WO2008139924A1 - 新規エポキシ化合物、アルカリ現像性樹脂組成物およびアルカリ現像性感光性樹脂組成物 - Google Patents

新規エポキシ化合物、アルカリ現像性樹脂組成物およびアルカリ現像性感光性樹脂組成物 Download PDF

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WO2008139924A1
WO2008139924A1 PCT/JP2008/058210 JP2008058210W WO2008139924A1 WO 2008139924 A1 WO2008139924 A1 WO 2008139924A1 JP 2008058210 W JP2008058210 W JP 2008058210W WO 2008139924 A1 WO2008139924 A1 WO 2008139924A1
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Prior art keywords
alkali
resin composition
developable
halogen atom
epoxy compound
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PCT/JP2008/058210
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English (en)
French (fr)
Inventor
Taiki Mihara
Kiyoshi Murata
Koichi Kimijima
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Adeka Corporation
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Publication date
Application filed by Adeka Corporation filed Critical Adeka Corporation
Priority to KR1020097017622A priority Critical patent/KR101450705B1/ko
Priority to AT08752220T priority patent/ATE526321T1/de
Priority to CN200880006594.XA priority patent/CN101622236B/zh
Priority to EP08752220A priority patent/EP2145880B1/en
Priority to US12/528,176 priority patent/US8252512B2/en
Priority to JP2009514096A priority patent/JP5214598B2/ja
Publication of WO2008139924A1 publication Critical patent/WO2008139924A1/ja

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F290/00—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
    • C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
    • C07D303/24—Ethers with hydroxy compounds containing no oxirane rings with polyhydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
    • C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
    • C07D303/24—Ethers with hydroxy compounds containing no oxirane rings with polyhydroxy compounds
    • C07D303/26—Ethers with hydroxy compounds containing no oxirane rings with polyhydroxy compounds having one or more free hydroxyl radicals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/46—Polymerisation initiated by wave energy or particle radiation
    • C08F2/48—Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F283/00—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G
    • C08F283/10—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G on to polymers containing more than one epoxy radical per molecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F290/00—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups
    • C08F290/02—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups on to polymers modified by introduction of unsaturated end groups
    • C08F290/06—Polymers provided for in subclass C08G
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F290/00—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups
    • C08F290/02—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups on to polymers modified by introduction of unsaturated end groups
    • C08F290/06—Polymers provided for in subclass C08G
    • C08F290/064—Polymers containing more than one epoxy group per molecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F290/00—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups
    • C08F290/08—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups on to polymers modified by introduction of unsaturated side groups
    • C08F290/14—Polymers provided for in subclass C08G
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F290/00—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups
    • C08F290/08—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups on to polymers modified by introduction of unsaturated side groups
    • C08F290/14—Polymers provided for in subclass C08G
    • C08F290/144—Polymers containing more than one epoxy group per molecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/14—Polycondensates modified by chemical after-treatment
    • C08G59/1433—Polycondensates modified by chemical after-treatment with organic low-molecular-weight compounds
    • C08G59/1438—Polycondensates modified by chemical after-treatment with organic low-molecular-weight compounds containing oxygen
    • C08G59/1455—Monocarboxylic acids, anhydrides, halides, or low-molecular-weight esters thereof
    • C—CHEMISTRY; METALLURGY
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    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/14—Polycondensates modified by chemical after-treatment
    • C08G59/1433—Polycondensates modified by chemical after-treatment with organic low-molecular-weight compounds
    • C08G59/1438—Polycondensates modified by chemical after-treatment with organic low-molecular-weight compounds containing oxygen
    • C08G59/1455—Monocarboxylic acids, anhydrides, halides, or low-molecular-weight esters thereof
    • C08G59/1461—Unsaturated monoacids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/182—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing using pre-adducts of epoxy compounds with curing agents
    • C08G59/186—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing using pre-adducts of epoxy compounds with curing agents with acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
    • C08G59/22—Di-epoxy compounds
    • C08G59/24—Di-epoxy compounds carbocyclic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
    • C08G59/22—Di-epoxy compounds
    • C08G59/24—Di-epoxy compounds carbocyclic
    • C08G59/245—Di-epoxy compounds carbocyclic aromatic
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    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
    • G—PHYSICS
    • G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
    • G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
    • G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
    • G03F7/004—Photosensitive materials
    • G03F7/027—Non-macromolecular photopolymerisable compounds having carbon-to-carbon double bonds, e.g. ethylenic compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Physics & Mathematics (AREA)
  • Emergency Medicine (AREA)
  • General Chemical & Material Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Epoxy Resins (AREA)
  • Epoxy Compounds (AREA)
  • Macromonomer-Based Addition Polymer (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Materials For Photolithography (AREA)

