MGDA |
| JP5328781B2 (ja) * | 2007-07-03 | 2013-10-30 | ビーエーエスエフ ソシエタス・ヨーロピア | 本質的にα−アラニン−Ｎ，Ｎ−二酢酸及び／又はα−アラニン−Ｎ，Ｎ−二酢酸の１以上の誘導体を含有する、易流動性でかつ貯蔵安定性の固体の製造法 |
| WO2009103822A1 (en) | 2008-04-01 | 2009-08-27 | Unilever Nv | Preparation of free flowing granules of methyglycine diacetic acid |
| FR2935383B1 (fr) | 2008-08-26 | 2010-10-01 | Pancosma Sa Pour L Ind Des Pro | Procede et dispositif pour la fabrication de complexes organometalliques en poudre. |
| US8628684B2 (en) * | 2009-05-20 | 2014-01-14 | Basf Se | Process for the preparation of a powder comprising one or more derivatives of glycine-N,N diacetic acid and/or one or more derivatives of glutamine-N,N diacetic acid and methylglycine-N,N diacetic acid trisodium salt powder |
| DE102009038951A1 (de) * | 2009-08-26 | 2011-03-03 | Inprotec Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| WO2011045266A1 (de) * | 2009-10-12 | 2011-04-21 | Basf Se | Verfahren zur herstellung eines pulvers enthaltend eines oder mehrere komplexbildnersalze |
| GB2491619B (en) * | 2011-06-09 | 2014-10-01 | Pq Silicas Bv | Builder granules and process for their preparation |
-
2009
- 2009-08-26 DE DE102009038951A patent/DE102009038951A1/de not_active Withdrawn
-
2010
- 2010-08-25 MX MX2012002244A patent/MX2012002244A/es active IP Right Grant
- 2010-08-25 RU RU2012111127/04A patent/RU2551851C2/ru active
- 2010-08-25 WO PCT/EP2010/005219 patent/WO2011023382A2/de not_active Ceased
- 2010-08-25 EP EP10747834.9A patent/EP2470496B2/de active Active
- 2010-08-25 CA CA2771916A patent/CA2771916C/en not_active Expired - Fee Related
- 2010-08-25 KR KR1020127007333A patent/KR101755736B1/ko not_active Expired - Fee Related
- 2010-08-25 CN CN201080037900.3A patent/CN102574775B/zh active Active
- 2010-08-25 AU AU2010288872A patent/AU2010288872A1/en not_active Abandoned
- 2010-08-25 BR BR112012004179A patent/BR112012004179B1/pt active IP Right Grant
- 2010-08-25 ES ES10747834T patent/ES2563323T5/es active Active
- 2010-08-25 PL PL10747834.9T patent/PL2470496T5/pl unknown
- 2010-08-25 SG SG2012009312A patent/SG178352A1/en unknown
- 2010-08-25 US US13/391,397 patent/US9376649B2/en active Active
- 2010-08-25 MY MYPI2012000735A patent/MY158464A/en unknown
- 2010-08-25 JP JP2012525929A patent/JP5756107B2/ja active Active
-
2012
- 2012-03-22 ZA ZA2012/02132A patent/ZA201202132B/en unknown
-
2016
- 2016-04-12 US US15/096,678 patent/US9751829B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| ES2563323T3 (es) | 2016-03-14 |
| CN102574775B (zh) | 2014-09-24 |
| ES2563323T5 (es) | 2024-10-16 |
| US9376649B2 (en) | 2016-06-28 |
| PL2470496T3 (pl) | 2016-06-30 |
| WO2011023382A3 (de) | 2011-05-12 |
| EP2470496B2 (de) | 2024-03-27 |
| KR101755736B1 (ko) | 2017-07-07 |
| CA2771916C (en) | 2017-07-25 |
| AU2010288872A1 (en) | 2012-03-08 |
| RU2551851C2 (ru) | 2015-05-27 |
| BR112012004179A2 (pt) | 2016-03-29 |
| KR20120089470A (ko) | 2012-08-10 |
| JP2013503119A (ja) | 2013-01-31 |
| SG178352A1 (en) | 2012-03-29 |
| JP5756107B2 (ja) | 2015-07-29 |
| CA2771916A1 (en) | 2011-03-03 |
| US9751829B2 (en) | 2017-09-05 |
| MX2012002244A (es) | 2012-03-29 |
| BR112012004179B1 (pt) | 2018-09-11 |
| MY158464A (en) | 2016-10-14 |
| PL2470496T5 (pl) | 2024-07-15 |
| DE102009038951A1 (de) | 2011-03-03 |
| WO2011023382A2 (de) | 2011-03-03 |
| CN102574775A (zh) | 2012-07-11 |
| US20160221930A1 (en) | 2016-08-04 |
| US20120149936A1 (en) | 2012-06-14 |
| RU2012111127A (ru) | 2013-10-10 |
| EP2470496B1 (de) | 2016-01-06 |
| EP2470496A2 (de) | 2012-07-04 |
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