WO2015025752A1 - 植物栽培システムおよび植物栽培方法 - Google Patents
植物栽培システムおよび植物栽培方法 Download PDFInfo
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- WO2015025752A1 WO2015025752A1 PCT/JP2014/071141 JP2014071141W WO2015025752A1 WO 2015025752 A1 WO2015025752 A1 WO 2015025752A1 JP 2014071141 W JP2014071141 W JP 2014071141W WO 2015025752 A1 WO2015025752 A1 WO 2015025752A1
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- film
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- nutrient solution
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G31/00—Soilless cultivation, e.g. hydroponics
- A01G31/02—Special apparatus therefor
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G25/00—Watering gardens, fields, sports grounds or the like
- A01G25/02—Watering arrangements located above the soil which make use of perforated pipe-lines or pipe-lines with dispensing fittings, e.g. for drip irrigation
- A01G25/023—Dispensing fittings for drip irrigation, e.g. drippers
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G31/00—Soilless cultivation, e.g. hydroponics
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/20—Reduction of greenhouse gas [GHG] emissions in agriculture, e.g. CO2
- Y02P60/21—Dinitrogen oxide [N2O], e.g. using aquaponics, hydroponics or efficiency measures
Definitions
- the present invention relates to a plant cultivation system and a plant cultivation method using a nonporous hydrophilic film, particularly a polyvinyl alcohol (PVA) film.
- a nonporous hydrophilic film particularly a polyvinyl alcohol (PVA) film.
- Patent Document 1 Plant cultivation instrument and plant cultivation method for cultivating a plant by integrating the film and plant root on a hydrophilic film
- Patent Document 2 Plant cultivation instrument and plant cultivation method for irrigating the upper part of the film
- Patent Document 3 Plant cultivation system
- Patent Document 4 a plant cultivation system using means for continuously supplying nutrient solution to the lower surface side of the film
- Patent Literature 5 a plant cultivation system using means for continuously supplying nutrient solution to the lower surface side of the film
- the plant root If the plant root penetrates the film, the plant root will be in direct contact with the nutrient solution, and the plant cultivated on the film will be infected with bacteria and viruses that have propagated in the nutrient solution, Plants cannot be cultivated in a healthy state.
- the thickness of the film has to be at least 60 ⁇ m or more.
- the thickness of the film is increased, there is a problem that the growth rate of the plant is hindered because the permeation rate of the nutrient solution is lowered, or the cost of the film is increased.
- the present inventors have an equilibrium swelling degree of polyvinyl alcohol (PVA) film at a predetermined temperature in water (30 ° C.) in the range of 125% to 250%. By doing so, it discovered that it became a PVA-type film excellent in the absorptivity and permeability
- PVA polyvinyl alcohol
- the loss tangent (tan ⁇ ) of the PVA film at 30 ° C. is 0.005 or more and 0.2 or less, it is found that the PVA film has excellent film strength for plant cultivation, and the present invention has been completed. It was.
- the present invention Polyvinyl alcohol (PVA) film for cultivating plants thereon, nutrient solution holding means arranged so as to be in contact with the lower surface of the PVA film, and the nutrient solution under the PVA film
- a system for plant cultivation comprising means for supplying to the water; the equilibrium swelling degree of the PVA film in water (30 ° C.) is in the range of 125% to 250% and the equilibrium swelling state of the PVA film in water ( A system for plant cultivation, characterized in that a loss tangent (tan ⁇ ) at 30 ° C is 0.005 or more and 0.2 or less.
- the plant cultivation system according to any one of 1) to 3) above, further comprising a nutrient solution supply means for supplying the nutrient solution.
- a nutrient solution supply means for supplying the nutrient solution.
- the nutrient solution supply means is a drip irrigation tube installed between the PVA film and the nutrient solution holding means.
- a plant cultivation system including means for supplying; the equilibrium swelling degree of the PVA film in water (30 ° C.) in the range of 125% or more and 250% or less, and the equilibrium swelling state of the PVA film in water (30 A loss tangent (tan ⁇ ) at 0.005) is 0.005 or more and 0.2 or less, and provides a plant cultivation system, (2) placing the plant on the PVA-based film in the system; and (3) contacting the nutrient solution with the plant via the PVA-based film, thereby planting the plant on the PVA-based film.
- a plant cultivation method that includes cultivating a plant.
- the PVA film used in the present invention is made of PVA as a raw material, and the PVA is not particularly limited and can be produced by a known method. That is, it is obtained by saponifying a vinyl ester polymer obtained by polymerizing a vinyl ester compound.
- vinyl ester compounds examples include vinyl formate, vinyl acetate, vinyl trifluoroacetate, vinyl propionate, vinyl butyrate, vinyl caprate, vinyl laurate, vinyl versatate, vinyl palmitate, vinyl stearate, etc. Although used in combination, vinyl acetate is preferred for practical use.
- other monomers can be copolymerized in an amount of about 0.5 to 10 mol% within the range not impairing the object of the present invention.
- monomers include propylene and isobutylene.
- Olefins such as ⁇ -octene, ⁇ -dodecene, ⁇ -octadecene, unsaturated acids such as acrylic acid, methacrylic acid, crotonic acid, maleic acid, maleic anhydride, itaconic acid or salts thereof, mono- or dialkyl esters, etc.
- Nitriles such as acrylonitrile and methacrylonitrile, amides such as acrylamide and methacrylamide, olefin sulfonic acids such as ethylene sulfonic acid, allyl sulfonic acid and methallyl sulfonic acid or salts thereof, alkyl vinyl ethers, N-acrylamidomethyltrimethylammonium chloride , Allyl Polyoxyalkylenes such as limethylammonium chloride, dimethyldiallylammonium chloride, dimethylallyl vinyl ketone, N-vinyl pyrrolidone, vinyl chloride, vinylidene chloride, polyoxyethylene (meth) allyl ether, polyoxypropylene (meth) allyl ether (meta ) Polyoxyalkylene (meth) acrylates such as allyl ether, polyoxyethylene (meth) acrylate, polyoxypropylene (meth) acrylate, polyoxyalkylenes such as polyoxyethylene
- the polymerization (or copolymerization), there is no particular limitation and a known polymerization method is arbitrarily used. Usually, solution polymerization using an alcohol such as methanol, ethanol or isopropyl alcohol as a solvent is carried out. Of course, emulsion polymerization and suspension polymerization are also possible.
- the polymerization reaction is carried out using a known radical polymerization catalyst such as azobisisobutyronitrile, acetyl peroxide, benzoyl peroxide, lauroyl peroxide, and the reaction temperature is 35 ° C. to 200 ° C. (more preferably 50 ° C.). It is selected from the range of about ⁇ 80 ° C.
- the polymer is dissolved in an alcohol or an alcohol / fatty acid ester mixed solvent in the presence of an alkali catalyst.
