WO2015088114A1 - 수소 음이온 함유물의 제조 방법 및 이를 이용하여 제조한 수소 음이온 함유물 - Google Patents

수소 음이온 함유물의 제조 방법 및 이를 이용하여 제조한 수소 음이온 함유물 Download PDF

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WO2015088114A1
WO2015088114A1 PCT/KR2014/005067 KR2014005067W WO2015088114A1 WO 2015088114 A1 WO2015088114 A1 WO 2015088114A1 KR 2014005067 W KR2014005067 W KR 2014005067W WO 2015088114 A1 WO2015088114 A1 WO 2015088114A1
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Prior art keywords
oxide
hydrogen
calcium
alkaline earth
negative ion
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PCT/KR2014/005067
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English (en)
French (fr)
Korean (ko)
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최태호
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최태호
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Priority to JP2016535013A priority Critical patent/JP6439994B2/ja
Priority to CN201480047256.6A priority patent/CN105472996A/zh
Publication of WO2015088114A1 publication Critical patent/WO2015088114A1/ko

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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38—Other non-alcoholic beverages
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/16—Inorganic salts, minerals or trace elements
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00—Drugs for dermatological disorders
    • A61P17/02—Drugs for dermatological disorders for treating wounds, ulcers, burns, scars, keloids, or the like
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00—Drugs for dermatological disorders
    • A61P17/18—Antioxidants, e.g. antiradicals

