WO2003095390A1 - Procede de production de carreau de type tenmoku denature par cuisson - Google Patents

Procede de production de carreau de type tenmoku denature par cuisson Download PDF

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Publication number
WO2003095390A1
WO2003095390A1 PCT/JP2003/005895 JP0305895W WO03095390A1 WO 2003095390 A1 WO2003095390 A1 WO 2003095390A1 JP 0305895 W JP0305895 W JP 0305895W WO 03095390 A1 WO03095390 A1 WO 03095390A1
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WIPO (PCT)
Prior art keywords
kiln
glaze
tile
mold
firing
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Application number
PCT/JP2003/005895
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English (en)
Japanese (ja)
Inventor
Ikuyoshi Kojima
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Ikuyoshi Kojima
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Publication date
Application filed by Ikuyoshi Kojima filed Critical Ikuyoshi Kojima
Priority to AU2003235218A priority Critical patent/AU2003235218A1/en
Publication of WO2003095390A1 publication Critical patent/WO2003095390A1/fr

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B28—WORKING CEMENT, CLAY, OR STONE
    • B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B11/00—Apparatus or processes for treating or working the shaped or preshaped articles
    • B28B11/04—Apparatus or processes for treating or working the shaped or preshaped articles for coating or applying engobing layers
    • B28B11/044—Apparatus or processes for treating or working the shaped or preshaped articles for coating or applying engobing layers with glaze or engobe or enamel or varnish