- the alcohol include methanol, ethanol, butanol and the like.
- the fatty acid ester solvent include methyl acetate, ethyl acetate, butyl acetate and the like, and benzene, hexane and the like may be used in combination.
- the concentration of the copolymer in the alcohol is selected from the range of 20 to 50% by weight.
- alkali catalysts such as alkali metal hydroxides and alcoholates such as sodium hydroxide, potassium hydroxide, sodium methylate, sodium ethylate and potassium methylate can be used.
- the amount of the catalyst used may be 1 to 100 mmol equivalents relative to the vinyl ester copolymer.
- it may be saponified with an acid catalyst such as hydrochloric acid, sulfuric acid, p-toluenesulfonic acid or the like.
- the saponification degree of PVA is preferably 90 mol% or more (more preferably 95 mol% or more, particularly 99 mol% or more). When the saponification degree is less than 90 mol%, the water resistance may decrease. Absent.
- the average degree of polymerization of PVA is preferably 1100 or more (more preferably 1300 to 4500, particularly 1300 to 4200). If the average degree of polymerization is less than 1100, the strength as a film cannot be obtained, and breakage or the like may occur. It may occur easily and is not preferable.
- the average degree of polymerization conforms to JIS K6726.
- the amount of sodium acetate contained can be adjusted to 0.8% by weight or less (more preferably 0.5% by weight or less) in order to improve heat resistance and coloring prevention ability. preferable.
- a PVA solution used for film production a PVA aqueous solution having a PVA content (concentration) of 5 to 70% by weight (more preferably 10 to 60% by weight) may be prepared.
- aqueous solutions may contain, as necessary, polyhydric alcohols such as ethylene glycol, glycerin, polyethylene glycol, diethylene glycol, and triethylene glycol, antioxidants such as phenols and amines, and stabilizers such as phosphate esters.
- polyhydric alcohols such as ethylene glycol, glycerin, polyethylene glycol, diethylene glycol, and triethylene glycol
- antioxidants such as phenols and amines
- stabilizers such as phosphate esters.
- Ordinary additives such as colorants, fragrances, bulking agents, defoaming agents, release agents, ultraviolet absorbers, inorganic powders, and surfactants may be appropriately blended.
- water-soluble resins other than polyvinyl alcohol such as starch, carboxymethylcellulose, methylcellulose, and hydroxymethylcellulose.
- the PVA aqueous solution prepared above is formed into a film by a film forming machine (extruder).
- the melt kneading temperature in the extruder is preferably from 55 to 140 ° C. (more preferably from 55 to 130 ° C.). If the temperature is less than 55 ° C., the film skin will be defective.
- the film formed by extrusion is then dried, and the drying temperature at this time is preferably 70 to 120 ° C. (more preferably 80 to 100 ° C.). If it takes too much or the residual moisture becomes excessive, and the temperature exceeds 120 ° C., the flexibility of the film is lost, which may hinder the subsequent stretching process, which is not preferable.
- the first prepared aqueous solution can be used for film formation as it is, but this is once pelletized or flaked in a water-containing state, and then supplied to a film forming machine to perform extrusion film formation. It is also possible.
- a PVA film used in the plant cultivation system of the present invention can be obtained.
- such a film is stretched so that the physical properties of flexibility and mechanical strength can be stably imparted.
- a stretching method will be described.
- the film may be uniaxially stretched in the longitudinal (machine) direction, but biaxially stretching in both the longitudinal and lateral directions is preferable because the above physical properties can be further improved.
- Such biaxial stretching may be either sequential biaxial stretching or simultaneous biaxial stretching.
- the water content of the PVA film obtained above is 5 to 30% by weight (more preferably 20 to 30% by weight). %) Is preferable, and when the moisture content is outside these ranges, the draw ratio cannot be sufficiently increased, which is not preferable.
- the adjustment of the moisture content and the moisture content is adjusted by drying the PVA film or by immersing or conditioning the PVA film having a moisture content of less than 5% by weight in water. The method etc. which adjust or can be mentioned.
- the draw ratio is not particularly limited, but the draw ratio in the longitudinal direction is 1.5 to 5.0, preferably 2.0 to 5.0 times, the draw ratio in the transverse direction is 1.5 to 5.0, Preferably, it is 2.0 to 5.0 times, and when the draw ratio in the machine direction is less than 1.5 times, it is difficult to improve physical properties by stretching, that is, to reduce loss tangent (tan ⁇ ) in a swollen state in water, If it exceeds 5.0 times, the film tends to tear in the longitudinal direction, which is not preferable.
- the stretching ratio in the transverse direction is less than 1.5 times, it is difficult to improve physical properties by stretching, that is, loss tangent (tan ⁇ ) reduction in a swollen state in water, and if it exceeds 5.0 times, the film will be broken, which is not preferable. .
- the temperature of the heat setting is preferably selected to be lower than the melting point of polyvinyl alcohol.
- the temperature is lower than the melting point by 80 ° C. or more, the dimensional stability is poor and the shrinkage rate is increased.
- the temperature is higher than the melting point, the thickness variation of the film is increased.
- the heat setting temperature is preferably 140 to 250 ° C.
- the heat setting time is preferably 1 to 30 seconds, more preferably 5 to 10 seconds.
- the heat setting may be performed in one step or divided into multiple steps depending on different temperatures and times, but in order to obtain the desired physical property value, that is, the loss tangent (tan ⁇ ) in the swollen state in water, it is divided into multiple steps. It is preferable to carry out.
- the biaxially stretched PVA film is subjected to water washing and drying as necessary, but the water washing method and the drying method are not particularly limited. For example, it is conceivable to adjust the amount of water by immersing in a water bath at an appropriate temperature and allowing it to contain water, and then drying by applying normal temperature air or high temperature air.
- the thickness of the PVA film used in the present invention is preferably 5 to 100 ⁇ m (more preferably 10 to 60 ⁇ m). Below this range, it becomes difficult for the PVA film to withstand the penetration of plant roots, and when it exceeds this range, it takes time to penetrate the fertilizer components. This range is also advantageous in industrial productivity.
- the equilibrium swelling degree in water (30 ° C.) of the PVA film used in the present invention is preferably in the range of 125% to 250%, more preferably 150% to 200%. If the equilibrium swelling degree of the PVA film is below this range, the permeability of water and fertilizer components will be insufficient, and the growth rate of the plant will be slow. On the other hand, when the equilibrium swelling degree of the PVA film exceeds this range, the strength of the PVA film in water decreases and it becomes difficult to withstand penetration of plant roots.
