WO2008149985A1 - 金属珪素の凝固方法 - Google Patents

金属珪素の凝固方法 Download PDF

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Publication number
WO2008149985A1
WO2008149985A1 PCT/JP2008/060472 JP2008060472W WO2008149985A1 WO 2008149985 A1 WO2008149985 A1 WO 2008149985A1 JP 2008060472 W JP2008060472 W JP 2008060472W WO 2008149985 A1 WO2008149985 A1 WO 2008149985A1
Authority
WO
WIPO (PCT)
Prior art keywords
metallic silicon
solidifying
solidifying metallic
monodirectionally
ppm
Prior art date
Application number
PCT/JP2008/060472
Other languages
English (en)
French (fr)
Inventor
Motoyuki Yamada
Kazuhisa Hatayama
Original Assignee
Shin-Etsu Chemical Co., Ltd.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shin-Etsu Chemical Co., Ltd. filed Critical Shin-Etsu Chemical Co., Ltd.
Priority to AU2008260891A priority Critical patent/AU2008260891A1/en
Priority to EP08765285A priority patent/EP2172424A4/en
Priority to CN200880019233A priority patent/CN101778795A/zh
Priority to CA2689603A priority patent/CA2689603A1/en
Priority to BRPI0814930-5A2A priority patent/BRPI0814930A2/pt
Priority to US12/663,462 priority patent/US20100178195A1/en
Priority to JP2009517913A priority patent/JPWO2008149985A1/ja
Publication of WO2008149985A1 publication Critical patent/WO2008149985A1/ja

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/02—Silicon
    • C01B33/037—Purification
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B11/00—Single-crystal growth by normal freezing or freezing under temperature gradient, e.g. Bridgman-Stockbarger method
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/02—Elements
    • C30B29/06—Silicon

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)

Abstract

　鉄の濃度が８００ｐｐｍ以下である金属珪素を一方向凝固することを特徴とする金属珪素の凝固方法。 　本発明によれば、安価、かつ短縮された工程で、金属珪素中の金属不純物成分を効果的に除去できる。
PCT/JP2008/060472 2007-06-08 2008-06-06 金属珪素の凝固方法 WO2008149985A1 (ja)

Priority Applications (7)

Application Number Priority Date Filing Date Title
AU2008260891A AU2008260891A1 (en) 2007-06-08 2008-06-06 Method of solidifying metallic silicon
EP08765285A EP2172424A4 (en) 2007-06-08 2008-06-06 METHOD FOR FIXING METALLIC SILICON
CN200880019233A CN101778795A (zh) 2007-06-08 2008-06-06 金属硅的凝固方法
CA2689603A CA2689603A1 (en) 2007-06-08 2008-06-06 Method of solidifying metallic silicon
BRPI0814930-5A2A BRPI0814930A2 (pt) 2007-06-08 2008-06-06 Método de solidificação de silício metálico
US12/663,462 US20100178195A1 (en) 2007-06-08 2008-06-06 Method of solidifying metallic silicon
JP2009517913A JPWO2008149985A1 (ja) 2007-06-08 2008-06-06 金属珪素の凝固方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007152294 2007-06-08
JP2007-152294 2007-06-08

Publications (1)

Publication Number Publication Date
WO2008149985A1 true WO2008149985A1 (ja) 2008-12-11

Family

ID=40093789

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/060472 WO2008149985A1 (ja) 2007-06-08 2008-06-06 金属珪素の凝固方法

Country Status (9)

Country Link
US (1) US20100178195A1 (ja)
EP (1) EP2172424A4 (ja)
JP (1) JPWO2008149985A1 (ja)
KR (1) KR20100022516A (ja)
CN (1) CN101778795A (ja)
AU (1) AU2008260891A1 (ja)
BR (1) BRPI0814930A2 (ja)
CA (1) CA2689603A1 (ja)
WO (1) WO2008149985A1 (ja)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010119502A1 (ja) * 2009-04-14 2010-10-21 信越化学工業株式会社 金属珪素の精製方法
US20110200514A1 (en) * 2010-02-12 2011-08-18 Masahiro Hoshino Method for purifying metallurgical silicon for solar cells
US8236266B2 (en) 2010-07-21 2012-08-07 Masahiro Hoshino Method and apparatus for purifying metallurgical silicon for solar cells
US8257492B2 (en) 2009-11-16 2012-09-04 Masahiro Hoshino Methods for purifying metallurgical silicon
JP2013512188A (ja) * 2009-12-01 2013-04-11 ダウ コーニング コーポレーション 回転成型プロセス

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102011004753A1 (de) * 2011-02-25 2012-08-30 Evonik Degussa Gmbh Verfahren zum Aufreinigen von Silicium
CN102659110B (zh) * 2012-04-19 2014-03-19 厦门大学 一种采用硅铁合金定向凝固提纯多晶硅的方法

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04231315A (ja) * 1990-08-13 1992-08-20 Dow Corning Corp 直流炉におけるケイ素の溶解法
JPH10120493A (ja) 1996-10-14 1998-05-12 Kawasaki Steel Corp 太陽電池用シリコンの鋳造方法
JPH10182137A (ja) 1996-12-26 1998-07-07 Kawasaki Steel Corp 太陽電池用シリコンの凝固精製方法及び装置
JPH10182134A (ja) 1996-10-31 1998-07-07 Kawasaki Steel Corp シリコンの精製方法
JPH10236815A (ja) 1997-02-28 1998-09-08 Kawasaki Steel Corp 太陽電池用シリコンの製造方法
JP2004535354A (ja) * 2001-07-23 2004-11-25 アンヴァンシル 中純度金属シリコンとその製錬法

