WO2009020203A1 - α－不飽和アミン化合物の分離精製方法 - Google Patents

α－不飽和アミン化合物の分離精製方法 Download PDF

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Publication number
WO2009020203A1
WO2009020203A1 PCT/JP2008/064293 JP2008064293W WO2009020203A1 WO 2009020203 A1 WO2009020203 A1 WO 2009020203A1 JP 2008064293 W JP2008064293 W JP 2008064293W WO 2009020203 A1 WO2009020203 A1 WO 2009020203A1
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WO
WIPO (PCT)
Prior art keywords
alkyl group
formula
amine compound
unsaturated amine
group
Prior art date
Application number
PCT/JP2008/064293
Other languages
English (en)
French (fr)
Inventor
Hiroshi Souda
Original Assignee
Sumitomo Chemical Company, Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Chemical Company, Limited filed Critical Sumitomo Chemical Company, Limited
Priority to CN200880102298XA priority Critical patent/CN101778823B/zh
Priority to EP08826943A priority patent/EP2186802A4/en
Priority to KR1020107004837A priority patent/KR101503096B1/ko
Priority to US12/672,209 priority patent/US8263779B2/en
Priority to BRPI0815144A priority patent/BRPI0815144B1/pt
Publication of WO2009020203A1 publication Critical patent/WO2009020203A1/ja
Priority to IL203368A priority patent/IL203368A/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/61—Halogen atoms or nitro radicals
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P33/00—Antiparasitic agents
    • A61P33/10—Anthelmintics

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  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Tropical Medicine & Parasitology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Pyridine Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

　式（１） （式中、Ｒ１は、水素原子、Ｃ１－４アルキル基、ハロＣ１－４アルキル基、Ｃ１－４アルコキシ－Ｃ１－４アルキル基、Ｃ７－９アラルキル基、または置換していてもよいフェニル基を表し、Ｒ２は、水素原子、Ｃ１－４アルキル基またはＣ７－９アラルキル基を表し、Ｒ３は、水素原子、Ｃ１－５アルキル基、ハロＣ１－４アルキル基、ヒドロキシＣ１－４アルキル基、Ｃ１－４アルコキシ－Ｃ１－４アルキル基、Ｃ２－４アルケニル基、またはＣ７－９アラルキル基を表す。） で示されるα－不飽和アミン化合物の粗製物から式（１）の化合物を水で抽出する工程、および当該工程で得られた式（１）の化合物を含む水溶液から式（１）のα－不飽和アミン化合物をピリジン系溶媒で抽出して式（１）の化合物のピリジン系溶媒溶液を得る工程からなる式（１）のα－不飽和アミン化合物の精製方法。
PCT/JP2008/064293 2007-08-08 2008-08-08 α－不飽和アミン化合物の分離精製方法 WO2009020203A1 (ja)

Priority Applications (6)

Application Number Priority Date Filing Date Title
CN200880102298XA CN101778823B (zh) 2007-08-08 2008-08-08 α-不饱和胺化合物的分离纯化方法
EP08826943A EP2186802A4 (en) 2007-08-08 2008-08-08 METHOD FOR SEPARATING AND CLEANING ALPHA-UNSATURATED AMINE COMPOUNDS
KR1020107004837A KR101503096B1 (ko) 2007-08-08 2008-08-08 α-불포화 아민 화합물의 분리 정제 방법
US12/672,209 US8263779B2 (en) 2007-08-08 2008-08-08 Method for separating and purifying α-unsaturated amine compound
BRPI0815144A BRPI0815144B1 (pt) 2007-08-08 2008-08-08 método para separar e purificar um composto de amina alfa-insaturado
IL203368A IL203368A (en) 2007-08-08 2010-01-18 A method for separating and purifying an unsaturated alpha amine compound

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007-206350 2007-08-08
JP2007206350 2007-08-08

Publications (1)

Publication Number Publication Date
WO2009020203A1 true WO2009020203A1 (ja) 2009-02-12

Family

ID=40341430

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/064293 WO2009020203A1 (ja) 2007-08-08 2008-08-08 α－不飽和アミン化合物の分離精製方法

Country Status (8)