Definitions

  • the present invention relates to a method for manufacturing a glazed tile, a glaze, and a glazed tile. More particularly, the present invention relates to a method for manufacturing a kiln with a modified Tenmoku tile, a kiln with a modified Tenmoku glaze, and a kiln with a modified Tenmoku tile.
  • Tiles that emit metallic colours or irises include the so-called ras-yui tiles, which are raster-colored.
  • Ras Yuichi tiles are tiles that are heated to 400 ° C to 450 ° C and a metal salt solution (for example, titanium chloride solution) is deposited on the surface to form an extremely thin metal film. Is generated.
  • the metal film itself does not have adhesiveness, and is easily scratched and bald due to its micron-order thickness. Also, if used on the outer wall, it will fade in several years and will not shine. Therefore, it is difficult to use it as a building material. Also, since a large amount of chlorine gas is generated in the manufacturing process, metal equipment and equipment corrode, and there are many health problems.
  • Another method for producing luminous tiles is to use glaze that contains a large amount of PbO.
  • This method does not have a large problem because the amount of PbO used is small for products with relatively low production volume such as ceramics, but when applied to products such as ceramic tiles with large production volume, lead poisoning problem in glaze treatment There is a problem that it will occur, and there has been almost no demand for building materials since the 1970s.
  • a further method is to dissolve soluble oil in an oily solvent.
  • water gold containing 10 to 20% by mass of the compound is applied to the tile surface with a brush or by transfer and fired.
  • this method is very expensive and difficult to apply as a method of manufacturing building materials except in special cases. Disclosure of the invention
  • the present invention provides a method for producing a glazed tile, a glaze, and a glazed tile, in particular, a method for producing a kiln-modified Tenmoku tile, a kiln-modified Tenmoku glaze, and a kiln-modified Tenmoku tile glazed thereon.
  • the mold is filled with a powdery tile body and a powdery kiln varnished glaze, molded under pressure, demolded, dried and fired to produce a kiln varnished tile. Law.
  • Glaze A method of manufacturing a kiln with a multi-layered or multi-layered drug, followed by drying and firing.
  • a method for manufacturing a kiln tentem tile which comprises multiplying or multiplying, drying and firing.
  • a kiln characterized by kneading or stirring the raw material of the tile body, wet- or mold-molding it, drying it, and then glazing it with a plaster-like or mud-like kiln, and drying and firing. The method of manufacturing the phenomena tile.
  • Fe 2 0 3 material is Benigara, demon plate, an iron compound, selected from the group consisting of iron-containing raw material, and these mixtures of two or more, (2) feldspathic raw materials, Schuu feldspar, Selected from the group consisting of Kamado feldspar, Ohira feldspar, and a mixture of two or more of them; (3) the siliceous raw material is silica stone and Z or silica sand; (4) a coloring agent and / or a coloring auxiliary material Is selected from the group consisting of copper oxide, copper carbonate, cobalt oxide, manganese oxide, tin oxide, bone ash, rutile, manganese dioxide, titanium oxide, antimony oxide, and a mixture of two or more of these.
  • the clay raw material is selected from the group consisting of frog eye clay, kaolin, kibushi clay, ceramic waste soil, and a mixture of two or more of these.
  • the solvent-soluble raw materials are limestone, limestone, and fluorite.
  • the above 12 selected from the group consisting of strontium carbonate, lithium carbonate, waste glass, sewage sludge incineration ash, sewage sludge melting slag, municipal waste incineration ash, municipal waste melting slag, earth ash, and a mixture of two or more of these Or
  • Tile body raw materials are sewage sludge incineration ash, sewage sludge melting slag, Tokyo garbage incineration ash, Tokyo garbage melting slag, crushed stone, ceramic waste material, inorganic silica sand, mineral sand, ceramic chamotte, recycled material 15.
  • a kiln metaten tile made by glazing the tile body base with the kiln metaten glaze described in 19 or 20 above.
  • Tile body raw materials are sewer sludge incineration ash, sewer sludge melting slag, Tokyo garbage incineration ash, Tokyo garbage melting slag, crushed stone, ceramic waste material, inorganic silica sand, mineral sand, ceramic chamotte, and these.
  • 21. The kiln-modified tile according to 21 above, comprising a material selected from the group consisting of a mixture of two or more types.
  • an electromagnetic wave with a wavelength of 4.0 to 14.0 zm is also called a growing light ray, and has the strongest energy as a weak energy that has a good effect on the cells of an object or a moving plant.
  • a photoelectric effect which is a materialization phenomenon of light, is provided to atoms or molecules as units.