Definitions

  • the present invention relates to a method for producing a hydrogen anion content and a hydrogen anion content prepared using the same, more specifically, a method for producing a hydrogen anion content capable of promoting metabolism of cells and removing active oxygen in the body, and It relates to a hydrogen anion content prepared using this.
  • anion generators capable of purifying indoor air, anion products that remove mineral odors from tap water, and mineralize are being developed.
  • anion which has remained at the level of improvement of the living environment as described above, is now being developed as an edible product, and commercially available anion products are sold.
  • commercially available anionic products have poor solubility in water, which does not promote smooth antioxidant activity in the body.
  • commercially available anion products are not easy to store for a long time, causing a lot of side effects due to flour, etc. used to prepare anion products. Therefore, there is still a lot of research on the anion products that can be ingested.
  • Another object of the present invention is to provide a hydrogen anion content produced by the above production method.
  • a method for producing a hydrogen anion-containing product comprises a first firing step of producing a first calcined body by firing an alkaline earth metal compound containing an organic calcium carbonate; A second firing step of firing an alkaline earth metal oxide including the first firing body to produce a second firing body; And blending the second calcined body and the organic acid.
  • the first firing step may include firing the alkaline earth metal compound at 300 to 1000 ° C. for at least 2 hours.
  • the alkaline earth metal compound may further include a beryllium compound, a magnesium compound, a barium compound, or a mixture thereof.
  • the second firing step may include adding beryllium oxide, magnesium oxide, barium oxide or a mixture thereof.
  • the alkaline earth metal oxide may include 1 to 60 moles of beryllium oxide, magnesium oxide, barium oxide, or a mixture thereof based on 100 moles of calcium oxide.
  • the second firing step may include firing the alkaline earth metal oxide at 300 to 1000 ° C. for at least 2 hours under a hydrogen atmosphere.
  • the second fired body may be blended with 0.5 to 10 moles of organic acid based on 100 moles of calcium ions included in the second fired body.
  • Hydrogen anion content according to another embodiment of the present invention may be prepared by the above production method.
  • the hydrogen anion content has a pH of 6-12 immediately after dissolution in water; Has a redox potential of -0.1 mV to -900 mV immediately after dissolution in water; Or it may be one having a reducing power duration of 1 to 150 hours.
  • Hydrogen anion content according to an embodiment of the present invention can promote the metabolism of cells and remove the active oxygen in the body.
  • the hydrogen anion-containing content prepared by the manufacturing method according to an embodiment of the present invention is not sensitive to changes in the surrounding environment, for example, temperature, and is not denatured even when exposed to air, so that it is easy to store, various beverages or various It can be added to food materials to exhibit the above functions.
  • the hydrogen anion content may be added to food materials such as fruits, vegetables, fish and meat to prevent their oxidation to maintain high freshness for a long time.
  • the hydrogen anion content may restore the oxidized skin and traumatized skin by reducing action.
  • Example 1 is a photograph of an aqueous solution in which the hydrogen anion content prepared in Example 1 is dissolved.
  • Method for producing a hydrogen anion-containing product comprises a first firing step of producing a first calcined body by firing an alkaline earth metal compound containing an organic calcium carbonate; A second firing step of firing an alkaline earth metal oxide including the first firing body to produce a second firing body; And blending the second calcined body and the organic acid.
  • the organic calcium carbonate is an organic substance containing calcium carbonate, which is distinguished from calcium carbonate collected from an inorganic substance such as mineral.
  • Organic calcium carbonate contains a very small amount of heavy metals or no heavy metals compared to calcium carbonate taken from minerals such as minerals.
  • the organic calcium carbonate contains abundant minerals as compared to the calcium carbonate collected from inorganic substances such as minerals. Therefore, organocalcium carbonate is well suited for preparing edible hydrogen anion contents.
  • organic calcium carbonate for example, at least one selected from the group consisting of eggshell calcium, pearl calcium, shell calcium and seaweed calcium can be used.
  • the egg shell calcium can be obtained from egg shells, shell calcium can be obtained from oysters, shellfish, abalone or fish bones, and the seaweed calcium can be obtained from starfish or corals. Among them, eggshell calcium, shell calcium and mixtures thereof can be used as organocalcium carbonate in view of availability.
  • an organic earth carbonate compound is used by physically blending an organic calcium carbonate and a compound containing an alkaline earth metal except calcium.
  • an organic calcium carbonate is used as the alkaline earth metal compound.
  • the alkaline earth metal compound may further include a beryllium compound, a magnesium compound, a barium compound, or a mixture thereof in addition to the organic calcium carbonate.
  • Compounds containing alkaline earth metals other than the calcium affect the reducing power of the produced hydrogen anion-containing, it is possible to adjust the reducing power of the hydrogen anion-containing by employing an appropriate compound.
  • the alkaline earth metal compound may further include a magnesium compound in addition to the organic calcium carbonate.
  • the magnesium compound can efficiently control the reducing power of the hydrogen anion content.
  • by interacting with calcium it can help the extracorporeal discharge of sodium, promote the production of nitric oxide, increase the blood flow, and reduce acetaldehyde, which can relieve hangover and fatigue.
  • the type of magnesium compound is not particularly limited as long as it can produce magnesium oxide through a first firing step.
  • Such magnesium compounds include magnesium (Mg), magnesium chloride (MgCl 2 ), magnesium stearate (Mg (C 18 H 35 O 2 ) 2 ), magnesium carbonate (MgCO 3 ), magnesium sulfate (MgSO 4 ), magnesium hydroxide (Mg (OH) 2 ), magnesium triphosphate (Mg 3 (PO 4 ) 2 ), dibasic magnesium phosphate (MgHPO 4 ), magnesium silicate (MgSiO 3 ), magnesium gluconate (C 12 H 22 MgO 14 ), L- Magnesium lactate (Mg (C 3 H 5 O 3 ) 2 .2H 2 O), magnesium oxide (MgO), mixtures thereof, and the like.
