WO2007006830A3 - Método de análisis de residuos de plaguicidas en muestras vegetales - Google Patents
Método de análisis de residuos de plaguicidas en muestras vegetales Download PDFInfo
- Publication number
- WO2007006830A3 WO2007006830A3 PCT/ES2006/000394 ES2006000394W WO2007006830A3 WO 2007006830 A3 WO2007006830 A3 WO 2007006830A3 ES 2006000394 W ES2006000394 W ES 2006000394W WO 2007006830 A3 WO2007006830 A3 WO 2007006830A3
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- analysis
- gas chromatography
- extract
- pesticide residues
- volumes
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 4
- 238000004458 analytical method Methods 0.000 title abstract 2
- 239000000447 pesticide residue Substances 0.000 title abstract 2
- 238000004817 gas chromatography Methods 0.000 abstract 3
- 238000004587 chromatography analysis Methods 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 abstract 1
- 230000008878 coupling Effects 0.000 abstract 1
- 238000010168 coupling process Methods 0.000 abstract 1
- 238000005859 coupling reaction Methods 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 238000002347 injection Methods 0.000 abstract 1
- 239000007924 injection Substances 0.000 abstract 1
- 238000004811 liquid chromatography Methods 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 239000000575 pesticide Substances 0.000 abstract 1
- 238000002336 sorption--desorption measurement Methods 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/12—Preparation by evaporation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N2030/062—Preparation extracting sample from raw material
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/12—Preparation by evaporation
- G01N2030/126—Preparation by evaporation evaporating sample
- G01N2030/127—PTV evaporation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/72—Mass spectrometers
- G01N30/7206—Mass spectrometers interfaced to gas chromatograph
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2008520896A JP2009500638A (ja) | 2005-07-11 | 2006-07-11 | 植物試料中にある殺虫剤残留物の分析方法 |
US11/995,364 US20080206739A1 (en) | 2005-07-11 | 2006-07-11 | Analysis Method for Pesticide Residues in Plant Samples |
EP06807847A EP1935467A4 (en) | 2005-07-11 | 2006-07-11 | PROCESS FOR ANALYZING PESTICIDE RESIDUES IN PLANT SAMPLES |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ES200501686A ES2265284B1 (es) | 2005-07-11 | 2005-07-11 | Metodo de analisis de residuos de plaguicidas en muestras vegetales. |
ESP200501686 | 2005-07-11 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2007006830A2 WO2007006830A2 (es) | 2007-01-18 |
WO2007006830A3 true WO2007006830A3 (es) | 2007-04-12 |
Family
ID=37637530
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/ES2006/000394 WO2007006830A2 (es) | 2005-07-11 | 2006-07-11 | Método de análisis de residuos de plaguicidas en muestras vegetales |
Country Status (6)
Country | Link |
---|---|
US (1) | US20080206739A1 (es) |
EP (1) | EP1935467A4 (es) |
JP (1) | JP2009500638A (es) |
CN (1) | CN101262917A (es) |
ES (1) | ES2265284B1 (es) |
WO (1) | WO2007006830A2 (es) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103558298A (zh) * | 2013-08-07 | 2014-02-05 | 公安部物证鉴定中心 | 利用凝胶渗透色谱处理生物检材的有机磷农药检验方法 |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2327198B1 (es) * | 2008-04-23 | 2010-08-10 | Universidad De Castilla-La Mancha | Procedimiento para analizar plaguicidas en frutos secos. |
CN101498692B (zh) * | 2008-08-18 | 2012-05-02 | 通标标准技术服务(天津)有限公司 | 皮革中农药残留量的测定方法 |
ES2364565B1 (es) * | 2010-02-26 | 2012-09-19 | Universidad De Castilla-La Mancha | Procedimiento para analizar esteroles en aceites comestibles |