- the equilibrium swelling degree of PVA film in water (30 ° C.) is measured as follows. First, a dry PVA film is cut into a 20 cm ⁇ 20 cm square, and its weight (a) g is measured. Next, the cut-out PVA film is immersed in 30 ° C. water and left to stand for 30 minutes. The film is taken out from the water, excess water adhering to the film surface is quickly wiped off, and the weight (b) g of the film is measured. The equilibrium swelling degree is calculated as b / a x 100%.
- the dynamic viscoelastic behavior required for the PVA film of the present invention is that the storage elastic modulus (G ′) of the film in an equilibrium swelling state in water (30 ° C.) is 5,000 Pa to 100,000 Pa. More preferably, it is the range of 10,000 Pa or more and 80,000 Pa or less.
- the dynamic viscoelastic behavior required for the PVA-based film of the present invention is that the loss elastic modulus (G ′′) of the film in an underwater (30 ° C.) equilibrium swelling state is 100 Pa or more and 10,000 Pa or less. The range is from 300 Pa to 8,000 Pa.
- the dynamic viscoelastic behavior required for the PVA film of the present invention is the ratio of loss elastic modulus (G ′′) to storage elastic modulus (G ′) (G ′′ / G ′) of the film in an equilibrium swelling state in water (30 ° C.). ) Is a loss tangent (tan ⁇ ) of 0.005 or more and 0.2 or less. More preferably, it is the range of 0.01 or more and 0.1 or less.
- the PVA film swollen with water is a hydrogel and behaves as a viscoelastic body.
- a viscoelastic body When a viscoelastic body is deformed by applying stress, most of the applied force is stored as energy of internal deformation and becomes a driving force for restoration when the stress is removed, but some of the internal molecular movement accompanying strain is part of it. It is consumed due to friction and eventually turns into heat.
- a value indicating the magnitude of the internal friction is a loss tangent (Tan ⁇ ).
- the loss tangent (Tan ⁇ ) of the PVA film swollen with water is small has a strong property of returning to its original state even when it is deformed.
- a large loss tangent (Tan ⁇ ) means that when a stress to be deformed is applied, molecular migration is likely to occur in the PVA film swollen with water, and the stress is relaxed by the deformation.
- the penetration of PVA film by plant roots is considered to occur as follows.
- the roots that are in close contact with the film seek the nutrients present on the lower surface of the film and stretch while dragging the film toward the lower surface of the film.
- stress is generated in the film due to elongation of the roots.
- the PVA film itself is deformed by molecular movement inside the PVA film in an attempt to relieve stress due to root elongation.
- the root penetrates the film having a large loss tangent (Tan ⁇ ). That is, the PVA film swollen with water leads to ductile fracture.
- the dynamic viscoelastic behavior of the underwater equilibrium swollen PVA film is observed as follows. That is, storage modulus (G '), loss modulus (G "), loss tangent (measured when a 1Hz vibration is applied to a film immersed in water at 30 ° C for 30 minutes in a 30 ° C saturated water vapor environment ( tan ⁇ ) is measured.
- the dynamic viscoelastic behavior of an underwater equilibrium swollen PVA film is observed using a stress-controlled viscoelasticity measuring apparatus (Rheometer AR-500, manufactured by TA Instruments Japan Co., Ltd.). . Shape and dimensions of measurement cell: Stainless steel parallel disk (diameter: 4.0 cm), aluminum solvent trap used. Observation frequency: 1 Hz. Measurement temperature: 30 ° C. Applied stress and displacement: in the linear region. Specifically, the applied stress is, for example, 10 Pa to 200 Pa, and the displacement is 10 ⁇ 6 radians to 10 ⁇ 5 radians.
- the present invention aims to perform plant cultivation using the PVA film obtained as described above in a plant cultivation system, and the plant cultivation system and the plant cultivation method will be specifically described.
- the PVA film of the present invention is indispensable as a component of the plant cultivation system of the present invention, but can be roughly divided into two types depending on the difference in nutrient solution holding means.
- the first type is that the nutrient solution holding means is a hydroponics tank, and the nutrient solution arranged so as to come into contact with the lower surface of the PVA film of the present invention is accommodated in the hydroponics tank.
- This is a plant cultivation system.
- Patent Document 1 Such a system is disclosed in Patent Document 1.
- the nutrient solution holding means has a water-impermeable surface, and the PVA film of the present invention is laid thereon, and between the PVA film of the present invention and the nutrient solution holding means.
- a plant cultivation system characterized by further comprising a nutrient solution supply means for supplying the nutrient solution continuously or intermittently.
- a typical nutrient solution supply means is the PVA film of the present invention and the nutrient solution holding system.
- a drip irrigation tube placed between the means. That is, this second type of cultivation system is a system having a multilayer structure in which the nutrient solution holding means is a base material layer and the PVA film of the present invention is laminated directly or indirectly thereon. Such a system is disclosed in Patent Document 5.
- FIG. 1 is a schematic cross-sectional view showing a basic aspect of a first type of plant cultivation system.
- a water tank (2) is installed under the PVA film (1) of the present invention, and a nutrient solution (3) containing a fertilizer component is accommodated in the water tank.
- the nutrient solution (3) is absorbed by the PVA film (1) of the present invention, and the root (5) of the plant (4) is in close contact with the upper surface of the PVA film (1) of the present invention. Absorbs water and fertilizer components contained in PVA film (1).
- a support for plant cultivation such as soil (6) and / or a water-permeable or low-permeability evaporation suppressing member (for example, mulching described later) on the PVA film (1).
- Material) or fixed planting board (7) can be arranged.
- the plant cultivation support (6) is disposed on the PVA film (1), the effect of protecting the roots of the plant can be obtained.
- an evaporation suppression member or a fixed planting plate (7) is disposed, water vapor evaporating from the PVA film (1) into the atmosphere is condensed on the surface of the evaporation suppression member or the plant cultivation support (6). Plants can be used with water vapor as water.
- the nutrient solution (3) containing the fertilizer component is supplied to the plant via the PVA film (1) of the present invention.
- the surface of water or nutrient solution is in contact with the air layer, so that bacteria and fungi in the air It is easily mixed, and bacteria and fungi propagate to the roots of plants, causing significant growth problems and plant diseases.
- the root of the plant absorbs oxygen dissolved in water, so the amount of dissolved oxygen in water used for cultivation exceeds a certain level. There was a need to keep.
- the root of the plant is in the air layer on the PVA film (1) of the present invention, so that oxygen can be absorbed from the air.
- means for fine mist spraying (8) for example, a valve
- water, nutrient solution or agricultural chemical diluent can be sprayed intermittently.
- plant roots cultivated on the PVA film (1) of the present invention try to absorb nutrient solution through the PVA film (1) of the present invention, thereby And the PVA film (1) of the present invention are substantially integrated.
- PVA film of the present invention In the plant cultivation system of the present invention, the PVA film of the present invention for cultivating a plant thereon is essential. Although the production method and characteristic physical properties of the PVA film of the present invention used in the present invention have been described above, those satisfying all the various physical properties described later are preferable.