  • Compounds containing alkaline earth metals other than the calcium may be used in an appropriate amount in consideration of the reducing power of the desired hydrogen anion content, the duration of the reducing power and / or the concentration of the hydrogen anion.
  • the compound is 1 to 60 moles, 1.6 to 57 moles, 1.6 to 50 moles, 1.6 to 40 moles, 1.6 to 30 moles, 5 to 20 moles, relative to 100 moles of calcium carbonate contained in the organic calcium carbonate, or It may be included in 5 to 15 moles.
  • the hydrogen anion content of the hydrogen anion content is too weak or the reducing power duration is too short, and if it exceeds the above range, the hydrogen anion content having a reducing power so large that it is not suitable for taking This can be obtained and such hydrogen anion content can interfere with metabolism in the body.
  • the magnesium compound when used as the compound including the alkaline earth metal except calcium, the magnesium compound may be used in an amount of 0.5 to 20 parts by weight based on 80 to 99.5 parts by weight of calcium carbonate contained in the organic calcium carbonate.
  • the hydrogen anion content which exhibits the above-mentioned effect can be provided.
  • the first firing step is about 300 to 1000 °C, about 400 to 900 °C, about 500 to 800 °C, about 600 to 800 °C, about 650 to 800 °C, about 600 to 750 °C or about 650 to 750 alkaline earth metal compound Firing at ° C.
  • the calcining of the alkaline earth metal compound may be performed for about 2 hours or more, about 3 hours or more, or about 4 hours or more.
  • the upper limit of the firing time is not particularly limited and may be adjusted, for example, to 10 hours or less.
  • the alkaline earth metal compound may not be oxidized to the desired level, and the calcining is performed for a time above the range at a temperature above the range. Enormous energy can be wasted in this case.
  • the first firing step is not particularly limited, but may be performed, for example, in the atmosphere.
  • the method of preparing the hydrogen anion-containing product may further include cooling the first calcined body after the first calcining step.
  • the method of cooling the first fired body is not particularly limited, but may be naturally cooled, for example.
  • the natural cooling may be performed by leaving until the temperature of the first fired body contained in the heated container reaches room temperature or the desired temperature.
  • the normal temperature means a natural temperature that is not heated or reduced in temperature.
  • the first fired body is a beryllium oxide (BeO) and magnesium oxide (MgO) obtained from a compound containing calcium oxide (CaO) obtained from organic calcium carbonate and alkaline earth metal except calcium. , Barium oxide (BaO) or a mixture thereof.
  • BeO beryllium oxide
  • MgO magnesium oxide
  • the first calcined body may include calcium oxide and magnesium oxide.
  • the first calcined body includes calcium oxide (CaO) obtained from organic calcium carbonate. Therefore, in this case, an oxide containing alkaline earth metal except calcium may be added in the second firing step so as to have the same configuration as the first fired body manufactured according to the first embodiment.
  • An oxide including an alkaline earth metal except for calcium may be beryllium oxide (BeO), magnesium oxide (MgO), barium oxide (BaO), or a mixture thereof.
  • the oxide including an alkaline earth metal except calcium may be magnesium oxide. That is, in the second embodiment, the first calcined body and the magnesium oxide can be used as the alkaline earth metal oxide. Therefore, alkaline earth metal oxide can have the same structure in 1st embodiment or 2nd embodiment.
  • the alkaline earth metal oxide is 1 to 60 moles, 1.6 to 57 moles, 1.6 to 50 moles, 1.6 to 40 moles, 1.6 to 30 moles, 5 to 20 moles or 5 to 15 moles of calcium, except for 100 moles of calcium oxide. Oxides including earth metals. As a result, a hydrogen anion content having an appropriate reducing power can be produced.
  • the first fired body of the first embodiment and the second embodiment includes various minerals derived from organic calcium carbonate in addition to the above-mentioned components.
  • the hydrogen anion containing product which is the final product, may also contain various minerals derived from organic calcium carbonate.
  • the second firing step is an alkaline earth metal oxide of about 300 to 1000 °C, about 300 to 900 °C, about 400 to 900 °C, about 400 to 800 °C, about 500 to 800 °C, about 500 to 700 °C or about 600 to 700 Firing at ° C.
  • the calcining of the alkaline earth metal oxide may be performed for about 2 hours or more, about 3 hours or more, or about 4 hours or more.
  • the upper limit of the firing time is not particularly limited and may be adjusted, for example, to 10 hours or less.
  • Alkaline earth metal oxide may not be reduced as desired if the firing is performed at a temperature below the range for less than the range, and if the firing is performed for a time above the range at a temperature above the range Enormous energy can be wasted.
  • the second firing step may be performed under a hydrogen atmosphere. Therefore, hydrogen gas can be supplied while calcining the alkaline earth metal oxide is in progress.
  • the hydrogen gas may be injected alone or in combination with other carrier gases.
  • the carrier gas any gas that is commonly used without particular limitation may be used as long as it is not reactive in the firing temperature range. Examples of the carrier gas may include nitrogen, helium, argon, and the like.
  • the method of preparing the hydrogen anion-containing product may further include cooling the second calcined body even after the second calcining step.
  • the method of cooling a 2nd baking body is not specifically limited, It can cool like the method of cooling the 1st baking body.
  • the production method of the hydrogen anion content includes combining the second calcined body and the organic acid after the second calcining step.
  • the second fired body includes calcium hydride (CaH 2 ) and hydrides of alkaline earth metals except calcium (MH 2 , M is Be, Mg, or Ba).
  • CaH 2 calcium hydride
  • M is Be, Mg, or Ba
  • the former is called a 2nd baking body and the latter is called a hydrogen anion containing thing.
  • the blending of the organic acid in the second fired body may be performed by adding the organic acid to the container containing the second fired body and physically mixing the acid.