  • the kiln Tenten-y ⁇ which is glazed with the kiln-tenten glaze of the present invention efficiently emits far-infrared rays even at a low temperature such as room temperature. Therefore, in addition to the beauty of the Tenten tiles, it also functions as a far-infrared radiator. Therefore, the kiln-modified tile of the present invention can also be used as a far-infrared radiator.
  • Fig. 1 shows the far-infrared emissivity curves of the kiln tentacle tiles obtained in Example 1 and Example 3. In each case, the high-efficiency emissivity characteristics approximated to a flat blackbody in the far-infrared region. Is shown. Note that Examples 1 and 3 were both samples that were fired after double application, and the far-infrared emissivity was measured by the spectral emissivity measurement method of JIS, R1801, FTII (see Fig. The same applies to the measurements of 2 to 4).
  • FIG. 2 is a far-infrared radiation divergence curve at 400 ° C. of the kiln-modified tiles obtained in Example 1 and Example 3. Each shows a high divergence curve close to a black body.
  • FIG. 3 is a far-infrared radiation divergence curve at 100 ° C. of the kiln Tenten tiles obtained in Examples 1 and 3. It encompasses the 4.0 to 14.0 micron region, which is generally called far-infrared, and has a gentle curve close to the ideal blackbody. Various applications can be expected in this region in the future.
  • FIG. 4 shows far-infrared radiation divergence curves at 3 ° C. of the kiln-modified Tenmoku tiles obtained in Example 1 and Example 3. Although the radiant emittance has been reduced, it has an indispensable attractiveness at room temperature.
  • Kiln Transformation Tiles are tiles that exhibit unexpected glaze color and glaze phase during firing due to the temperature of the kiln and the components of the glaze. Say. In particular, iron glaze is mainly applied since there are many changes due to iron and iron-containing dangling products. Means a tile that has been used.
  • the present invention provides a method for producing a glazed evening file that retains a very beautiful pattern and luminosity over many years without any fading of the kiln color even when used on the inner and outer walls. Is in the following points.
  • the glass is fired at a high temperature of 1300 ° C or higher, so that the glaze melts and even if it contains a small amount of harmful substances such as heavy metals, it is sealed in the glaze, and the It does not elute.
  • the surface layer is thick, for example, 1.0 to 2.0, and has a composition that is resistant to air pollution.
  • the glaze surface has a beautiful and attractive pattern color, and a silver-colored spot appears in a drip-like manner on the glaze surface. It is pronounced of oil droplets, moss, characters, shukko, and akiha, produced in the Southern Song Dynasty in the 12th and 13th centuries of China. Even today, with the advancement of science, the principle of formation of these glazes has not been clearly elucidated. Therefore, these pottery works are designated as national treasures and rebuns, and are very precious and expensive.
  • the present invention challenges these unknown worlds, and as a result of scientifically investigating the origins, provides a method for stably mass-producing kiln-mounted tentacle tiles with a surface finish comparable to Chinese products 900 years ago. Is what you do. Further, as shown in the representative examples 1 and 3 described later, the composition contains a high-efficiency far-infrared radiator.
  • the raw material for the tile body used in the present invention is not particularly limited, and sewage sludge incineration ash, sewage sludge melting slag, Tokyo garbage incineration ash, Tokyo garbage melting slag, crushed stone, ceramics waste raw material, inorganic silica sand, and mineral sand , Pottery chamotte, recycled materials, and mixtures of two or more of these.
  • Recycling raw materials such as waste ceramic waste, silica sand gira, ceramic waste, ceramic waste, etc., which were previously discarded, are mainly used, and the use of virgin materials is kept to a minimum. It is possible.
  • the above-mentioned kiln meta-temporary glaze is applied to the kiln meta-temple tile used in the present invention.
  • This glaze is characterized in that it contains a predetermined amount of iron oxide and phosphorus.
  • the amount of glaze is in the range of 0.5 to 2.5 bandages, preferably 1.0 to 2.0 Ornrn in terms of thickness after firing.
  • the reason why the thickness of the glaze layer is made thicker than usual is to promote the active movement of the glaze melted during firing and the generation of kiln phenomena.
  • far-infrared emissivity is also highly developed.
  • first kiln phenomena glaze after the above-mentioned first kiln phenomena glaze, further, glazes having properties different from those of the first kiln phenomena glaze are double-coated, triple-coated, or multiply-coated, and It can be dried and fired.
