JP5756107B2 - グリシン−ｎ，ｎ−ジアセチックアシッド誘導体ｉから、吸湿性が十分に低い結晶性固体を製造するための方法 - Google Patents

グリシン−ｎ，ｎ−ジアセチックアシッド誘導体ｉから、吸湿性が十分に低い結晶性固体を製造するための方法 Download PDF

Info

Publication number
JP5756107B2
JP5756107B2 JP2012525929A JP2012525929A JP5756107B2 JP 5756107 B2 JP5756107 B2 JP 5756107B2 JP 2012525929 A JP2012525929 A JP 2012525929A JP 2012525929 A JP2012525929 A JP 2012525929A JP 5756107 B2 JP5756107 B2 JP 5756107B2
Authority
JP
Japan
Prior art keywords
groups
formula
alkyl
diacetic acid
group
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2012525929A
Other languages
English (en)
Japanese (ja)
Other versions
JP2013503119A (ja
JP2013503119A5 (enExample
Inventor
バランヤイ，アンドレアス
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=43500504&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=JP5756107(B2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by BASF SE filed Critical BASF SE
Publication of JP2013503119A publication Critical patent/JP2013503119A/ja
Publication of JP2013503119A5 publication Critical patent/JP2013503119A5/ja
Application granted granted Critical
Publication of JP5756107B2 publication Critical patent/JP5756107B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
    • C07C229/10—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C07C229/16—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of hydrocarbon radicals substituted by amino or carboxyl groups, e.g. ethylenediamine-tetra-acetic acid, iminodiacetic acids
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00—Other inorganic fertilisers
    • C05D9/02—Other inorganic fertilisers containing trace elements
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22—Organic compounds
    • C11D7/32—Organic compounds containing nitrogen
    • C11D7/3245—Aminoacids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/02—Systems containing two condensed rings the rings having only two atoms in common
    • C07C2602/04—One of the condensed rings being a six-membered aromatic ring
    • C07C2602/12—One of the condensed rings being a six-membered aromatic ring the other ring being at least seven-membered

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)
JP2012525929A 2009-08-26 2010-08-25 グリシン−ｎ，ｎ−ジアセチックアシッド誘導体ｉから、吸湿性が十分に低い結晶性固体を製造するための方法 Active JP5756107B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102009038951.2 2009-08-26
DE102009038951A DE102009038951A1 (de) 2009-08-26 2009-08-26 Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
PCT/EP2010/005219 WO2011023382A2 (de) 2009-08-26 2010-08-25 Verfahren zur herstellung eines kristallinen feststoffes aus glycin-n, n-diessigsäure-derivaten mit hinreichend geringer hygroskopizität

Publications (3)

Publication Number Publication Date
JP2013503119A JP2013503119A (ja) 2013-01-31
JP2013503119A5 JP2013503119A5 (enExample) 2015-03-05
JP5756107B2 true JP5756107B2 (ja) 2015-07-29

Family

ID=43500504

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2012525929A Active JP5756107B2 (ja) 2009-08-26 2010-08-25 グリシン−ｎ，ｎ−ジアセチックアシッド誘導体ｉから、吸湿性が十分に低い結晶性固体を製造するための方法

Country Status (17)

Country Link
US (2) US9376649B2 (enExample)
EP (1) EP2470496B2 (enExample)
JP (1) JP5756107B2 (enExample)
KR (1) KR101755736B1 (enExample)
CN (1) CN102574775B (enExample)
AU (1) AU2010288872A1 (enExample)
BR (1) BR112012004179B1 (enExample)
CA (1) CA2771916C (enExample)
DE (1) DE102009038951A1 (enExample)
ES (1) ES2563323T5 (enExample)
MX (1) MX2012002244A (enExample)
MY (1) MY158464A (enExample)
PL (1) PL2470496T5 (enExample)
RU (1) RU2551851C2 (enExample)
SG (1) SG178352A1 (enExample)
WO (1) WO2011023382A2 (enExample)
ZA (1) ZA201202132B (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20210062413A (ko) 2019-11-21 2021-05-31 (주)아모레퍼시픽 고함량의 락테이트 금속염 및 실리콘계 오일의 혼합물을 포함하는 w/s형 화장료 조성물

