TWI510473B - 製備5-氟-1-烷基-3-氟烷基-1h-吡唑-4-碳醯氯 - Google Patents

製備5-氟-1-烷基-3-氟烷基-1h-吡唑-4-碳醯氯 Download PDF

Info

Publication number
TWI510473B
TWI510473B TW099139630A TW99139630A TWI510473B TW I510473 B TWI510473 B TW I510473B TW 099139630 A TW099139630 A TW 099139630A TW 99139630 A TW99139630 A TW 99139630A TW I510473 B TWI510473 B TW I510473B
Authority
TW
Taiwan
Prior art keywords
alkyl
pyrazole
formula
fluoroalkyl
carbaldehyde
Prior art date
Application number
TW099139630A
Other languages
English (en)
Chinese (zh)
Other versions
TW201127817A (en
Inventor
Sergii Pazenok
Norbert Lui
Marc Kosten
Original Assignee
Bayer Ip Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Ip Gmbh filed Critical Bayer Ip Gmbh
Publication of TW201127817A publication Critical patent/TW201127817A/zh
Application granted granted Critical
Publication of TWI510473B publication Critical patent/TWI510473B/zh

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/16Halogen atoms or nitro radicals
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/561,2-Diazoles; Hydrogenated 1,2-diazoles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Diaphragms For Electromechanical Transducers (AREA)
  • Finger-Pressure Massage (AREA)
  • Vehicle Interior And Exterior Ornaments, Soundproofing, And Insulation (AREA)
TW099139630A 2009-11-19 2010-11-18 製備5-氟-1-烷基-3-氟烷基-1h-吡唑-4-碳醯氯 TWI510473B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US26264109P 2009-11-19 2009-11-19
EP09176426A EP2325173A1 (de) 2009-11-19 2009-11-19 Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden

Publications (2)

Publication Number Publication Date
TW201127817A TW201127817A (en) 2011-08-16
TWI510473B true TWI510473B (zh) 2015-12-01

Family

ID=42077022

Family Applications (1)

Application Number Title Priority Date Filing Date
TW099139630A TWI510473B (zh) 2009-11-19 2010-11-18 製備5-氟-1-烷基-3-氟烷基-1h-吡唑-4-碳醯氯

Country Status (13)

Country Link
US (2) US8436191B2 (no)
EP (2) EP2325173A1 (no)
JP (1) JP5802213B2 (no)
KR (2) KR101749561B1 (no)
CN (1) CN102666492B (no)
BR (1) BR112012011961B1 (no)
DK (1) DK2501682T3 (no)
ES (1) ES2600864T3 (no)
IL (1) IL219682A (no)
IN (1) IN2012DN04414A (no)
MX (2) MX2012005676A (no)
TW (1) TWI510473B (no)
WO (1) WO2011061205A1 (no)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR076839A1 (es) * 2009-05-15 2011-07-13 Bayer Cropscience Ag Derivados fungicidas de pirazol carboxamidas
EP2325173A1 (de) 2009-11-19 2011-05-25 Bayer CropScience AG Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden
EP2560961B1 (de) 2010-04-23 2016-11-16 Bayer Intellectual Property GmbH Verfahren zum herstellen von 5-fluor-1-alkyl-3-fluoralkyl-1h-pyrazol-4-carbonsäurechloriden und -fluoriden
BR112014028292B1 (pt) 2012-05-14 2021-07-20 Bayer Cropscience Ag Método de preparação de cloretos de 1-alquil-3-fluoroalquil-1h-pirazol-4-carbonila
WO2014023667A1 (en) 2012-08-07 2014-02-13 Bayer Cropscience Ag Method for the preparation of perfluoroalkyl containing pyrazoles carboxylates
EP2945933B1 (en) * 2013-01-17 2016-10-12 Bayer Cropscience AG Process for preparing 5-fluoro-1-methyl-3-difluoromethyl-1h-pyrazole-4-carbaldehyde
JP6366722B2 (ja) * 2013-09-20 2018-08-01 バイエル・クロップサイエンス・アクチェンゲゼルシャフト 5−フルオロ−1−アルキル−3−フルオロアルキル−1h−ピラゾール−4−カルボアルデヒドの製造方法
JP6462703B2 (ja) * 2014-01-24 2019-01-30 バイエル・クロップサイエンス・アクチェンゲゼルシャフト 1−アルキル−3−ジフルオロメチル−5−フルオロ−1h−ピラゾール−4−カルバルデヒド類及び1−アルキル−3−ジフルオロメチル−5−フルオロ−1h−ピラゾール−4−カルボキシレート類を調製する方法
EP3122727B1 (en) 2014-03-24 2018-01-31 Bayer CropScience Aktiengesellschaft Process for preparing 3,5-bis(haloalkyl)pyrazole derivatives from alpha , alpha-dihaloamines and ketimines
EP3015458A1 (en) * 2014-11-03 2016-05-04 Bayer CropScience AG Process for preparing 3,5-bis(haloalkyl)pyrazole derivatives from a,a-dihaloamines and ketimines
TWI705055B (zh) 2015-04-29 2020-09-21 德商拜耳作物科學公司 製備5-氟-1h-吡唑-4-羰基氟化物之方法
JP6911143B2 (ja) 2018-11-07 2021-07-28 福建永晶科技股▲ふん▼有限公司Fujian Yongjing Technology Co., Ltd ピラゾール又はピリミジノンの新しい製造方法
EP4052576A4 (en) 2019-10-29 2023-10-11 Shenyang Sinochem Agrochemicals R & D Co., Ltd. AMIDE COMPOUND CONTAINING FRAGMENT OF SUBSTITUTED ACETOPHENONE STRUCTURE, PREPARATION METHOD THEREFOR AND USE THEREOF
WO2022233129A1 (en) 2021-05-05 2022-11-10 Fujian Yongjing Technology Co., Ltd New process for the synthesis of 5-fluoro-3- (difuoromethyl) -5-fluoro-1-methyl-1h-pyrazole-4-carboxylic acid derivatives and the free acid thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040110749A1 (en) * 2001-02-08 2004-06-10 Masao Nakatani Isoxazoline derivative and herbicide comprising the same as active ingredient
DE102007002674A1 (de) * 2007-01-18 2008-07-24 Bayer Cropscience Ag Verfahren zum Herstellen von substituierten Pyrazolcarbonsäurechloriden