  • organic acid for example, formic acid (formic acid), acetic acid (acetic acid), citric acid (citric acid), lactic acid (lactic acid), tartaric acid (tartaric acid), succinic acid (succinic acid) selected from the group consisting of 1 More than one species may be used.
  • a solid at room temperature may be used to prepare a hydrogen anion content in powder form.
  • citric acid, lactic acid, tartaric acid, succinic acid or mixtures thereof can be used as the organic acid.
  • the second calcined body is 0.5 to 10 mol, 0.88 to 10 mol, 1 to 9 mol, and 2 to 8 with respect to 100 mol of calcium ions contained in the second calcined body. Moles, 3 to 8 moles, 3 to 7 moles or 3 to 6 moles of organic acid.
  • the hydrogen anion content has an appropriate reducing power and an appropriate reducing power duration that cause an appropriate antioxidant action in the body.
  • the duration of reducing power means the time during which the aqueous solution in which the hydrogen anion content is dissolved exhibits a negative value of oxidation-reduction potential (ORP).
  • the hydrogen anion content may have a suitable pH in the body, including organic acids in the content in the above range.
  • the measured pH is about 10 to 12 by adding 400 mg of the second calcined body to 300 mL of water, the second calcined body may be blended with an organic acid in the above range to lower the pH to about 6 to 11. have. Therefore, the hydrogen anion content which exhibits the objective effect of this invention can be provided, without giving a burden to a body.
  • Another embodiment of the present invention provides a hydrogen anion content prepared by the above method.
  • Hydrogen anion content prepared according to the above production method may have a pH of 6 to 12, 7 to 12, 8 to 12, 8 to 11 or 9 to 11 immediately after dissolving in water.
  • the hydrogen anion content is -0.1mV to -900mV, -0.1mV to -800mV, -0.1mV to -700mV, -0.1mV to -600mV -0.1mV to -500mV, -10mV to-immediately after dissolving in water
  • the redox potential of 450mV, -100mV to -400mV, -150mV to -300mV, -180mV to -250mV, and -190mV to -230mV can be shown to have an appropriate reducing power.
  • the duration of the reducing power may be 1 to 150 hours, 5 to 120 hours, 10 to 100 hours, 30 to 100 hours, 50 to 100 hours or 70 to 100 hours.
  • the hydrogen anion content prepared according to the preparation method may have a pH of 9 to 11 immediately after dissolving in water.
  • the hydrogen anion content may be -190mV to -230mV redox potential immediately after dissolution in water.
  • the duration of the reducing power may be about 50 to 100 hours. Hydrogen anion content having such physical properties can be ingested without difficulty in the body, promote metabolism of cells, and smoothly remove free radicals from the body.
  • the hydrogen anion content having the above properties can be produced using an alkaline earth metal compound or oxide in an appropriate amount.
  • Hydrogen anion content prepared by the production method is not sensitive to changes in the surrounding environment can be utilized in various fields that require an antioxidant action.
  • the hydrogen anion content can be used, for example, to prevent the oxidation of fruits, vegetables, fish and meat.
  • the hydrogen anion content can restore oxidized skin and traumatized skin to a reducing action.
  • the hydrogen anion content may be used in various fields such as beauty ingredients, health foods and hangover beverages.
  • the washed oyster shell was calcined at a temperature of 700 ° C. for 4 hours in an air atmosphere to obtain a first fired body.
  • the first calcined body contained 56.08 g of calcium oxide.
  • citric acid was mixed with the second calcined body at a ratio of 17.5 wt% based on the total hydrogen anion content to prepare a hydrogen anion content in powder form.
  • a hydrogen anion content was prepared in the same manner as in Example 1 except for changing the content of magnesium oxide to 0.66 g in Example 1 as shown in Table 1 below.
  • a hydrogen anion content was prepared in the same manner as in Example 1, except that the content of magnesium oxide in Example 1 was changed to 9.53 g as shown in Table 1 below.
  • Example 1 As shown in Table 1, except that the content of magnesium oxide in Example 1 was changed to 22.95g, a hydrogen anion content was prepared in the same manner as in Example 1.
  • Example 1 As shown in Table 1, except that the content of citric acid blended in the second fired body in Example 1 was changed to a ratio of 12.5% by weight based on the total hydrogen anion content, the hydrogen anion content was the same as that of Example 1 Was prepared.
  • Example 1 As described in Table 1, except that the content of citric acid blended in the second calcined body in Example 1 was changed to a ratio of 25.0 wt% based on the total hydrogen anion content, the hydrogen anion content was the same as that of Example 1 Was prepared.
  • the redox potential (ORP) change, pH change, and reduction power duration of the hydrogen anion-containing product prepared in Example were measured, and the turbidity of the aqueous solution in which the hydrogen anion-containing solution was dissolved was observed.
  • the physical properties of the hydrogen anion-containing content of the example were compared with those of the tap water (Comparative Example 1) and the first calcined body (Comparative Example 2: The first calcined body of Example 1).
  • Duration of reducing power The time during which the aqueous solutions prepared above maintain a negative redox potential is defined as the duration of reducing power, and is oxidized from the time of dissolving the first calcined body or the hydrogen anion content. The time until the reduction potential became zero was measured.
  • Turbidity of the aqueous solution The aqueous solution in which the first calcined body or the hydrogen anion-containing substance was dissolved was visually observed to be cloudy and marked as 'cloudy', and when transparently observed, 'clear'. Representatively, a photograph of the aqueous solution of Example 1 is disclosed in FIG. 1.
  • the present invention promotes metabolism of cells and can remove free radicals in the body.
  • it since it is not sensitive to changes in the surrounding environment, for example, temperature, and is not denatured even when exposed to air, it is easy to store, and thus, it can be added to various beverages or various food ingredients to exhibit the above functions.
  • it can be added to food materials such as fruits, vegetables, fish and meat to prevent their oxidation to maintain high freshness for a long time.
  • oxidized and traumatized skin can be restored by a reducing action.