- the PVA-based film of the present invention is a film that can be “substantially integrated with the roots of a plant” that is being cultivated.
- the film “which can be substantially integrated with the roots of the plant body” means that when the plant is cultivated for 35 days on the PVA film of the present invention of the plant cultivation system of the present invention, the PVA film of the present invention is It is a film having a peel strength of 10 g or more for peeling from the roots of cultivated plants.
- the “integration test” for measuring the integration of the root and the film can be performed as follows.
- the film to be tested 200 x 200mm
- seedlings of sunny lettuce (one real leaf) 2 are planted.
- the rice cake is placed in a bowl filled with 240 to 300 g of nutrient solution, and the film is brought into contact with the nutrient solution to grow seedlings.
- Cultivation is carried out in a house, using natural light, at a temperature of 0 to 25 ° C., and a humidity of 50 to 90% RH for 35 days.
- the stems and leaves are cut at the roots of the cultivated plants, and the film is cut into a width of 5 cm (length: about 20 cm) so that the stems of the film with which the roots are closely attached are centered to form a test piece.
- the (BA) gram obtained by subtracting the initial weight from this value is the peeling load of 5 cm in width, and this peeling load is the peeling strength.
- the peel strength of the PVA film of the present invention used in the present invention is preferably 10 g or more, more preferably 30 g or more, and most preferably 100 g or more.
- the plant When a plant is cultivated using the plant cultivation system of the present invention, the plant absorbs the fertilizer as ions through the film. Therefore, the salt (ion) permeability of the film used affects the amount of fertilizer component given to the plant.
- a film having a difference in degree (EC) of 4.5 dS / m or less is preferable.
- the difference in electrical conductivity between water and salt water is more preferably 3.5 dS / m or less, and most preferably 2.0 dS / m or less.
- Electrical conductivity is an index of the amount of salts (or ions) dissolved in the liquid and is also called specific conductivity.
- EC Electrical conductivity
- Siemens S
- S Siemens
- mS / cm which is a unit of 1/1000, is used (in the international unit system, dS / m (d is deci)).
- the ion permeability of the film can be measured as follows. 10 g of commercially available salt is dissolved in 2000 ml of water to make 0.5% salt water (EC: about 9 dS / m). Using the “Zaru Bowl Set”, place the film to be tested (size: 200-260 ⁇ 200-260 mm) on the sieve and add 150 g of water onto the film. On the other hand, 150 g of the above-mentioned salt water is added to the bowl side, and the entire system obtained is wrapped with a food wrap (polyvinylidene chloride film, trade name: Saran Wrap (registered trademark), manufactured by Asahi Kasei Co., Ltd.) to prevent evaporation of moisture.
- a food wrap polyvinylidene chloride film, trade name: Saran Wrap (registered trademark), manufactured by Asahi Kasei Co., Ltd.
- the PVA film of the present invention preferably exhibits a predetermined glucose permeability from the viewpoint of facilitating nutrient absorption (organic matter) of plant roots via the PVA film of the present invention.
- This film with excellent glucose permeability is obtained at the cultivation temperature of water and glucose solution when water and 5% glucose aqueous solution are opposed to each other for 3 days (72 hours) through the PVA film of the present invention.
- It is a film having a difference in measured density (Brix%) of 4 or less, more preferably 3 or less, more preferably 2 or less, and most preferably 1.5 or less.
- the glucose permeability of the film can be measured as follows. A 5% glucose solution is prepared using commercially available glucose (glucose). Using the same “Zaru Bowl Set” as in the ion permeability test above, place the PVA film of the present invention to be tested (size: 200 to 260 ⁇ 200 to 260 mm) on the sieve and add 150 g of water onto the film. . On the other hand, 150 g of the above glucose solution is added to the bowl side, and the entire system obtained is wrapped in a food wrap (polyvinylidene chloride film, trade name: Saran Wrap (registered trademark), manufactured by Asahi Kasei Co., Ltd.) to prevent moisture evaporation. . In this state, the sample is left at room temperature, and the sugar content (Brix%) on the water side and glucose solution side is measured with a saccharimeter every 24 hrs.
- a food wrap polyvinylidene chloride film, trade name: Saran Wrap (registered trademark), manufactured by
- the PVA film of the present invention preferably has a water impermeability of 10 cm or more as a water pressure resistance.
- a water impermeability of 10 cm or more as a water pressure resistance.
- the water pressure resistance can be measured by a method according to JIS L1092 (Method B).
- the water pressure resistance of the PVA film of the present invention used in the present invention is preferably 10 cm or more, more preferably 20 cm or more, still more preferably 30 cm or more, and particularly preferably 200 cm or more.
- a plant cultivation support such as soil can be disposed on the PVA film of the present invention in order to protect the roots of the plant body.
- or culture medium normally used can be used. Examples of such soil or medium include soil used for soil cultivation and medium used for hydroponics.
- inorganic supports for plant cultivation include natural sand, rubble, and pumice sand, and processed products (high temperature firing etc.) include rock wool, vermiculite, perlite, ceramic, rice husk charcoal, etc.
- processed products include rock wool, vermiculite, perlite, ceramic, rice husk charcoal, etc.
- the support for cultivation include natural peat moss, coconut fiber, bark culture medium, rice husk, neat and sotan, and synthetic granular phenol resins. These may be used alone or in combination as appropriate. You can also. Synthetic fiber cloth or non-woven fabric can also be used as a plant cultivation support.
- ⁇ Minimum fertilizer and trace elements may be added to the plant cultivation support.
- the root of the plant grows to the extent that water or nutrients can be absorbed from the water / nutrient solution in contact with the PVA film, in other words, the root and the PVA film of the present invention Until these are integrated, it is desirable to add nutrients to the plant cultivation support on the PVA film of the present invention as "minimum required fertilizer and trace elements" mentioned here.
- the plant cultivation system of the present invention includes nutrient solution holding means for holding the nutrient solution under the PVA film of the present invention.
- nutrient solution holding means for holding the nutrient solution under the PVA film of the present invention.
- either a container-shaped nutrient solution holding means for storing a nutrient solution or a nutrient solution holding layer functioning as a base material layer having a water-impermeable surface can be used.
- the container-shaped nutrient solution holding means for storing the nutrient solution is not particularly limited as long as it is a container capable of holding a necessary amount of nutrient solution, and the material thereof is light weight, easy moldability and low cost.
- general-purpose plastics such as polystyrene, polypropylene, polyvinyl chloride, polyethylene, and polyacrylate can be suitably used.
- a conventionally used hydroponics tank can be used.
- the water-impermeable surface of the nutrient solution holding layer is not particularly limited as long as it is made of a material that does not allow water to pass through, and examples thereof include synthetic resin, wood, metal, and ceramic.