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
WO2011045266A1 (de) 2009-10-12 2011-04-21 Basf Se Verfahren zur herstellung eines pulvers enthaltend eines oder mehrere komplexbildnersalze
DE102009060814A1 (de) 2009-12-30 2011-07-07 inprotec AG, 79423 Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält
ES2547417T3 (es) * 2010-09-27 2015-10-06 Basf Se Procedimiento para la producción de un granulado que contiene una o varias sales de agentes complejantes
US9227915B2 (en) * 2011-05-03 2016-01-05 Basf Se Process for the preparation of a crystalline L-MGDA trialkali metal salt
GB2491619B (en) 2011-06-09 2014-10-01 Pq Silicas Bv Builder granules and process for their preparation
EP2931699A1 (en) 2012-12-14 2015-10-21 Akzo Nobel Chemicals International B.V. Crystalline particles of glutamic acid n,n-diacetic acid
WO2014090943A1 (en) 2012-12-14 2014-06-19 Akzo Nobel Chemicals International B.V. Crystalline particles of salts of glutamic acid n,n-diacetic acid
WO2015173157A2 (en) * 2014-05-13 2015-11-19 Akzo Nobel Chemicals International B.V. Process to crystallize chelating agents
JP2019507671A (ja) 2015-12-11 2019-03-22 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 顆粒の製造方法
RU2742268C2 (ru) * 2016-06-20 2021-02-04 Басф Се Порошки и гранулы и способ получения таких порошков и гранул
BR112019017127A2 (pt) 2017-02-24 2020-04-14 Basf Se processo para produção de sal de metal alcalino de diacetato de metilglicina sólido, partículas sólidas de sal de metal alcalino de diacetato de metilglici-na, e, uso de partículas sólidas
US10836709B2 (en) 2017-07-07 2020-11-17 Nouryon Chemicals International B.V. Process to prepare a solid composition of an amino acid diacetic acid
CN112166102A (zh) 2018-05-30 2021-01-01 巴斯夫欧洲公司 制造固体甲基甘氨酸二乙酸(mgda)碱金属盐的方法和固体颗粒
US12263299B2 (en) 2018-06-26 2025-04-01 Juul Labs, Inc. Devices and methods for cessation of nicotine addiction
EP3898575B1 (en) 2018-12-21 2023-02-15 Nouryon Chemicals International B.V. Crumbly phase composition of methylglycine n,n diacetic acid
WO2021255525A1 (en) 2020-06-19 2021-12-23 Nouryon Chemicals International B.V. Process to prepare a co granule of methylglycine n,n diacetic acid salts employing a crumbly phase composition of methylglycine n,n diacetic acid salts

