MX2012002244A - Metodo para producir un solido cristalino de derivados de acido glicina-n, n-diacetico con higroscopicidad suficientemente reducida. - Google Patents

Metodo para producir un solido cristalino de derivados de acido glicina-n, n-diacetico con higroscopicidad suficientemente reducida.

Info

Publication number
MX2012002244A
MX2012002244A MX2012002244A MX2012002244A MX2012002244A MX 2012002244 A MX2012002244 A MX 2012002244A MX 2012002244 A MX2012002244 A MX 2012002244A MX 2012002244 A MX2012002244 A MX 2012002244A MX 2012002244 A MX2012002244 A MX 2012002244A
Authority
MX
Mexico
Prior art keywords
glycine
producing
acid derivatives
crystalline solid
diacetic acid
Prior art date
Application number
MX2012002244A
Other languages
English (en)
Inventor
Andreas Baranyai
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=43500504&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=MX2012002244(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Basf Se filed Critical Basf Se
Publication of MX2012002244A publication Critical patent/MX2012002244A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
    • C07C229/10—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C07C229/16—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of hydrocarbon radicals substituted by amino or carboxyl groups, e.g. ethylenediamine-tetra-acetic acid, iminodiacetic acids
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00—Other inorganic fertilisers
    • C05D9/02—Other inorganic fertilisers containing trace elements
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22—Organic compounds
    • C11D7/32—Organic compounds containing nitrogen
    • C11D7/3245—Aminoacids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/02—Systems containing two condensed rings the rings having only two atoms in common
    • C07C2602/04—One of the condensed rings being a six-membered aromatic ring
    • C07C2602/12—One of the condensed rings being a six-membered aromatic ring the other ring being at least seven-membered

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)

Abstract

La presente invención se refiere a un proceso para preparar un sólido cristalino a partir de derivados de ácido glicina-N,N-diacético (por ejemplo, MGDA) de higroscopicidad suficientemente baja, que se caracteriza porque por lo menos un compuesto cristalino de la fórmula I se introduce como semilla, y se lleva a cabo una granulación de aspersión con al menos un compuesto de la fórmula I, preferiblemente seguido por un tratamiento con calor.
MX2012002244A 2009-08-26 2010-08-25 Metodo para producir un solido cristalino de derivados de acido glicina-n, n-diacetico con higroscopicidad suficientemente reducida. MX2012002244A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102009038951A DE102009038951A1 (de) 2009-08-26 2009-08-26 Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
PCT/EP2010/005219 WO2011023382A2 (de) 2009-08-26 2010-08-25 Verfahren zur herstellung eines kristallinen feststoffes aus glycin-n, n-diessigsäure-derivaten mit hinreichend geringer hygroskopizität

Publications (1)

Publication Number Publication Date
MX2012002244A true MX2012002244A (es) 2012-03-29

Family

ID=43500504

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2012002244A MX2012002244A (es) 2009-08-26 2010-08-25 Metodo para producir un solido cristalino de derivados de acido glicina-n, n-diacetico con higroscopicidad suficientemente reducida.

Country Status (17)

Country Link
US (2) US9376649B2 (es)
EP (1) EP2470496B2 (es)
JP (1) JP5756107B2 (es)
KR (1) KR101755736B1 (es)
CN (1) CN102574775B (es)
AU (1) AU2010288872A1 (es)
BR (1) BR112012004179B1 (es)
CA (1) CA2771916C (es)
DE (1) DE102009038951A1 (es)
ES (1) ES2563323T5 (es)
MX (1) MX2012002244A (es)
MY (1) MY158464A (es)
PL (1) PL2470496T5 (es)
RU (1) RU2551851C2 (es)
SG (1) SG178352A1 (es)
WO (1) WO2011023382A2 (es)
ZA (1) ZA201202132B (es)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
AU2010305833A1 (en) 2009-10-12 2012-04-19 Basf Se Method for producing a powder containing one or more complexing agent salts
DE102009060814A1 (de) 2009-12-30 2011-07-07 inprotec AG, 79423 Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält
MX342570B (es) * 2010-09-27 2016-10-05 Basf Se Proceso para producir granulos que comprende una o mas sales de agentes complejantes.
US9227915B2 (en) * 2011-05-03 2016-01-05 Basf Se Process for the preparation of a crystalline L-MGDA trialkali metal salt
GB2491619B (en) * 2011-06-09 2014-10-01 Pq Silicas Bv Builder granules and process for their preparation
WO2014090942A1 (en) 2012-12-14 2014-06-19 Akzo Nobel Chemicals International B.V. Crystalline particles of glutamic acid n,n-diacetic acid
US9738594B2 (en) 2012-12-14 2017-08-22 Akzo Nobel Chemicals International B.V. Crystalline particles of salts of glutamic acid N,N-diacetic acid
EP3143001B1 (en) 2014-05-13 2018-07-18 Akzo Nobel Chemicals International B.V. Process to crystallize chelating agents
WO2017097657A1 (en) * 2015-12-11 2017-06-15 Basf Se Process for manufacturing granules
BR112018075476B1 (pt) * 2016-06-20 2022-10-04 Basf Se Processo para produção de um pó ou grânulo, pó ou grânulo, e, uso de grânulos e de pós
RU2019129794A (ru) 2017-02-24 2021-03-25 Басф Се Способ получения твердой соли щелочного металла метилглициндиацетата (mgda) и твердые частицы
WO2019007943A1 (en) * 2017-07-07 2019-01-10 Akzo Nobel Chemicals International B.V. PROCESS FOR THE PREPARATION OF A DIACETIC AMINO ACID SOLID COMPOSITION
BR112020022158A2 (pt) 2018-05-30 2021-01-26 Basf Se processo para produzir sal de metal alcalino de diacetato de metilglicina sólido.
CN113382980B (zh) 2018-12-21 2024-06-21 诺力昂化学品国际有限公司 甲基甘氨酸n,n-二乙酸的易碎相组合物
KR20210062413A (ko) 2019-11-21 2021-05-31 (주)아모레퍼시픽 고함량의 락테이트 금속염 및 실리콘계 오일의 혼합물을 포함하는 w/s형 화장료 조성물
WO2021255525A1 (en) 2020-06-19 2021-12-23 Nouryon Chemicals International B.V. Process to prepare a co granule of methylglycine n,n diacetic acid salts employing a crumbly phase composition of methylglycine n,n diacetic acid salts