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US4193975A (en) * 1977-11-21 1980-03-18 Union Carbide Corporation Process for the production of improved refined metallurgical silicon
US4193974A (en) * 1977-11-21 1980-03-18 Union Carbide Corporation Process for producing refined metallurgical silicon ribbon
US4124410A (en) * 1977-11-21 1978-11-07 Union Carbide Corporation Silicon solar cells with low-cost substrates
US4195067A (en) * 1977-11-21 1980-03-25 Union Carbide Corporation Process for the production of refined metallurgical silicon
US4247528A (en) * 1979-04-11 1981-01-27 Dow Corning Corporation Method for producing solar-cell-grade silicon
US4457902A (en) * 1980-10-24 1984-07-03 Watson Keith R High efficiency hydrocarbon reduction of silica
US4612179A (en) * 1985-03-13 1986-09-16 Sri International Process for purification of solid silicon
JP3497355B2 (ja) * 1997-10-06 2004-02-16 信越フィルム株式会社 シリコンの精製方法
US7732012B2 (en) * 2004-06-22 2010-06-08 Shin-Etsu Film Co., Ltd Method for manufacturing polycrystalline silicon, and polycrystalline silicon for solar cells manufactured by the method
JP4115432B2 (ja) * 2004-07-14 2008-07-09 シャープ株式会社 金属の精製方法
JP4689373B2 (ja) * 2005-07-04 2011-05-25 シャープ株式会社 シリコンの再利用方法
DE112006003557T5 (de) * 2005-12-27 2008-11-20 Sumitomo Chemical Co., Ltd. Verfahren zur Herstellung von polykristallinem Silicium
JP5398260B2 (ja) * 2006-07-06 2014-01-29 ロータスアロイ株式会社 多孔質体の製造方法
CN101506097B (zh) * 2006-08-31 2011-06-29 三菱麻铁里亚尔株式会社 金属硅及其制备方法
UA97488C2 (ru) * 2006-09-14 2012-02-27 Силисиум Беканкур Инк. Способ очистки кремнийсодержащего материала низкой чистоты, применение барабанной печи в нем, расплав кремнийсодержащего материала, отходящие газы и твердый поликристаллический кремний, полученные данным способом
FR2908125B1 (fr) * 2006-11-02 2009-11-20 Commissariat Energie Atomique Procede de purification de silicium metallurgique par solidification dirigee
JP2008115040A (ja) * 2006-11-02 2008-05-22 Sharp Corp シリコン再生装置、シリコン再生方法
WO2009033255A1 (en) * 2007-09-13 2009-03-19 Silicium Bécancour Inc. Process for the production of medium and high purity silicon from metallurgical grade silicon

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04231315A (ja) * 1990-08-13 1992-08-20 Dow Corning Corp 直流炉におけるケイ素の溶解法
JPH10120493A (ja) 1996-10-14 1998-05-12 Kawasaki Steel Corp 太陽電池用シリコンの鋳造方法
JPH10182134A (ja) 1996-10-31 1998-07-07 Kawasaki Steel Corp シリコンの精製方法
JPH10182137A (ja) 1996-12-26 1998-07-07 Kawasaki Steel Corp 太陽電池用シリコンの凝固精製方法及び装置
JPH10236815A (ja) 1997-02-28 1998-09-08 Kawasaki Steel Corp 太陽電池用シリコンの製造方法
JP2004535354A (ja) * 2001-07-23 2004-11-25 アンヴァンシル 中純度金属シリコンとその製錬法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of EP2172424A4 *

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010119502A1 (ja) * 2009-04-14 2010-10-21 信越化学工業株式会社 金属珪素の精製方法
US8257492B2 (en) 2009-11-16 2012-09-04 Masahiro Hoshino Methods for purifying metallurgical silicon
US8673073B2 (en) 2009-11-16 2014-03-18 Masahiro Hoshino Methods for purifying metallurgical silicon
JP2013512188A (ja) * 2009-12-01 2013-04-11 ダウ コーニング コーポレーション 回転成型プロセス
US20110200514A1 (en) * 2010-02-12 2011-08-18 Masahiro Hoshino Method for purifying metallurgical silicon for solar cells
US8236265B2 (en) * 2010-02-12 2012-08-07 Masahiro Hoshino Method for purifying metallurgical silicon for solar cells
US8461487B2 (en) 2010-02-12 2013-06-11 Masahiro Hoshino Apparatus for purifying metallurgical silicon for solar cells
US8524188B2 (en) 2010-02-12 2013-09-03 Masahiro Hoshino Method for purifying metallurgical silicon for solar cells
US8236266B2 (en) 2010-07-21 2012-08-07 Masahiro Hoshino Method and apparatus for purifying metallurgical silicon for solar cells
US8501140B2 (en) 2010-07-21 2013-08-06 Masahiro Hoshino Method and apparatus for purifying metallurgical silicon for solar cells

Also Published As

Publication number Publication date
EP2172424A1 (en) 2010-04-07
BRPI0814930A2 (pt) 2015-02-03
CA2689603A1 (en) 2008-12-11
US20100178195A1 (en) 2010-07-15
EP2172424A4 (en) 2012-03-07
CN101778795A (zh) 2010-07-14
JPWO2008149985A1 (ja) 2010-08-26
KR20100022516A (ko) 2010-03-02
AU2008260891A1 (en) 2008-12-11

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