- the shape of the nutrient solution holding layer is not particularly limited, and examples thereof include a film shape, a sheet shape, a plate shape, and a box shape.
- the nutrient solution supply means is not particularly limited as long as it is a means conventionally used for continuous or intermittent supply of water or nutrient solution.
- a drip irrigation tube also referred to as “drip tube” capable of supplying a nutrient solution little by little.
- the water-absorbing material is further mixed with the PVA film of the present invention. It can be placed between the permeable surfaces.
- the water-absorbing material is basically not particularly limited as long as it is a material that absorbs and holds water. Examples include sponges and non-woven fabrics made from synthetic resins, fabrics made from woven fabrics, plant fibers, chips, powders, or materials commonly used as plant supports such as peat moss and moss. Can also be used.
- plants that can be cultivated using the plant cultivation system of the present invention there is no particular limitation on the plants that can be cultivated using the plant cultivation system of the present invention, and all plants that are normally grown in the fields of agriculture, forestry, and horticulture can be targeted.
- the cultivation method of the present invention is (1) the PVA film of the present invention for cultivating a plant thereon, a nutrient solution for promoting the growth of the plant, and disposed so as to contact the lower surface of the film A plant culture system comprising a nutrient solution and a nutrient solution holding means for holding the nutrient solution under the film is provided. (2) The PVA film of the present invention in the system A plant cultivation method comprising cultivating a plant on the film by placing the plant on the substrate and (3) contacting the nutrient solution with the plant through the film.
- the plant can be placed in the seed or seedling state on the PVA film of the present invention that has absorbed the nutrient solution.
- the plant When seeded on the film in a seed state, it is necessary to germinate and root first, and a small amount of irrigation necessary for seed germination and rooting is performed.
- a large amount of water is present on the film, the integration of the roots of the plant and the film is hindered, so it is necessary to keep the minimum watering necessary for germination and rooting of seeds.
- the plant cultivation support having high water retention is arranged on the film, it is easy to maintain a wet state around the root while avoiding the presence of a large amount of moisture on the film as described above. preferable.
- PVA film production example Example 1 Polyvinyl alcohol in which 40 parts of PVA (average saponification degree 99.7 mol%, average polymerization degree 1700, 4% aqueous solution viscosity (25 ° C.) 40 mPa ⁇ s, sodium acetate content 0.3%) is dissolved in 60 parts of water
- the cooled film was peeled off from the cast roll and dried for 30 seconds using 10 continuous rotary heating rolls adjusted to 90 ° C. to prepare a PVA film having a moisture content of 25%.
- the PVA film is stretched 3 times in the longitudinal direction, then stretched 3.5 times in the transverse direction by a tenter stretching machine to form a biaxially stretched PVA film, and then heat treated at 130 ° C. for 8 seconds (first stage heat treatment). Subsequently, a heat treatment (second-stage heat treatment) was performed at 170 ° C. for 8 seconds to obtain a biaxially stretched PVA film (F-1, thickness 30 ⁇ m) having a water content of 0.8%.
- the obtained film having a thickness of 30 ⁇ m was cut into a square having a winding direction of 20.0 cm and a width direction of 20.0 cm, and its weight was measured to be 1.55 g.
- the weight was 2.85 g.
- Example 2 In Example 1, a water content of 0.8 was obtained in the same manner as in Example 1 except that the speed after the cast roll cooled to 5 ° C. was changed to 0.75 times to prepare a PVA film having a water content of 25%. % Biaxially stretched PVA film (F-2, thickness 40 ⁇ m). When the equilibrium swelling degree in water (30 ° C.) was determined in the same manner as in Example 1, it was calculated to be 183%.
- Example 3 In Example 1, after obtaining a biaxially stretched PVA film, heat treatment was performed at 145 ° C. for 8 seconds (first-stage heat treatment), followed by heat treatment at 180 ° C. for 8 seconds (second-stage heat treatment). In the same manner as in Example 1, a biaxially stretched PVA film (F-3, thickness 30 ⁇ m) having a water content of 0.8% was obtained. When the equilibrium swelling degree in water (30 ° C.) was determined in the same manner as in Example 1, it was calculated to be 152%.
- Example 4 In Example 3, a water content of 0.8 was obtained in the same manner as in Example 3 except that the speed after the cast roll cooled to 5 ° C. was changed to 0.75 times to prepare a PVA film having a water content of 25%. % Biaxially stretched PVA film (F-4, thickness 40 ⁇ m). When the equilibrium swelling degree in water (30 ° C.) was determined in the same manner as in Example 1, it was calculated to be 152%.
- Comparative Example 1 (F-5) PVA (average saponification degree 99.7 mol%, average polymerization degree 1700, 4% aqueous solution viscosity (25 ° C.) 40 mPa ⁇ s, sodium acetate content 0.3%), plasticizer 12 parts glycerin, surfactant As a solution, 1.2 parts of polyoxyethylene sorbitan monolaurate was dissolved in water to obtain an 18% aqueous dispersion.
- Comparative Example 2 (F-6) A PVA film (F-6, thickness 60 ⁇ m) was obtained in the same manner as in Comparative Example 1 except that the film was formed at a speed of 12 m / min in Comparative Example 1. The obtained film (60 ⁇ m) was separately dried at 200 ° C. for 60 seconds to obtain a heat-treated film. When the equilibrium swelling degree in water (30 ° C.) was determined in the same manner as in Example 1, it was calculated to be 127%.
- PVA average saponification degree 99.7 mol%, average polymerization degree 1700, 4% aqueous solution viscosity (25 ° C.) 40 mPa ⁇ s, sodium acetate content 0.3%)
- the cooled film was peeled off from the cast roll and dried for 30 seconds using 10 continuous rotary heating rolls adjusted to 90 ° C. to prepare a PVA film having a moisture content of 25%.
- the polyvinyl alcohol film was stretched 3 times in the longitudinal direction, then stretched 3.5 times in the transverse direction by a tenter stretching machine to form a biaxially stretched PVA film, and then heat treated at 165 ° C.
- Comparative Example 4 (F-8) The equilibrium swelling degree in water (30 ° C.) of “Imec Film” (thickness: 65 ⁇ m) sold by Meviol Co., Ltd. was calculated in the same manner as in Example 1, and was calculated to be 148%.
- Comparative Example 5 The equilibrium swelling degree in water (30 ° C.) of “Imec Film 2” (thickness 60 ⁇ m) sold by Meviol Co., Ltd. was calculated in the same manner as in Example 1 and was calculated to be 153%.