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3932316A (en) 1974-11-13 1976-01-13 The Procter & Gamble Company Free flowing detergent compositions containing benzoate salts
JPH0678225B2 (ja) * 1985-11-27 1994-10-05 株式会社林原生物化学研究所 脱水医薬品とその製造方法
DE4319935A1 (de) * 1993-06-16 1994-12-22 Basf Ag Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen
JP4711471B2 (ja) 1996-07-05 2011-06-29 三菱商事フードテック株式会社 結晶マルチトール及びそれを含有する含蜜結晶の製造方法
DE19649681A1 (de) * 1996-11-29 1998-06-04 Basf Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
MY131293A (en) * 2001-04-13 2007-08-30 Urea Casale Sa Fluid bed granulation apparatus
DE102004032320A1 (de) * 2004-07-02 2006-01-19 Basf Ag Mischpulver oder Mischgranulat auf Basis von MGDA
CN101687156B (zh) * 2007-07-03 2013-08-07 巴斯夫欧洲公司 生产主要包含α-氨基丙酸-N,N-二乙酸和/或一种或多种α-氨基丙酸-N,N-二乙酸衍生物的自由流动且存储稳定的固体的方法
PL3061744T3 (pl) 2008-04-01 2018-10-31 Unilever N.V. Wytwarzanie sypkich granul kwasu metyloglicynodioctowego
FR2935383B1 (fr) * 2008-08-26 2010-10-01 Pancosma Sa Pour L Ind Des Pro Procede et dispositif pour la fabrication de complexes organometalliques en poudre.
CA2762507C (en) * 2009-05-20 2018-08-21 Basf Se Process for the preparation of a powder comprising one or more derivatives of glycine-n,n-diacetic acid and/or one or more derivatives of glutamine-n,n-diacetic acid and methylglycine-n,n-diacetic acid trisodium salt powder
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
AU2010305833A1 (en) * 2009-10-12 2012-04-19 Basf Se Method for producing a powder containing one or more complexing agent salts
GB2491619B (en) * 2011-06-09 2014-10-01 Pq Silicas Bv Builder granules and process for their preparation

Also Published As

Publication number Publication date
CA2771916C (en) 2017-07-25
CA2771916A1 (en) 2011-03-03
KR20120089470A (ko) 2012-08-10
ZA201202132B (en) 2013-05-29
RU2551851C2 (ru) 2015-05-27
US20120149936A1 (en) 2012-06-14
CN102574775B (zh) 2014-09-24
EP2470496A2 (de) 2012-07-04
SG178352A1 (en) 2012-03-29
US20160221930A1 (en) 2016-08-04
ES2563323T3 (es) 2016-03-14
WO2011023382A3 (de) 2011-05-12
CN102574775A (zh) 2012-07-11
US9376649B2 (en) 2016-06-28
AU2010288872A1 (en) 2012-03-08
KR101755736B1 (ko) 2017-07-07
WO2011023382A2 (de) 2011-03-03
BR112012004179B1 (pt) 2018-09-11
PL2470496T3 (pl) 2016-06-30
EP2470496B2 (de) 2024-03-27
US9751829B2 (en) 2017-09-05
PL2470496T5 (pl) 2024-07-15
DE102009038951A1 (de) 2011-03-03
JP2013503119A (ja) 2013-01-31
BR112012004179A2 (pt) 2016-03-29
RU2012111127A (ru) 2013-10-10
JP5756107B2 (ja) 2015-07-29
ES2563323T5 (es) 2024-10-16
EP2470496B1 (de) 2016-01-06
MY158464A (en) 2016-10-14

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