  • first kiln variant Tenten glaze forming the glaze surface layer and the double haze glaze having different properties are melted and mixed, This has the advantage that the surface layer becomes more rigid and covered, making it less prone to scratches.
  • the double coating may cause a chemical reaction between the glaze and the glaze during firing, forming a certain beautiful pattern.
  • glazes with different properties are multiplied three times or more, so that the glaze and the glaze melt and mix with each other to make the surface layer thicker and stronger, but also unexpected glows, patterns, oil spots It is possible to form texts and produce literal kiln tiles.
  • the multiply or more multiply technique of the present invention can be used in the past. This is a unique method.
  • triple or multiple glazing with a variety of glazes with different properties and applying them in multiple layers, patterns and kiln phenomena that suddenly surpass the expectation are suddenly deposited. This rare chemical reaction is very complex and hard to explain, but it is the result of the excellence of modern science in a controlled atmosphere.
  • a transparent glaze represented by the following Zegel formula is preferable.
  • Ti0 2 double hung, glazed amount in triple seat, or more multi-threading is 0 in thickness after firing. 1 to 0. 5 mm, preferably 0.1 5 ⁇ 0.4 is recommended. If the amount of glaze is less than this range, the desired effect will not be sufficiently exhibited, and if it is too large, the glaze will flow too much in the kiln and the kiln and the kiln tools may be damaged.
  • the mold is filled with a powdery tile body or a powdery evening body and a powdery kiln varnished glaze, molded under pressure, demolded, and dried. , Firing.
  • the pressure at the time of pressure molding is preferably 150 to 300 kg / cm 2 , and more preferably 180 to 250 kg / cm 2 . Drying must be performed sufficiently at 80 to 120 ° C for about 8 to 20 hours.
  • glazes of different properties may be doubled or multiplied if necessary, dried, and fired. Firing should be performed at 1280 ⁇ 1; 330 ° C for 1 hour to 3 hours for Laura-Haaskirn, and for 5 hours to 15 hours for tunnel kiln and ⁇ ⁇ shtor kiln. Is preferred.
  • the calcination can be carried out in an oxidized, neutral or reduced state.
  • Double gel type of transparent hanging glaze (A)
  • the mold (length: 157.5 thigh x width: 157.5 ⁇ , height: 26 ⁇ ) has tile body material (30% by mass of silica sand, elutriation clay: 15% by mass, applied mass: 15% by mass, ceramic waste soil) Powder (20 mesh) of 15 mass%, 15 mass% of feldspar and 10 mass% of crushed cerben) was filled with 56 Og, and the thickness was averaged so as to average. On top of this, 84 g of the above No. 1 glaze powder (100 mesh) was filled and molded under a pressure of 230 kg / cm 2 . Remove the molded body (length 157.5 recommended X width 157.5 brain X height 14) from the mold, RHK (length 50m width 1.5m, height 0.3m), maximum temperature 1300 ° Oxidation and baking for 160 minutes at C.
  • the glaze is completely melted during the next 32 minutes while traveling 10 m and kept at 1300 ° C for 25 minutes.
  • This glaze has a large amount of clay and is hard to flow, but it reacts with CaO and MgO as a solvent to promote melting.
  • P 2 0 5, Sb 2 0 3 coloring adjuvant also, contaminants traces contained and therein F e 2 0 3 of ⁇ also narrowing melted in the glaze, creating bubbles, saturation state
  • the activated Fe 2 O 3 behaves vigorously and exerts various glaze effects, and crystals of metal spots precipitate on the glaze surface.
  • the baked tiles have a shiny rat-silver-colored kiln-denten glaze deposited on the entire surface of the glaze.
  • the method of manufacturing the Tenten tiles in the kiln by the extremely short-time firing by the RHK of the present invention is a kiln with uniform quality by adopting a glaze mix suitable for the kiln, firing time, firing temperature, firing atmosphere and appropriate cooling. It is a baking method that can stably produce metamorphic tiles and breaks the conventional belief.
  • the above-mentioned transparent glaze is slightly double-coated on the molded body prepared in the above (1) so as to have a thickness of 0.1 to 0.2 after firing, and then the same as in the above (1).
  • Double hanging transparent glaze A) Seedling type of transparent glaze (B)
  • No. 2 glaze 100 mesh
  • the No.2 glaze, A1 2 0 medium solvent than in 3 alkali metal oxides and alkaline earth metal oxides
  • the glaze used in the powder so as to have a thickness of glaze becomes nonuniform, consciously evening with the unevenness with Irubode one matrix material in ⁇ layer, integrally molded by applying a pressure of 25 Okg / cm 2 Was.
  • the first pre-tropical zone will go 10m in 15 minutes and reach 800 ° C.
  • the glaze will melt completely during 10m, and keep at 1300 ° C for 12 minutes.
  • This glaze is a sticky and hard glaze, but moves slightly from the convex part to the concave part of the glaze layer.
  • the double-glazed transparent glaze has low viscosity and is easy to flow, so it starts to work first, and iron flows into bubbles to promote the deposition of vivid silver raster.