- Example 6 Measurement of Dynamic Elastic Modulus
- the film samples (F-1) to (F-9) of Examples 1 to 4 and Comparative Examples 1 to 5 were each immersed in water at 30 ° C. for 30 minutes, cut into a 4 cm diameter circle, and stress-controlled viscoelasticity Dynamic viscoelastic behavior was observed using a measuring device (Rheometer AR-500, manufactured by TA Instruments Japan Co., Ltd.).
- the measurement conditions were as follows.
- Shape and dimensions of measurement cell Stainless steel parallel disk (diameter: 4.0 cm), aluminum solvent trap used. Observation frequency: 1 Hz. Measurement temperature: 30 °C Applied stress and displacement: in the linear region. Specifically, the applied stress is 10 Pa to 200 Pa, and the displacement is 10 ⁇ 6 radians to 10 ⁇ 5 radians.
- the PVA film in equilibrium swelling state is taken out of water, cut into a 4 cm diameter circle in accordance with a stainless steel parallel disk (diameter: 4.0 cm), which is a measurement device, and the solvent remains in close contact with the measurement device.
- a trap and water as a solvent were placed on it and attached to the measuring device.
- the measurement stage was raised, the PVA film to be measured was sandwiched between the measurement device and the measurement stage, and the gap was adjusted so that the film was in close contact with the measurement device and the measurement stage. At this time, care was taken not to compress the film so that no slip would occur between the PVA film and the measuring device and measuring stage.
- the temperature of the measurement stage was set to 30 ° C., and dynamic viscoelasticity was observed under stress and displacement within the linear region at an observation frequency of 1 Hz, and the loss tangent (tan ⁇ ) was obtained.
- the results for each sample were compared and summarized in Table 1.
- An A4 size PVA film obtained in the comparative example was placed. Place a coconut chip as a soil on a PVA film with a thickness of 1.5cm, sow turf seeds (Western turf “Perennial ryegrass accent
- Example 1 the plants grew smoothly with roots on the PVA film, and the roots of the plants were prevented from penetrating the film over 150 days.
- Comparative Example 3 since the film permeability of nutrients was low, plant growth was suppressed.
- Comparative Examples 1, 2, 4, and 5 the strength of the film was insufficient, so that plant roots penetrated the film in a relatively short period of time.
- the present invention can be used in a wide range of industries including plant cultivation, such as agriculture, horticulture, and pharmaceutical manufacturing.
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Abstract
Description
1)植物をその上で栽培するためのポリビニルアルコール(PVA)系フィルム、該PVA系フィルムの下面に接触するように配置された養液保持手段、および該養液を、該PVA系フィルムの下に供給するための手段を含む植物栽培用システムであって;該PVA系フィルムの水中(30℃)における平衡膨潤度が125%以上250%以下の範囲かつ該PVA系フィルムの水中平衡膨潤状態(30℃)での損失正接(tan δ)が0.005以上0.2以下であることを特徴とする、植物栽培用システム。
2)該PVA系フィルムが二軸延伸されたものであることを特徴とする、上記1)に記載の植物栽培用システム。
3)該PVA系フィルムの乾燥厚さが5~100μmの範囲であることを特徴とする、上記1)または2)に記載の植物栽培用システム。
4)養液保持手段が水耕栽培用水槽であり、該PVA系フィルムの下面に接触するように配置された養液が水耕栽培用水槽に収容されてなることを特徴とする、上記1)~3)いずれかに記載の植物栽培用システム。
5)該養液保持手段が水不透過性表面を有し、その上に該PVA系フィルムが敷設されてなり、PVA系フィルムと養液保持手段との間に該養液を連続的または間歇的に供給する養液供給手段をさらに含むことを特徴とする、上記1)~3)いずれかに記載の植物栽培用システム。
6)養液供給手段が、PVA系フィルムと養液保持手段との間に設置された点滴灌水チューブであることを特徴とする、上記5)に記載の植物栽培用システム。
7)(1)植物をその上で栽培するためのPVA系フィルム、該PVA系フィルムの下面に接触するように配置された養液保持手段、および該養液を、該PVA系フィルムの下に供給するための手段を含む植物栽培用システムであって;該PVA系フィルムの水中(30℃)における平衡膨潤度が125%以上250%以下の範囲かつ該PVA系フィルムの水中平衡膨潤状態(30℃)での損失正接(tan δ)が0.005以上0.2以下であることを特徴とする植物栽培用システムを提供し、