Country Link
US (1) US8263779B2 (ja)
EP (1) EP2186802A4 (ja)
JP (1) JP5266944B2 (ja)
KR (1) KR101503096B1 (ja)
CN (1) CN101778823B (ja)
BR (1) BRPI0815144B1 (ja)
IL (1) IL203368A (ja)
WO (1) WO2009020203A1 (ja)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010143598A1 (ja) * 2009-06-08 2010-12-16 住友化学株式会社 ピラゾリノン誘導体の精製方法

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102816112B (zh) * 2012-09-13 2014-01-22 浙江禾本科技有限公司 一种杀虫剂烯啶虫胺的制备方法
CN105330593A (zh) * 2015-11-23 2016-02-17 上海晋景化学有限公司 一种制备烯啶虫胺的改进方法
CN106885855A (zh) * 2017-03-09 2017-06-23 江苏泰洁检测技术有限公司 一种1,1,1‑三氯硝基乙烷的气相色谱测定法
CN107382736B (zh) * 2017-08-09 2019-09-03 江苏克胜集团股份有限公司 1,1-二氯-2-硝基乙烯及烯啶虫胺的合成方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02171A (ja) * 1987-08-01 1990-01-05 Takeda Chem Ind Ltd α‐不飽和アミン類及びそれを含む組成物
GB2228003A (en) * 1989-02-13 1990-08-15 Shell Int Research Pesticidal nitroethene compounds
JPH02275841A (ja) * 1989-01-31 1990-11-09 Takeda Chem Ind Ltd ハロゲン化ニトロエタンの製造方法およびこれを用いる殺虫性α―不飽和アミン類の製造方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3173905D1 (en) 1980-11-20 1986-04-03 Crosfield Electronics Ltd Coating of polymerical substrates
DE3856183T2 (de) * 1987-08-01 1998-11-05 Takeda Chemical Industries Ltd Zwischenprodukte, ihre Herstellung und Verwendung zur Herstellung alpha-ungesättigter Amine
US5364989A (en) 1989-01-31 1994-11-15 Takeda Chemical Industries, Ltd. 1,1,1-trichloro-2-nitroethane production
JP3038781B2 (ja) 1989-04-21 2000-05-08 日本電気株式会社 メモリアクセス制御回路

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02171A (ja) * 1987-08-01 1990-01-05 Takeda Chem Ind Ltd α‐不飽和アミン類及びそれを含む組成物
JPH02275841A (ja) * 1989-01-31 1990-11-09 Takeda Chem Ind Ltd ハロゲン化ニトロエタンの製造方法およびこれを用いる殺虫性α―不飽和アミン類の製造方法
JP3048370B2 (ja) * 1989-01-31 2000-06-05 武田薬品工業株式会社 ハロゲン化ニトロエタンの製造方法およびこれを用いる殺虫性α―不飽和アミン類の製造方法
GB2228003A (en) * 1989-02-13 1990-08-15 Shell Int Research Pesticidal nitroethene compounds

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
MINAMIDA I. ET AL.: "Synthesis and Insecticidal Activity of Acyclic Nitroethene Compounds Containing a 3-Pyridylmethylamino Group", JOURNAL OF PESTICIDE SCIENCE, vol. 18, no. 1, 20 February 1993 (1993-02-20), pages 31 - 40, XP008131852 *
NINAMIDA I. ET AL.: "Synthesis and Insecticidal Activity of Acyclic Nitroethene Compounds Containing a Heteroarylmethylamino Group", JOURNAL OF PESTICIDE SCIENCE, vol. 18, no. 1, 20 February 1993 (1993-02-20), pages 41 - 48, XP008130673 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010143598A1 (ja) * 2009-06-08 2010-12-16 住友化学株式会社 ピラゾリノン誘導体の精製方法
US9296700B2 (en) 2009-06-08 2016-03-29 Sumitomo Chemical Company, Limited Method for purifying a pyrazolinone derivative

Also Published As

Publication number Publication date
KR20100052513A (ko) 2010-05-19
BRPI0815144B1 (pt) 2016-06-28
JP5266944B2 (ja) 2013-08-21
EP2186802A4 (en) 2011-06-01
EP2186802A1 (en) 2010-05-19
US20110184184A1 (en) 2011-07-28
CN101778823A (zh) 2010-07-14
CN101778823B (zh) 2013-02-13
KR101503096B1 (ko) 2015-03-16
IL203368A (en) 2015-01-29
JP2009057378A (ja) 2009-03-19
US8263779B2 (en) 2012-09-11
BRPI0815144A2 (pt) 2015-02-03

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