  • ⁇ During the next 15 minutes, cool rapidly from 1250 ° C to 600 ° C while traveling 10m. During this time, the bubbles subside.
  • the triple-glazed transparent glaze (B) was glazed (approximately 0.2 strokes after firing) on the double-glazed molded product, and dried at 100 ° C for 10 hours. Oxidized and calcined at 1300 ° C for 160 minutes with RHK, as in 1. As a result, an even deeper mottle pattern was deposited on the entire surface. This phenomenon is Fe 2 0 3 and Ti_ ⁇ 2 contained in different glaze compositions further actively moved from the time of the double-seat, presumably because the crystal with a large grain oil droplets tenmoku have emerged.
  • Example 2 (1) In the same manner as in Example 1, a mold (length: 157.5 thigh x width: 157.5 wisteria x height: 26 mm) was filled with 510 g of powder (20 mesh) of a raw material for tile body, and the thickness was reduced. Averaged to average. This was molded under a pressure of 23 Okg cm 2 . Remove the molded body (length 157.5, X 157.5 ⁇ , height 12.5 flat) from the mold and put 84 g of the above No. 3 glaze powder (100 mesh) on 210 ml of water. The mixture was thickly applied (approximately 1.3 thighs after baking), dried, kept at 1300 ° C. for 12 minutes at RHK, and baked for 70 minutes with oxidized water.
  • Double hanging transparent glaze (A)
  • Example 1 (1) In the same manner as in Example 1, the mold was filled with 56 Og of powder (20 mesh) of the tile body raw material, and the thickness was equalized so as to average. 84 g of the above No.4 glaze powder (100 mesh) is filled on top of this, and a pressure of 230 kg / cm 2 is applied to this. And molded. The molded body (157.5 in length X 157.5 in thigh X height 14.0 recommended) was removed from the mold and baked with RHK at 1300 ° C for 80 minutes with oxidized water. As a result, fine dots glistened on the upper layer, and glazes comparable to the mosquitoes appeared on the surface. This formulation is a hard glaze and hard to flow, but it is considered that the iron was precipitated in a short period of time by combining with a metallic substance containing various trace impurities.
  • Example 1 (1) In the same manner as in Example 1, the mold was filled with 560 g of the powder of the tile body raw material, and the thickness was averaged so as to average. On top of this, 84 g of the above No. 5 glaze powder (100 mesh) was filled and molded under a pressure of 230 kg / cm 2 . Remove the molded body (length 157.5mm x width 157.5 thigh x height 14. Omni) from the mold and disperse the above transparent glaze (B) powder (100 mesh) 24. Og in 95ml water The resulting product was double hung so that the thickness after firing became 0.2 to 0.4 thigh, and oxidized and fired at 1300 ° C for 160 minutes at RHK.
  • No. 5 glaze powder 100 mesh
  • the composition of the No. 5 glaze A1 2 0 3 is small, on the easily flows glaze, double hung with transparent glaze (B) also for easily flows glaze, P 2 0 5 to Fe 2 0 3 of glaze, Ti0 melted 2 in the early to reaction step, further each other and easily flows glaze be likewise melted flow above reaction glaze, is also considered to and to form an attractive reptile pattern.
  • Example 1 Similar to 10.7% Fe 2 0 3 Example 1, the mold filled with powder (2 0 mesh) 2 9 O g of Tairubode one matrix material and leveled to a thickness to average. On top of this, 280 g of the powder of No. 6 glaze (100 mesh) was filled, and on top of this, The powder was filled with 290 g, and the thickness was averaged so as to average. This was molded under a pressure of 200 kg // cm 2 . The molded body (length 2 48 8 x width 66 6 x height 31 fiber) was removed from the mold, and nails were inserted into the glaze layer from both sides to split the glaze layer into two. This was fired at 1300 ° C for 80 minutes with an oxide at RHK.
  • the present invention thoroughly investigates these unknown reasons scientifically, and provides a kiln-adapted tile that does not lose its beauty as a building material that can withstand aging over many years.
  • most of the glaze raw materials used in the tile manufacturing process use purified raw materials from which impurities and contaminants have been removed to improve productivity.
  • the glazes for kiln Tenten tiles are manufactured using such high-purity raw materials, only extremely ordinary or disappointing standardized products can be obtained.
  • the present invention uses glaze containing natural raw materials and recycled raw materials produced from the natural world.
  • the dagger contains trace amounts of copper, tungsten, manganese, titanium, and the like as impurities, and these impurities are considered to have contributed to the formation of subtle surface patterns on the kiln-deformed tiles.
  • the present invention uses raw materials produced in various states as much as possible, adjusts to a sticky glaze or a free-flowing glaze according to the purpose, and, if necessary, doubles or triples or more multiples The variety of metal glazes and kiln varieties of glaze that precipitates from them is sought to stabilize.

