YU48328B - Postupak za selektivno dobijanje hidratnih kristala - Google Patents
Postupak za selektivno dobijanje hidratnih kristalaInfo
- Publication number
- YU48328B YU48328B YU35491A YU35491A YU48328B YU 48328 B YU48328 B YU 48328B YU 35491 A YU35491 A YU 35491A YU 35491 A YU35491 A YU 35491A YU 48328 B YU48328 B YU 48328B
- Authority
- YU
- Yugoslavia
- Prior art keywords
- methyl
- procedure
- hydrate crystals
- selective obtaining
- benzoxazine
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- 239000013078 crystal Substances 0.000 title 1
- GSDSWSVVBLHKDQ-JTQLQIEISA-N Levofloxacin Chemical compound C([C@@H](N1C2=C(C(C(C(O)=O)=C1)=O)C=C1F)C)OC2=C1N1CCN(C)CC1 GSDSWSVVBLHKDQ-JTQLQIEISA-N 0.000 abstract 2
- 239000003125 aqueous solvent Substances 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 150000004682 monohydrates Chemical class 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D498/00—Heterocyclic compounds containing in the condensed system at least one hetero ring having nitrogen and oxygen atoms as the only ring hetero atoms
- C07D498/02—Heterocyclic compounds containing in the condensed system at least one hetero ring having nitrogen and oxygen atoms as the only ring hetero atoms in which the condensed system contains two hetero rings
- C07D498/06—Peri-condensed systems
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
HRP-354/91A HRP930086B1 (en) | 1990-03-01 | 1993-02-01 | Process for the selective production of hydrate crystals |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP5045490 | 1990-03-01 |
Publications (2)
Publication Number | Publication Date |
---|---|
YU35491A YU35491A (sh) | 1994-04-05 |
YU48328B true YU48328B (sh) | 1998-05-15 |
Family
ID=12859314
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
YU35491A YU48328B (sh) | 1990-03-01 | 1991-02-28 | Postupak za selektivno dobijanje hidratnih kristala |
Country Status (12)
Country | Link |
---|---|
US (1) | US5545737A (en, 2012) |
EP (1) | EP0444678B1 (en, 2012) |
KR (1) | KR970000045B1 (en, 2012) |
AT (1) | ATE157666T1 (en, 2012) |
DE (1) | DE69127485T2 (en, 2012) |
ES (1) | ES2106739T3 (en, 2012) |
GR (1) | GR3025276T3 (en, 2012) |
IE (1) | IE910692A1 (en, 2012) |
IN (1) | IN172207B (en, 2012) |
PT (1) | PT96917B (en, 2012) |
TW (1) | TW208013B (en, 2012) |
YU (1) | YU48328B (en, 2012) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ZA946853B (en) * | 1993-09-10 | 1995-04-24 | Daiichi Seiyaku Co | Crystals of antimicrobial compound. |
PE20011061A1 (es) | 2000-02-01 | 2001-11-20 | Procter & Gamble | Cristalizacion selectiva del acido 3-piridil-1-hidroxi-etiliden-1,1-bisfosfonico sodio como el hemipentahidrato o el monohidrato |
US6562974B2 (en) | 2000-02-01 | 2003-05-13 | The Procter & Gamble Company | Process for making geminal bisphosphonates |
EP1772457A3 (en) | 2001-10-03 | 2007-07-04 | Teva Pharmaceutical Industries Ltd. | Preparation of levofloxacin and forms thereof |
US7425628B2 (en) | 2001-10-03 | 2008-09-16 | Teva Pharmaceutical Industries Ltd. | Methods for the purification of levofloxacin |
AU2002365416A1 (en) * | 2001-11-29 | 2003-06-10 | Teva Pharmaceutical Industries Ltd. | Methods for the purification of levofloxacin |
US20060276463A1 (en) * | 2002-12-16 | 2006-12-07 | Sharma Tarun K | Pure levofloxacin hemihydrate and processes for preparation thereof |
KR100704641B1 (ko) * | 2004-07-21 | 2007-04-06 | 주식회사유한양행 | 고순도의 레보플록사신 제조방법 |
EP1797101A4 (en) * | 2004-09-17 | 2009-11-11 | Matrix Lab Ltd | IMPROVED PROCESS FOR THE PREPARATION OF LEVOFLOXACIN HEMIHYDRATE |
