RU2551851C2 - Способ получения кристаллического твердого вещества из производных глицин-n,n-диуксусной кислоты - Google Patents

Способ получения кристаллического твердого вещества из производных глицин-n,n-диуксусной кислоты Download PDF

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Publication number
RU2551851C2
RU2551851C2 RU2012111127/04A RU2012111127A RU2551851C2 RU 2551851 C2 RU2551851 C2 RU 2551851C2 RU 2012111127/04 A RU2012111127/04 A RU 2012111127/04A RU 2012111127 A RU2012111127 A RU 2012111127A RU 2551851 C2 RU2551851 C2 RU 2551851C2
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RU
Russia
Prior art keywords
formula
diacetic acid
glycine
crystalline solid
compound
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RU2012111127/04A
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English (en)
Russian (ru)
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RU2012111127A (ru
Inventor
Андреас БАРАНИАЙ
Original Assignee
Басф Се
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
    • C07C229/10—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C07C229/16—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of hydrocarbon radicals substituted by amino or carboxyl groups, e.g. ethylenediamine-tetra-acetic acid, iminodiacetic acids
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00—Other inorganic fertilisers
    • C05D9/02—Other inorganic fertilisers containing trace elements
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22—Organic compounds
    • C11D7/32—Organic compounds containing nitrogen
    • C11D7/3245—Aminoacids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/02—Systems containing two condensed rings the rings having only two atoms in common
    • C07C2602/04—One of the condensed rings being a six-membered aromatic ring
    • C07C2602/12—One of the condensed rings being a six-membered aromatic ring the other ring being at least seven-membered

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)
RU2012111127/04A 2009-08-26 2010-08-25 Способ получения кристаллического твердого вещества из производных глицин-n,n-диуксусной кислоты RU2551851C2 (ru)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102009038951.2 2009-08-26
DE102009038951A DE102009038951A1 (de) 2009-08-26 2009-08-26 Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
PCT/EP2010/005219 WO2011023382A2 (de) 2009-08-26 2010-08-25 Verfahren zur herstellung eines kristallinen feststoffes aus glycin-n, n-diessigsäure-derivaten mit hinreichend geringer hygroskopizität

Publications (2)

Publication Number Publication Date
RU2012111127A RU2012111127A (ru) 2013-10-10
RU2551851C2 true RU2551851C2 (ru) 2015-05-27

Family

ID=43500504

Family Applications (1)

Application Number Title Priority Date Filing Date
RU2012111127/04A RU2551851C2 (ru) 2009-08-26 2010-08-25 Способ получения кристаллического твердого вещества из производных глицин-n,n-диуксусной кислоты

Country Status (17)

Country Link
US (2) US9376649B2 (enExample)
EP (1) EP2470496B2 (enExample)
JP (1) JP5756107B2 (enExample)
KR (1) KR101755736B1 (enExample)
CN (1) CN102574775B (enExample)
AU (1) AU2010288872A1 (enExample)
BR (1) BR112012004179B1 (enExample)
CA (1) CA2771916C (enExample)
DE (1) DE102009038951A1 (enExample)
ES (1) ES2563323T5 (enExample)
MX (1) MX2012002244A (enExample)
MY (1) MY158464A (enExample)
PL (1) PL2470496T5 (enExample)
RU (1) RU2551851C2 (enExample)
SG (1) SG178352A1 (enExample)
WO (1) WO2011023382A2 (enExample)
ZA (1) ZA201202132B (enExample)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
AU2010305833A1 (en) * 2009-10-12 2012-04-19 Basf Se Method for producing a powder containing one or more complexing agent salts
DE102009060814A1 (de) 2009-12-30 2011-07-07 inprotec AG, 79423 Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält
PL2621892T3 (pl) * 2010-09-27 2015-12-31 Basf Se Sposób wytwarzania granulatu zawierającego jedną lub większą liczbę soli kompleksotwórczych
US9227915B2 (en) * 2011-05-03 2016-01-05 Basf Se Process for the preparation of a crystalline L-MGDA trialkali metal salt
GB2491619B (en) * 2011-06-09 2014-10-01 Pq Silicas Bv Builder granules and process for their preparation
US9738594B2 (en) 2012-12-14 2017-08-22 Akzo Nobel Chemicals International B.V. Crystalline particles of salts of glutamic acid N,N-diacetic acid
EP2931699A1 (en) 2012-12-14 2015-10-21 Akzo Nobel Chemicals International B.V. Crystalline particles of glutamic acid n,n-diacetic acid
CN106458851B (zh) * 2014-05-13 2019-01-11 阿克苏诺贝尔化学品国际有限公司 将螯合剂结晶的方法
CN108368459B9 (zh) * 2015-12-11 2021-12-17 巴斯夫欧洲公司 制造颗粒的方法
BR112018075476B1 (pt) * 2016-06-20 2022-10-04 Basf Se Processo para produção de um pó ou grânulo, pó ou grânulo, e, uso de grânulos e de pós
WO2018153876A1 (en) 2017-02-24 2018-08-30 Basf Se Process for making solid methylglycine diacetate (mgda) alkali metal salt, and solid particles
EP3649103B1 (en) * 2017-07-07 2022-03-30 Nouryon Chemicals International B.V. Process to prepare a solid composition of an amino acid diacetic acid
EP3802481A1 (en) 2018-05-30 2021-04-14 Basf Se Process for making solid methylglycine diacetate (mgda) alkali metal salt, and solid particles
WO2020006109A1 (en) 2018-06-26 2020-01-02 Juul Labs, Inc. Devices and methods for cessation of nicotine addiction
US12258541B2 (en) 2018-12-21 2025-03-25 Nouryon Chemicals International B.V. Crumbly phase composition of methylglycine N,N diacetic acid
KR102771094B1 (ko) 2019-11-21 2025-02-24 (주)아모레퍼시픽 고함량의 락테이트 금속염 및 실리콘계 오일의 혼합물을 포함하는 w/s형 화장료 조성물
JP7518926B2 (ja) 2020-06-19 2024-07-18 ヌーリオン ケミカルズ インターナショナル ベスローテン フェノーツハップ メチルグリシンｎ，ｎの二酢酸塩の脆砕相組成物を用いたメチルグリシンｎ，ｎの二酢酸塩の共顆粒を調製するためのプロセス