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3932316A (en) 1974-11-13 1976-01-13 The Procter & Gamble Company Free flowing detergent compositions containing benzoate salts
JPH0678225B2 (ja) 1985-11-27 1994-10-05 株式会社林原生物化学研究所 脱水医薬品とその製造方法
DE4319935A1 (de) * 1993-06-16 1994-12-22 Basf Ag Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen
JP4711471B2 (ja) 1996-07-05 2011-06-29 三菱商事フードテック株式会社 結晶マルチトール及びそれを含有する含蜜結晶の製造方法
DE19649681A1 (de) 1996-11-29 1998-06-04 Basf Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
RU2305604C2 (ru) * 2001-04-13 2007-09-10 Уреа Касале С.А. Гранулятор с псевдоожиженным слоем и используемый в нем распылитель
DE102004032320A1 (de) * 2004-07-02 2006-01-19 Basf Ag Mischpulver oder Mischgranulat auf Basis von MGDA
JP5328781B2 (ja) * 2007-07-03 2013-10-30 ビーエーエスエフ ソシエタス・ヨーロピア 本質的にα−アラニン−Ｎ，Ｎ−二酢酸及び／又はα−アラニン−Ｎ，Ｎ−二酢酸の１以上の誘導体を含有する、易流動性でかつ貯蔵安定性の固体の製造法
WO2009103822A1 (en) 2008-04-01 2009-08-27 Unilever Nv Preparation of free flowing granules of methyglycine diacetic acid
FR2935383B1 (fr) 2008-08-26 2010-10-01 Pancosma Sa Pour L Ind Des Pro Procede et dispositif pour la fabrication de complexes organometalliques en poudre.
US8628684B2 (en) * 2009-05-20 2014-01-14 Basf Se Process for the preparation of a powder comprising one or more derivatives of glycine-N,N diacetic acid and/or one or more derivatives of glutamine-N,N diacetic acid and methylglycine-N,N diacetic acid trisodium salt powder
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
WO2011045266A1 (de) * 2009-10-12 2011-04-21 Basf Se Verfahren zur herstellung eines pulvers enthaltend eines oder mehrere komplexbildnersalze
GB2491619B (en) * 2011-06-09 2014-10-01 Pq Silicas Bv Builder granules and process for their preparation

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20210062413A (ko) 2019-11-21 2021-05-31 (주)아모레퍼시픽 고함량의 락테이트 금속염 및 실리콘계 오일의 혼합물을 포함하는 w/s형 화장료 조성물

Also Published As

Publication number Publication date
ES2563323T3 (es) 2016-03-14
CN102574775B (zh) 2014-09-24
ES2563323T5 (es) 2024-10-16
US9376649B2 (en) 2016-06-28
PL2470496T3 (pl) 2016-06-30
WO2011023382A3 (de) 2011-05-12
EP2470496B2 (de) 2024-03-27
KR101755736B1 (ko) 2017-07-07
CA2771916C (en) 2017-07-25
AU2010288872A1 (en) 2012-03-08
RU2551851C2 (ru) 2015-05-27
ZA201202132B (en) 2013-05-29
BR112012004179A2 (pt) 2016-03-29
KR20120089470A (ko) 2012-08-10
JP2013503119A (ja) 2013-01-31
SG178352A1 (en) 2012-03-29
CA2771916A1 (en) 2011-03-03
US9751829B2 (en) 2017-09-05
MX2012002244A (es) 2012-03-29
BR112012004179B1 (pt) 2018-09-11
MY158464A (en) 2016-10-14
PL2470496T5 (pl) 2024-07-15
DE102009038951A1 (de) 2011-03-03
WO2011023382A2 (de) 2011-03-03
CN102574775A (zh) 2012-07-11
US20160221930A1 (en) 2016-08-04
US20120149936A1 (en) 2012-06-14
RU2012111127A (ru) 2013-10-10
EP2470496B1 (de) 2016-01-06
EP2470496A2 (de) 2012-07-04

Similar Documents

Publication Publication Date Title
JP5756107B2 (ja) グリシン−ｎ，ｎ−ジアセチックアシッド誘導体ｉから、吸湿性が十分に低い結晶性固体を製造するための方法
JP5795329B2 (ja) グルタミン酸−ｎ，ｎ−アセト酢酸（ｇｌｄａ）又はその誘導体を含む、吸湿性が十分に低い固体を製造する方法
US5981798A (en) Preparation of a crystalline solid from glycine-N,N-diacetic acid derivatives with sufficiently low hygroscopicity
RU2554932C2 (ru) Способ изготовления порошка, содержащего одну или несколько комплексообразующих солей
EP2931700B1 (en) Crystalline particles of salts of glutamic acid n,n-diacetic acid
RU2728876C2 (ru) Способ получения гранул
US9815773B2 (en) Crystalline particles of glutamic acid N,N-diacetic acid

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20130808

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20130808

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20140924

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20141212

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20141219

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20150114

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20150428

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20150528

R150 Certificate of patent or registration of utility model

Ref document number: 5756107

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250