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  • Engineering & Computer Science (AREA)
  • Structural Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Ceramic Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Finishing Walls (AREA)
  • Compositions Of Oxide Ceramics (AREA)
  • Press-Shaping Or Shaping Using Conveyers (AREA)

Abstract

L'invention concerne un procédé de production d'un carreau de type Tenmoku dénaturé par cuisson, qui consiste à remplir un moule métallique d'une matière principale pulvérulente pour carreau et d'une glaçure Tenmoku pulvérulente pouvant être dénaturée par cuisson, à former ledit carreau sous pression et à le démouler, et éventuellement à procéder à une deuxième application de glaçure possédant des propriétés différentes, à sécher l'article moulé et à chauffer l'article moulé séché. L'invention porte également sur des glaçures à utiliser dans ledit procédé et sur un carreau de type Tenmoku dénaturé par cuisson.
PCT/JP2003/005895 2002-05-10 2003-05-12 Procede de production de carreau de type tenmoku denature par cuisson WO2003095390A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU2003235218A AU2003235218A1 (en) 2002-05-10 2003-05-12 Process for producing firing-denatured tenmoku tile, firing-denatured tenmoku tile and glaze

Applications Claiming Priority (2)

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JP2002135729A JP2005320174A (ja) 2002-05-10 2002-05-10 窯変天目タイルの製造法、窯変天目タイル及び釉薬
JP2002-135729 2002-05-10

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WO2003095390A1 true WO2003095390A1 (fr) 2003-11-20

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CN107129321A (zh) * 2017-06-05 2017-09-05 任合超 一种开片钧瓷用天蓝色组合釉
CN107140947A (zh) * 2017-06-07 2017-09-08 任合超 一种表面具有夜光斑点的钧瓷及其制备工艺
CN108585789A (zh) * 2018-06-07 2018-09-28 佛山市东鹏陶瓷有限公司 一种施泥浆釉砖坯及釉面光滑的瓷砖生产方法
CN109503141A (zh) * 2018-11-12 2019-03-22 苏州工业园区职业技术学院 一种具有均匀色泽的陶瓷装饰材料

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JP5227520B2 (ja) * 2007-02-16 2013-07-03 ニチハ株式会社 釉薬組成物
JP4576550B1 (ja) * 2010-01-22 2010-11-10 株式会社関東管財 エコ資源スラグ有効利用方法
JP5349573B2 (ja) * 2011-12-26 2013-11-20 ニチハ株式会社 無機質焼成体
JP6027995B2 (ja) * 2014-03-19 2016-11-16 品野セラミックタイル工業株式会社 セラミックス製品の製造方法及びセラミックス製品
CN105272150B (zh) * 2015-10-14 2017-05-03 德化恒忆陶瓷艺术股份有限公司 天目釉瓷
CN107857572B (zh) * 2017-10-24 2020-07-07 许昌学院 钧瓷及其制作方法
JP7109344B2 (ja) * 2018-10-30 2022-07-29 小野塚 恭彦 黒天目釉薬、黒天目茶碗の製造方法
CN112500122A (zh) * 2020-12-16 2021-03-16 蔡翔 灰被毫建盏的制备工艺

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JPH0732334A (ja) * 1993-07-21 1995-02-03 Mino Ganryo Kagaku Kk 釉薬タイル及びその製造方法
JP2609193B2 (ja) * 1992-05-27 1997-05-14 株式会社イナックス 二つ割タイルの製造方法
JP6069913B2 (ja) * 2012-07-06 2017-02-01 富士通株式会社 情報処理システム、情報処理システムの制御方法及び制御プログラム

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JPH0641395B2 (ja) * 1990-06-19 1994-06-01 麒麟麦酒株式会社 ビール麦芽灰を含有した陶磁器用釉薬
JP2609193B2 (ja) * 1992-05-27 1997-05-14 株式会社イナックス 二つ割タイルの製造方法
JPH0732334A (ja) * 1993-07-21 1995-02-03 Mino Ganryo Kagaku Kk 釉薬タイル及びその製造方法
JP6069913B2 (ja) * 2012-07-06 2017-02-01 富士通株式会社 情報処理システム、情報処理システムの制御方法及び制御プログラム

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107129321A (zh) * 2017-06-05 2017-09-05 任合超 一种开片钧瓷用天蓝色组合釉
CN107140947A (zh) * 2017-06-07 2017-09-08 任合超 一种表面具有夜光斑点的钧瓷及其制备工艺
CN108585789A (zh) * 2018-06-07 2018-09-28 佛山市东鹏陶瓷有限公司 一种施泥浆釉砖坯及釉面光滑的瓷砖生产方法
CN108585789B (zh) * 2018-06-07 2020-11-13 佛山市东鹏陶瓷有限公司 一种施泥浆釉砖坯及釉面光滑的瓷砖生产方法
CN109503141A (zh) * 2018-11-12 2019-03-22 苏州工业园区职业技术学院 一种具有均匀色泽的陶瓷装饰材料

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