Citations (2)

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DE19649681A1 (de) * 1996-11-29 1998-06-04 Basf Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
RU2305604C2 (ru) * 2001-04-13 2007-09-10 Уреа Касале С.А. Гранулятор с псевдоожиженным слоем и используемый в нем распылитель

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US3932316A (en) 1974-11-13 1976-01-13 The Procter & Gamble Company Free flowing detergent compositions containing benzoate salts
JPH0678225B2 (ja) * 1985-11-27 1994-10-05 株式会社林原生物化学研究所 脱水医薬品とその製造方法
DE4319935A1 (de) * 1993-06-16 1994-12-22 Basf Ag Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen
JP4711471B2 (ja) 1996-07-05 2011-06-29 三菱商事フードテック株式会社 結晶マルチトール及びそれを含有する含蜜結晶の製造方法
DE102004032320A1 (de) * 2004-07-02 2006-01-19 Basf Ag Mischpulver oder Mischgranulat auf Basis von MGDA
US20100187724A1 (en) * 2007-07-03 2010-07-29 Basf Se Process for producing a free-flowing and storage-stable solid comprising essentially alpha-alanine-n,n-diacetic acid and/or one or more derivatives of alpha-alanine-n,n-diacetic acid
TR201808032T4 (tr) 2008-04-01 2018-06-21 Unilever Nv Metilglisin diasetik asidin serbest akışlı granüllerinin hazırlanması.
FR2935383B1 (fr) * 2008-08-26 2010-10-01 Pancosma Sa Pour L Ind Des Pro Procede et dispositif pour la fabrication de complexes organometalliques en poudre.
WO2010133618A1 (de) * 2009-05-20 2010-11-25 Basf Se Verfahren zur herstellung eines pulvers enthaltend eines oder mehrere derivate der glycin-n,n-diessigsäure und/oder eines oder mehrere derivate der glutamin-n,n-diessigsäure und methylglycin-n,n-diessigsäure-trinatriumsalzpulver
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
AU2010305833A1 (en) * 2009-10-12 2012-04-19 Basf Se Method for producing a powder containing one or more complexing agent salts
GB2491619B (en) * 2011-06-09 2014-10-01 Pq Silicas Bv Builder granules and process for their preparation

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19649681A1 (de) * 1996-11-29 1998-06-04 Basf Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
RU2305604C2 (ru) * 2001-04-13 2007-09-10 Уреа Касале С.А. Гранулятор с псевдоожиженным слоем и используемый в нем распылитель

Also Published As

Publication number Publication date
CN102574775A (zh) 2012-07-11
KR20120089470A (ko) 2012-08-10
PL2470496T5 (pl) 2024-07-15
CA2771916A1 (en) 2011-03-03
US20160221930A1 (en) 2016-08-04
KR101755736B1 (ko) 2017-07-07
EP2470496B2 (de) 2024-03-27
CN102574775B (zh) 2014-09-24
ES2563323T5 (es) 2024-10-16
US9376649B2 (en) 2016-06-28
DE102009038951A1 (de) 2011-03-03
US20120149936A1 (en) 2012-06-14
MX2012002244A (es) 2012-03-29
AU2010288872A1 (en) 2012-03-08
BR112012004179B1 (pt) 2018-09-11
JP5756107B2 (ja) 2015-07-29
ES2563323T3 (es) 2016-03-14
PL2470496T3 (pl) 2016-06-30
ZA201202132B (en) 2013-05-29
EP2470496B1 (de) 2016-01-06
JP2013503119A (ja) 2013-01-31
EP2470496A2 (de) 2012-07-04
MY158464A (en) 2016-10-14
WO2011023382A2 (de) 2011-03-03
CA2771916C (en) 2017-07-25
WO2011023382A3 (de) 2011-05-12
RU2012111127A (ru) 2013-10-10
BR112012004179A2 (pt) 2016-03-29
SG178352A1 (en) 2012-03-29
US9751829B2 (en) 2017-09-05

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