(2)該システム内のPVA系フィルムの上に植物を配置し、そして
(3)該養液を、該PVA系フィルムを介して該植物に接触させることによって、該PVA系フィルムの上で植物を栽培することを包含する植物栽培方法。
本発明で用いられるPVA系フィルムは、PVAを原料とするもので、かかるPVAとしては、特に限定されず、公知の方法で製造することができる。すなわち、ビニルエステル系化合物を重合して得られたビニルエステル系重合体をケン化して得られるものである。
また、重合反応は、アゾビスイソブチロニトリル、過酸化アセチル、過酸化ベンゾイル、過酸化ラウロイルなどの公知のラジカル重合触媒を用いて行われ、反応温度は35℃~200℃(さらに好ましくは50~80℃)程度の範囲から選択される。
測定用セルの形状・寸法:ステンレス製平行円盤(直径4.0cm)、アルミ製ソルベントトラップ使用。
観測周波数:1Hz。
測定温度:30℃。
適用ストレス及び変位:線形領域内。具体的には、適用ストレスとして例えば10Pa~200Pa、変位として10-6ラジアン~10-5ラジアン。
1)測定対象となるPVA系フィルムを30℃の水に30分間浸漬する。
2)上記操作により平衡膨潤状態となったPVA系フィルムを取り出し、測定デバイスであるステンレス製平行円盤(直径4.0cm)に合わせて直径4cmの円形に切り取る。
3)該フィルムを測定デバイスに密着させたまま、ソルベントトラップと溶媒としての水を乗せ、測定装置に装着する。
4)測定ステージを上昇させ、測定対象となるPVA系フィルムを測定デバイスと測定ステージの間に挟み、該フィルムが測定デバイスと測定ステージに密着するようギャップを調整する。この時、PVA系フィルムと、測定デバイスおよび測定ステージの間にすべりが生じないように、またフィルムを圧縮しないように注意する。
5)測定ステージの温度を30℃に設定し、観測周波数1Hzで線形領域内となるストレスおよび変位において動的粘弾性の観測を行う。
本発明の植物栽培システムの構成要素として、本発明のPVA系フィルムは必須であるが、養液保持手段の違いによって、大きく2種に分けることができる。第1のタイプは、養液保持手段が水耕栽培用水槽であり、本発明のPVA系フィルムの下面に接触するように配置された養液が水耕栽培用水槽に収容されてなることを特徴とする、植物栽培用システムである。このようなシステムについては、特許文献1に開示されている。
以下、本発明の植物栽培システムにおける各部の構成について詳細に説明する。このような構成(ないしは機能)に関しては、必要に応じて、本発明者による文献(特許文献1~5)の「発明の詳細な説明」、「実施例」等を参照することができる。
本発明の植物栽培システムにおいては、植物をその上で栽培するための本発明のPVA系フィルムが必須である。本発明で使用する本発明のPVA系フィルムの製造法や特徴的な物性については先にも述べたが、さらに、後述する種々の物性をすべて満足するものが好ましい。
本発明のPVA系フィルムは、栽培している「植物体の根と実質的に一体化し得る」フィルムであることが重要である。「植物体の根と実質的に一体化し得る」フィルムとは、本発明の植物栽培用システムの本発明のPVA系フィルムの上で植物を35日間栽培した際に、本発明のPVA系フィルムを栽培した植物の根から剥離するための剥離強度が10g以上となるフィルムである。根とフィルムの一体化を測定するための「一体化試験」は、次のようにして実施することができる。
さらに本発明においては、本発明のPVA系フィルムが「植物体の根と実質的に一体化し得る」か否かを判断するための指標の1つとして、イオン透過性のバランスが挙げられる。
本発明においては、本発明のPVA系フィルムを介した植物の根の養分(有機物)吸収を容易とする点から、本発明のPVA系フィルムは、所定のグルコース透過性を示すことが好ましい。このグルコース透過性の優れたフィルムは、本発明のPVA系フィルムを介して水と5%グルコース水溶液とを対向して3日間(72時間)接触させた際に、水とグルコース溶液の栽培温度において測定した濃度(Brix%)の差が4以下、さらに好ましくは3以下、より好ましくは2以下、最も好ましくは1.5以下となるフィルムである。
市販のグルコース(ブドウ糖)を用いて5%グルコース溶液を作製する。上記イオン透過性試験と同様の「ざるボウルセット」を使い、ざる上に試験すべき本発明のPVA系フィルム(サイズ:200~260×200~260mm)を乗せ、該フィルム上に水150gを加える。他方、ボウル側に上記のグルコース溶液150gを加え、得られた系全体を食品用ラップ(ポリ塩化ビニリデンフィルム、商品名:サランラップ(登録商標)、旭化成社製)で包んで、水分の蒸発を防ぐ。この状態で、常温で放置して、24hrs毎に水側、グルコース溶液側の糖度(Brix%)を糖度計で測定する。
さらに本発明においては、本発明のPVA系フィルムが耐水圧として10cm以上の水不透性を有することが好ましい。このような本発明のPVA系フィルムを用いた際には、根とフィルムの一体化を促進することができる。また、根に対する好適な酸素供給および本発明のPVA系フィルムを介しての病原菌汚染を防止することが容易となる。
本発明の植物栽培システムにおいては、植物体の根を保護するために、本発明のPVA系フィルムの上に土壌などの植物栽培用支持体を配置することができる。使用する植物栽培用支持体に特に限定はなく、通常使用される土壌ないし培地が使用可能である。このような土壌ないし培地としては、例えば、土耕栽培に用いられる土壌、および水耕栽培に用いられる培地が挙げられる。
本発明の植物栽培システムは、養液を本発明のPVA系フィルムの下に保持するための養液保持手段を含んでいる。本発明の植物栽培システムにおいては、養液を収容する容器状の養液保持手段、あるいは水不透過性表面を有する基材層として機能する養液保持層の何れかが使用可能である。
本発明の栽培方法は、(1)植物をその上で栽培するための本発明のPVA系フィルム、植物の生育を促進する養液であって、該フィルムの下面に接触するように配置された養液、および該養液を、該フィルムの下に保持するための養液保持手段を含むことを特徴とする植物栽培用システムを提供し、(2)該システム内の本発明のPVA系フィルムの上に植物を配置し、そして(3)該養液を、該フィルムを介して該植物に接触させることによって、該フィルムの上で植物を栽培することを包含する植物栽培方法である。
実施例1(F-1)
PVA(平均ケン化度99.7モル%、平均重合度1700、4%水溶液粘度(25℃)40mPa・s、酢酸ナトリウム含有量0.3%)40部を水60部に溶解させたポリビニルアルコール水溶液を定量ポンプにより、ジャケット温度を60~150℃に設定した二軸押出型混錬機(スクリューL/D=40)に供給し、吐出量500kg/hrの条件で吐出した。この吐出物を直ちに、一軸押出機(スクリューL/D=30)に圧送し、温度85~140℃にて、混錬後、Tダイより5℃に冷却されたキャストロールに流延固化させ、キャストロールから冷却されたフィルムを剥離し、90℃に調整された連続した10個の回転加熱ロールを用いて30秒間乾燥し、含水率25%のPVAフィルムを作成した。
実施例1において、5℃に冷却されたキャストロール以降の速度を0.75倍に変えて、含水率25%のPVAフィルムを作成する以外は実施例1と同様にして、含水率0.8%の二軸延伸PVAフィルム(F-2、厚み40μm)を得た。 実施例1と同様にして水中(30℃)における平衡膨潤度を求めたところ、183%と算出された。
実施例1において、二軸延伸PVAフィルムを得た後、145℃で8秒間熱処理(一段目熱処理)を行い、続いて、180℃で8秒間熱処理(二段目熱処理)を行う以外は実施例1と同様にして、含水率0.8%の二軸延伸PVAフィルム(F-3、厚み30μm)を得た。 実施例1と同様にして水中(30℃)における平衡膨潤度を求めたところ、152%と算出された。