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  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
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  • Anti-Oxidant Or Stabilizer Compositions (AREA)
PCT/KR2014/005067 2013-12-09 2014-06-10 수소 음이온 함유물의 제조 방법 및 이를 이용하여 제조한 수소 음이온 함유물 WO2015088114A1 (ko)

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JP2016535013A JP6439994B2 (ja) 2013-12-09 2014-06-10 水素陰イオン含有物の製造方法
CN201480047256.6A CN105472996A (zh) 2013-12-09 2014-06-10 氢负离子内含物的制备方法及利用其来制备的氢负离子内含物

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KR10-2013-0152162 2013-12-09
KR1020130152162A KR101405431B1 (ko) 2013-12-09 2013-12-09 수소 음이온 함유물의 제조 방법 및 이를 이용하여 제조한 수소 음이온 함유물

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WO2018139682A1 (ko) * 2017-01-24 2018-08-02 (주)비피텍스 칼슘 항균제를 이용한 항균 원단의 제조방법
US20210205354A1 (en) * 2018-10-18 2021-07-08 Vovi C&E Co.,Ltd. Anti-inflammatory composition comprising hydrogen anions

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KR101881316B1 (ko) * 2016-10-07 2018-07-26 보비씨엔이(주) 항균성 및 항산화성을 갖는 조성물
KR101910334B1 (ko) 2016-10-07 2018-12-28 보비씨엔이(주) 항균성 섬유의 제조방법
JP6244051B1 (ja) * 2017-05-09 2017-12-06 株式会社アッチェ 水素担持粉末の製造方法
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JP6337192B1 (ja) * 2017-10-23 2018-06-06 株式会社アッチェ 水素担持粉末、並びに該水素担持粉末を含む食品及び肥料
CN108542794B (zh) * 2018-05-24 2021-02-02 河北云悦生物科技有限公司 一种富氢原料及护肤富氢产品
KR20200032460A (ko) * 2018-09-18 2020-03-26 보비씨엔이(주) 체내 알코올 및 아세트알데히드 분해기능을 갖는 숙취해소용 수소흡장 칼슘 함유 조성물
KR102230498B1 (ko) * 2019-07-31 2021-03-22 보비씨엔이(주) 골다공증 치료용 수소흡장 칼슘 함유 조성물
KR102403488B1 (ko) * 2020-03-30 2022-05-30 보비씨엔이(주) 수소음이온을 갖는 피부보습용 조성물
WO2024135810A1 (ja) * 2022-12-23 2024-06-27 サントリーホールディングス株式会社 容器詰め飲料

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