ES2390034B1 (es) * | 2010-07-29 | 2014-04-16 | Universidad De Castilla-La Mancha | Procedimiento para analizar ceras en aceites vegetales. |
CN102692468A (zh) * | 2012-05-22 | 2012-09-26 | 天津出入境检验检疫局动植物与食品检测中心 | 一种检测紫苏叶中常用杀菌剂前处理试剂盒及其方法 |
CN102735778A (zh) * | 2012-07-09 | 2012-10-17 | 吴桂玲 | 一种检测有机氯农药残留的前处理方法 |
CN103529153B (zh) * | 2013-07-26 | 2015-07-08 | 宁波检验检疫科学技术研究院 | 一种大豆中多种农药残留的通用快速检测方法 |
CN103472174A (zh) * | 2013-09-06 | 2013-12-25 | 邬金飞 | 气相色谱法检测农田地表水中毒死蜱农药残留量 |
CN104502497B (zh) * | 2014-12-04 | 2016-05-25 | 苏州国环环境检测有限公司 | 一种成熟桔子中杀扑磷残留的检测方法 |
JP2017075902A (ja) * | 2015-10-16 | 2017-04-20 | 公益財団法人科学技術交流財団 | 機器分析による残留農薬分析のための前処理方法 |
CN105334271A (zh) * | 2015-11-13 | 2016-02-17 | 无锡艾科瑞思产品设计与研究有限公司 | 一种中药提取物中农药残留物的检测方法 |
CN106391686A (zh) * | 2016-09-30 | 2017-02-15 | 陕西科技大学 | 一种氯吡硫磷污染黄土的热脱附修复方法 |
CN110376298B (zh) * | 2019-06-13 | 2022-04-19 | 杭州师范大学 | 一种铁皮石斛中残留农药的检测方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2222795A1 (es) * | 2003-03-28 | 2005-02-01 | Universidad De Castilla-La Mancha | Metodo de analisis de residuos de plaguicidas en aceites vegetales. |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2152153B1 (es) * | 1998-05-22 | 2001-08-16 | Consejo Superior Investigacion | Dispositivo de interfase para el acoplamiento directo de cromatografia de liquidos y cromatografia de gases. |
-
2005
- 2005-07-11 ES ES200501686A patent/ES2265284B1/es active Active
-
2006
- 2006-07-11 WO PCT/ES2006/000394 patent/WO2007006830A2/es active Application Filing
- 2006-07-11 CN CNA2006800332180A patent/CN101262917A/zh active Pending
- 2006-07-11 JP JP2008520896A patent/JP2009500638A/ja active Pending
- 2006-07-11 EP EP06807847A patent/EP1935467A4/en not_active Withdrawn
- 2006-07-11 US US11/995,364 patent/US20080206739A1/en not_active Abandoned
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2222795A1 (es) * | 2003-03-28 | 2005-02-01 | Universidad De Castilla-La Mancha | Metodo de analisis de residuos de plaguicidas en aceites vegetales. |
Non-Patent Citations (3)
Title |
---|
PEREZ M. ET AL.: "On-line reversed phase LC-GC by using the new TOTAD (Through Oven Transfer Adsorption Desorption) interface: Application to Parathion residue analysis", JOURNAL OF MICROCOLUMN SEPARATIONS, vol. 11, no. 8, 1999, pages 582 - 589, XP002508939 * |
SANCHEZ R. ET AL.: "Automated multiresidue analysis of pesticide residues in olive oil by on-line reversed phase liquid chromatography-gas chromatography using an automated through oven transfer adsorption desorption (TOTAD) interface", JOURNAL OF CHROMATOGRAPHY A, vol. 1029, no. 1-2, 2004, pages 167 - 172, XP004489251 * |
SANCHEZ R. ET AL.: "Direct analysis of pesticide residues in olive oil by on-line reversed phase liquid chromatography-gas chromatography using an automated through oven transfer adsorption desorption (TOTAD) interface", JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, vol. 51, no. 21, 2003, pages 6098 - 6102, XP003010295 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103558298A (zh) * | 2013-08-07 | 2014-02-05 | 公安部物证鉴定中心 | 利用凝胶渗透色谱处理生物检材的有机磷农药检验方法 |
CN103558298B (zh) * | 2013-08-07 | 2015-03-25 | 公安部物证鉴定中心 | 利用凝胶渗透色谱处理生物检材的有机磷农药检验方法 |
Also Published As
Publication number | Publication date |
---|---|
EP1935467A2 (en) | 2008-06-25 |
JP2009500638A (ja) | 2009-01-08 |
ES2265284B1 (es) | 2008-02-01 |
WO2007006830A2 (es) | 2007-01-18 |
US20080206739A1 (en) | 2008-08-28 |
EP1935467A4 (en) | 2010-10-20 |
ES2265284A1 (es) | 2007-02-01 |
CN101262917A (zh) | 2008-09-10 |
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