実施例3において、5℃に冷却されたキャストロール以降の速度を0.75倍に変えて、含水率25%のPVAフィルムを作成する以外は実施例3と同様にして、含水率0.8%の二軸延伸PVAフィルム(F-4、厚み40μm)を得た。実施例1と同様にして水中(30℃)における平衡膨潤度を求めたところ、152%と算出された。
PVA(平均ケン化度99.7モル%、平均重合度1700、4%水溶液粘度(25℃)40mPa・s、酢酸ナトリウム含有量0.3%)に、可塑剤としてグリセリン12部、界面活性剤としてポリオキシエチレンソルビタンモノラウレート1.2部を水に溶解して18%水分散液を得た。そして、上記水分散液を用い、ステンレス製のエンドレスベルトを備えたベルト製製膜機により、10m/minの速度で流延製膜法に従い製膜し、温度120℃の条件で乾燥させ、PVAフィルム(F-5、厚み70μm)を得た。実施例1と同様にして水中(30℃)における平衡膨潤度を求めたところ、200%と算出された。
比較例1において速度を12m/minの速度で製膜する以外は比較例1と同様にしてPVAフィルム(F-6、厚み60μm)を得た。得られたフィルム(60μm)を別途、200℃の条件で60秒乾燥させて熱処理を施したフィルムを得た。実施例1と同様にして水中(30℃)における平衡膨潤度を求めたところ、127%と算出された。
PVA(平均ケン化度99.7モル%、平均重合度1700、4%水溶液粘度(25℃)40mPa・s、酢酸ナトリウム含有量0.3%)40部を水60部に溶解させたPVA水溶液を定量ポンプにより、ジャケット温度を60~150℃に設定した二軸押出型混錬機(スクリューL/D=40)に供給し、吐出量500kg/hrの条件で吐出した。この吐出物を直ちに、一軸押出機(スクリューL/D=30)に圧送し、温度85~140℃にて、混錬後、Tダイより5℃に冷却されたキャストロールに流延固化させ、キャストロールから冷却されたフィルムを剥離し、90℃に調整された連続した10個の回転加熱ロールを用いて30秒間乾燥し、含水率25%のPVAフィルムを作成した。次いで、かかるポリビニルアルコールフィルムを縦方向に3倍延伸した後に、テンター延伸機で横方向に3.5倍延伸して、二軸延伸PVAフィルムとし、次いで165℃で8秒間熱処理(一段目熱処理)を行い、続いて、205℃で8秒間熱処理(二段目熱処理)を行い、含水率0.8%の二軸延伸PVAフィルム(F-7、厚み25μm)を得た。実施例1と同様にして水中(30℃)における平衡膨潤度を求めたところ、118%と算出された。
メビオール株式会社より販売されている「アイメックフィルム」(厚さ65μm)について、実施例1と同様にして水中(30℃)における平衡膨潤度を求めたところ、148%と算出された。
メビオール株式会社より販売されている「アイメックフィルム2」(厚さ60μm)について、実施例1と同様にして水中(30℃)における平衡膨潤度を求めたところ、153%と算出された。
実施例1~4、比較例1~5のフィルムサンプル(F-1)~(F-9)をそれぞれ、30℃の水に30分間浸漬し、直径4cmの円形に切り抜き、ストレス制御型粘弾性測定装置(ティー・エイ・インスツルメント・ジャパン株式会社製、レオメーター AR-500)を用いて、動的粘弾性挙動を観測した。
測定条件は以下の通りとした。
観測周波数:1Hz。
測定温度:30℃
適用ストレス及び変位:線形領域内。具体的には、適用ストレスとして10Pa~200Pa、変位として10-6ラジアン~10-5ラジアン。
平衡膨潤状態となったPVA系フィルムを水中から取り出し、測定デバイスであるステンレス製平行円盤(直径4.0cm)に合わせて直径4cmの円形に切り取り、該フィルムを測定デバイスに密着させたまま、ソルベントトラップと溶媒としての水を乗せ、測定装置に装着した。次いで測定ステージを上昇させ、測定対象となるPVA系フィルムを測定デバイスと測定ステージの間に挟み、該フィルムが測定デバイスと測定ステージに密着するようギャップを調整した。この時、PVA系フィルムと、測定デバイスおよび測定ステージの間にすべりが生じないように、フィルムを圧縮しないように注意した。測定ステージの温度を30℃に設定し、観測周波数1Hzで線形領域内となるストレスおよび変位において動的粘弾性の観測を行い、損失正接(tanδ)を求めた。各サンプルの結果を表1に比較してまとめた。
スチロール樹脂製トレー(縦19.5cmx横12.5cmx深さ5.5cm)に養液(大塚化学株式会社製、大塚ハウスA処方EC=2)600mL を入れ、養液に片面が接触するように実施例または比較例で得られたA4判サイズのPVAフィルムを配置した。PVAフィルムの上に、土壌として、ヤシガラチップを1.5cmの厚さで置き、芝の種(雪印種苗株式会社製 西洋芝「ペレニアルライグラス アクセント」)を50g/m2で蒔き、霧吹きで充分給水し、乾燥を防ぐため、全体を半透明ポリエチレンフィルム(好川産業株式会社製、YKシート、厚さ10μm)で覆った。これを25℃の室内に置き、6時~20時までの間、蛍光灯を用いて播種からフィルムに根が張るまでは2,000ルクス、フィルムに根が張ってからは半透明ポリエチレンフィルムを数日かけて少しずつはずし、6,000ルクスの照度で栽培した。試験結果を表1に比較してまとめた。根がPVAフィルムを貫通した日が栽培を開始してから150日以上の場合を「○」(良好)と評価し、150日未満の場合は「×」(不良)と評価し、貫通までの日数をカッコ内に記した。尚、芝の生長が悪く、芝の根がPVAフィルムに張らなかった場合を「-」(不能)と評価した。
Claims (7)
- 植物をその上で栽培するためのポリビニルアルコール(PVA)系フィルム、該PVA系フィルムの下面に接触するように配置された養液保持手段、および該養液を、該PVA系フィルムの下に供給するための手段を含む植物栽培用システムであって;該PVA系フィルムの水中(30℃)における平衡膨潤度が125%以上250%以下の範囲かつ該PVA系フィルムの水中平衡膨潤状態(30℃)での損失正接(tan δ)が0.005以上0.2以下であることを特徴とする、植物栽培用システム。
- 該PVA系フィルムが二軸延伸されたものであることを特徴とする、請求項1に記載の植物栽培用システム。
- 該PVA系フィルムの乾燥厚さが5~100μmの範囲であることを特徴とする、請求項1または2に記載の植物栽培用システム。
- 養液保持手段が水耕栽培用水槽であり、該PVA系フィルムの下面に接触するように配置された養液が水耕栽培用水槽に収容されてなることを特徴とする、請求項1~3いずれかに記載の植物栽培用システム。
- 該養液保持手段が水不透過性表面を有し、その上に該PVA系フィルムが敷設されてなり、PVA系フィルムと養液保持手段との間に該養液を連続的または間歇的に供給する養液供給手段をさらに含むことを特徴とする、請求項1~3いずれかに記載の植物栽培用システム。
- 養液供給手段が、PVA系フィルムと養液保持手段との間に設置された点滴灌水チューブであることを特徴とする、請求項5に記載の植物栽培用システム。
- (1)植物をその上で栽培するためのPVA系フィルム、該PVA系フィルムの下面に接触するように配置された養液保持手段、および該養液を、該PVA系フィルムの下に供給するための手段を含む植物栽培用システムであって;該PVA系フィルムの水中(30℃)における平衡膨潤度が125%以上250%以下の範囲かつ該PVA系フィルムの水中平衡膨潤状態(30℃)での損失正接(tan δ)が0.005以上0.2以下であることを特徴とする植物栽培用システムを提供し、
(2)該システム内のPVA系フィルムの上に植物を配置し、そして
(3)該養液を、該PVA系フィルムを介して該植物に接触させることによって、該PVA系フィルムの上で植物を栽培することを包含する植物栽培方法。
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