US20070244318A1 (en) * | 2004-11-08 | 2007-10-18 | Rao Davuluri R | Process for the Preparation of Levofloxacin Hemihydrate |
ES2255871B1 (es) * | 2004-12-31 | 2007-08-16 | Quimica Sintetica, S.A. | Procedimiento para la obtencion de levofloxacino exento de sales. |
CN1321121C (zh) * | 2005-04-21 | 2007-06-13 | 浙江医药股份有限公司新昌制药厂 | 左氧氟沙星制备及后处理方法 |
US7964723B2 (en) * | 2008-08-02 | 2011-06-21 | Apeloa-Kangyu | And practical process for exclusively producing (S)-9-fluoro-3-methyl-10-(4-methyl-1-piperazinyl)-7-oxo-2,3-dihydro-7H-pyrido-[1,2,3,de][1,4]benzoxazine-6-carboxylic acid hemihydrate |
CN101863904A (zh) * | 2010-07-08 | 2010-10-20 | 浙江东亚药业有限公司 | 一种高纯度左氧氟沙星半水合物的制备方法 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE203719C (en, 2012) * | 1907-11-02 | 1908-10-20 | ||
JPS5746986A (en) * | 1980-09-02 | 1982-03-17 | Dai Ichi Seiyaku Co Ltd | Pyrido(1,2,3-de)(1,4)benzoxazine derivative |
JPS57131769A (en) * | 1981-02-10 | 1982-08-14 | Kissei Pharmaceut Co Ltd | 4-(1-imidazolylmethyl)cinnamic acid hydrochloride monohydrate, its preparation and drug containing the same |
JPS5843977A (ja) * | 1981-09-09 | 1983-03-14 | Dai Ichi Seiyaku Co Ltd | ピリドベンズオキサジン誘導体の製法 |
JPS60226855A (ja) * | 1984-04-26 | 1985-11-12 | Nippon Kayaku Co Ltd | N−ベンジルオキシカルボニル−l−スレオニンアミド・1/2水和物およびその製造法 |
NO166131C (no) * | 1985-06-20 | 1991-06-05 | Daiichi Seiyaku Co | Analogifremgangsmaate for fremstilling av s(-)-pyridobenzoksazinforbindelser. |
ZA864518B (en) * | 1985-06-20 | 1987-03-25 | Daiichi Seiyaku Co | Optically active pyridobenzoxazine derivatives and intermediates thereof |
MY104139A (en) * | 1988-08-09 | 1994-02-28 | Daiichi Seiyaku Co | Antimicrobial agent for animals |
FI82240C (fi) * | 1988-10-20 | 1991-02-11 | Huhtamaeki Oy | Foerfarande foer framstaellning av farmakologiskt vaerdefullt s-timolol-hemihydrat. |
MTP1076B (en) * | 1990-01-12 | 1991-09-30 | Ciba Geigy Ag | Hemihydrate |
-
1990
- 1990-03-13 TW TW080108336A patent/TW208013B/zh active
-
1991
- 1991-02-28 IN IN175/MAS/91A patent/IN172207B/en unknown
- 1991-02-28 PT PT96917A patent/PT96917B/pt not_active IP Right Cessation
- 1991-02-28 YU YU35491A patent/YU48328B/sh unknown
- 1991-02-28 ES ES91103032T patent/ES2106739T3/es not_active Expired - Lifetime
- 1991-02-28 AT AT91103032T patent/ATE157666T1/de not_active IP Right Cessation
- 1991-02-28 KR KR1019910003413A patent/KR970000045B1/ko not_active Expired - Lifetime
- 1991-02-28 EP EP91103032A patent/EP0444678B1/en not_active Expired - Lifetime
- 1991-02-28 DE DE69127485T patent/DE69127485T2/de not_active Expired - Lifetime
- 1991-03-01 IE IE069291A patent/IE910692A1/en not_active IP Right Cessation
-
1994
- 1994-01-18 US US08/182,364 patent/US5545737A/en not_active Expired - Lifetime
-
1997
- 1997-11-05 GR GR970402914T patent/GR3025276T3/el unknown
Also Published As
Publication number | Publication date |
---|---|
KR970000045B1 (ko) | 1997-01-04 |
IN172207B (en, 2012) | 1993-05-01 |
KR910016748A (ko) | 1991-11-05 |
DE69127485D1 (de) | 1997-10-09 |
EP0444678B1 (en) | 1997-09-03 |
GR3025276T3 (en) | 1998-02-27 |
DE69127485T2 (de) | 1998-04-02 |
PT96917B (pt) | 1998-07-31 |
HK1002730A1 (en) | 1998-09-11 |
TW208013B (en, 2012) | 1993-06-21 |
US5545737A (en) | 1996-08-13 |
EP0444678A1 (en) | 1991-09-04 |
YU35491A (sh) | 1994-04-05 |
ATE157666T1 (de) | 1997-09-15 |
ES2106739T3 (es) | 1997-11-16 |
PT96917A (pt) | 1991-10-31 |
IE910692A1 (en) | 1991-09-11 |
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