Abstract

　新規エポキシ化合物は、下記一般式（Ｉ）で表される化合物であり、ベンゾ又はナフトシクロアルカン骨格を有することを特徴とする。 （式中、Ｘ、Ｙ及びＺは、それぞれ独立して、ハロゲン原子で置換されていてもよい炭素原子数１～１０のアルキル基、ハロゲン原子で置換されていてもよい炭素原子数６～２０のアリール基、ハロゲン原子で置換されていてもよい炭素原子数７～２０のアリールアルキル基、ハロゲン原子で置換されていてもよい炭素原子数２～２０の複素環基又はハロゲン原子を表し、ｋは０～４の数を表し、ｐは０～８の数を表し、ｒは０～４の数を表し、ｎは０～１０を表し、ｘは０～４の数を表し、ｙは０～４の数を表し、ｘとｙの数の合計は２～４であり、ｎが０でない時に存在する光学異性体は、どの異性体でもよい。）
PCT/JP2008/058210 2007-05-09 2008-04-28 新規エポキシ化合物、アルカリ現像性樹脂組成物およびアルカリ現像性感光性樹脂組成物 WO2008139924A1 (ja)

Priority Applications (6)

Application Number Priority Date Filing Date Title
KR1020097017622A KR101450705B1 (ko) 2007-05-09 2008-04-28 신규 에폭시화합물, 알칼리 현상성 수지 조성물 및 알칼리 현상성 감광성 수지 조성물
AT08752220T ATE526321T1 (de) 2007-05-09 2008-04-28 Neue epoxidverbindung, alkalisch entwickelbare harzzusammensetzung und alkalisch entwickelbare lichtempfindliche harzzusammensetzung
CN200880006594.XA CN101622236B (zh) 2007-05-09 2008-04-28 环氧化合物、碱显影性树脂组合物以及碱显影性感光性树脂组合物
EP08752220A EP2145880B1 (en) 2007-05-09 2008-04-28 Novel epoxy compound, alkali-developable resin composition, and alkali-developable photosensitive resin composition
US12/528,176 US8252512B2 (en) 2007-05-09 2008-04-28 Epoxy compound, alkali-developable resin composition, and alkali-developable photosensitive resin composition
JP2009514096A JP5214598B2 (ja) 2007-05-09 2008-04-28 新規エポキシ化合物、アルカリ現像性樹脂組成物およびアルカリ現像性感光性樹脂組成物

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JP2007-124550 2007-05-09
JP2007124550 2007-05-09

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WO2008139924A1 true WO2008139924A1 (ja) 2008-11-20

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US (1) US8252512B2 (ja)
EP (1) EP2145880B1 (ja)
JP (1) JP5214598B2 (ja)
KR (1) KR101450705B1 (ja)
CN (1) CN101622236B (ja)
AT (1) ATE526321T1 (ja)
TW (2) TWI423960B (ja)
WO (1) WO2008139924A1 (ja)

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JP2009185270A (ja) * 2007-05-30 2009-08-20 Nagase Chemtex Corp 縮環構造含有樹脂
JP2010126693A (ja) * 2008-11-28 2010-06-10 Nagase Chemtex Corp 非対称型の多官能水酸基含有縮環構造化合物及び縮環構造含有樹脂
WO2010101033A1 (ja) * 2009-03-04 2010-09-10 株式会社Adeka 重合性化合物、これを含有する重合性組成物及びその重合体
WO2011001788A1 (ja) * 2009-07-02 2011-01-06 株式会社Adeka 硬化性樹脂組成物及びその硬化物
JP2012241083A (ja) * 2011-05-18 2012-12-10 Adeka Corp エポキシ化合物、及びこれを含有する重合性組成物
JP2013144723A (ja) * 2012-01-13 2013-07-25 Adeka Corp グリシジルエーテルの製造方法
CN103382250A (zh) * 2009-09-18 2013-11-06 株式会社艾迪科 新型环硫化合物、含有该环硫化合物的固化性树脂组合物以及其固化物
KR20140109827A (ko) 2013-03-06 2014-09-16 가부시키가이샤 아데카 광경화성 조성물
JP2014196469A (ja) * 2013-03-06 2014-10-16 株式会社Adeka 光硬化性組成物
JP2016061939A (ja) * 2014-09-18 2016-04-25 株式会社Adeka 光硬化性組成物
JP2016090797A (ja) * 2014-11-05 2016-05-23 株式会社Adeka 硬化性組成物
JP2016130288A (ja) * 2015-01-14 2016-07-21 株式会社Adeka 着色剤分散液、着色組成物及びカラーフィルタ
JP2016193984A (ja) * 2015-03-31 2016-11-17 株式会社Adeka 樹脂及び該樹脂を用いた組成物

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US9102597B2 (en) 2012-09-05 2015-08-11 Sabic Global Technologies B.V. Indane bisphenols, polymers derived therefrom, and methods of use thereof
CN106536589A (zh) * 2014-07-22 2017-03-22 沙特基础工业全球技术有限公司 高热单体及其使用的方法
KR102322940B1 (ko) 2016-10-28 2021-11-05 미쯔비시 케미컬 주식회사 탄소섬유용 사이징제, 탄소섬유용 사이징제의 수분산액, 및 사이징제 부착 탄소섬유속
CN109233661A (zh) * 2017-05-05 2019-01-18 上海海优威新材料股份有限公司 基于辐照交联基材的新型多层粘结性薄膜及其制备方法

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ATE526321T1 (de) 2011-10-15
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