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5223526A (en) * 1991-12-06 1993-06-29 Monsanto Company Pyrazole carboxanilide fungicides and use
DE19544800A1 (de) * 1995-12-01 1997-06-05 Bayer Ag Verfahren zur Herstellung von 1,3-Dimethyl-5-fluor-pyrazol-4-carboxaniliden
EP1405853B1 (en) * 2001-06-21 2010-11-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
UA78071C2 (en) 2002-08-07 2007-02-15 Kumiai Chemical Industry Co Herbicidal composition
WO2006000020A1 (en) 2004-06-29 2006-01-05 European Nickel Plc Improved leaching of base metals
AP2313A (en) 2004-08-18 2011-10-31 Pfizer Inhibitors of hepatitis C virus RNA-dependent RNA ploymerase, and compositions and treatments using the same.
CN101227857B (zh) 2005-06-29 2011-10-19 电脑医师有限公司 具有导电桥的传感器组件
DE102005044451A1 (de) 2005-09-17 2007-03-22 Bayer Cropscience Gmbh Verfahren zum Herstellen von 5-Fluor-1,3-dialkyl-1H-pyrazol-4-carbonsäurefluoriden
DE602006021374D1 (de) * 2005-09-27 2011-06-01 Fujifilm Corp Lithographisches Druckverfahren
AR056882A1 (es) 2006-02-01 2007-10-31 Bayer Cropscience Sa Derivados del fungicida n- cicloalquil- bencil- amida
EP2325173A1 (de) 2009-11-19 2011-05-25 Bayer CropScience AG Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040110749A1 (en) * 2001-02-08 2004-06-10 Masao Nakatani Isoxazoline derivative and herbicide comprising the same as active ingredient
DE102007002674A1 (de) * 2007-01-18 2008-07-24 Bayer Cropscience Ag Verfahren zum Herstellen von substituierten Pyrazolcarbonsäurechloriden

Also Published As

Publication number Publication date
MX2012005676A (es) 2012-06-19
ES2600864T3 (es) 2017-02-13
US8765971B2 (en) 2014-07-01
KR20120084325A (ko) 2012-07-27
WO2011061205A1 (de) 2011-05-26
BR112012011961B1 (pt) 2018-05-08
IL219682A (en) 2016-08-31
US20110207940A1 (en) 2011-08-25
DK2501682T3 (en) 2016-11-14
KR20160054041A (ko) 2016-05-13
US8436191B2 (en) 2013-05-07
EP2501682B1 (de) 2016-08-03
JP5802213B2 (ja) 2015-10-28
BR112012011961A2 (pt) 2015-09-08
EP2325173A1 (de) 2011-05-25
KR101749561B1 (ko) 2017-06-21
MX344246B (es) 2016-12-07
KR101635046B1 (ko) 2016-07-01
EP2501682A1 (de) 2012-09-26
TW201127817A (en) 2011-08-16
IN2012DN04414A (no) 2015-08-07
CN102666492A (zh) 2012-09-12
JP2013511485A (ja) 2013-04-04
IL219682A0 (en) 2012-07-31
US20130165664A1 (en) 2013-06-27
CN102666492B (zh) 2016-03-23

Similar Documents

Publication Publication Date Title
TWI510473B (zh) 製備5-氟-1-烷基-3-氟烷基-1h-吡唑-4-碳醯氯
DK2560961T3 (en) METHOD FOR PREPARING 5-FLUORO-1-ALKYL-3-FLUORALKYL-1H-PYRAZOL-4-CARBOXYLYRIC CHLORIDE AND FLUORIDES
DK1682515T3 (en) PROCEDURE FOR PREPARING FLUORMETHYL-SUBSTITUTED HETEROCYCLES
KR102006518B1 (ko) 1-알킬-3-플루오로알킬-1h-피라졸-4-카르복실산 클로라이드의 제조 방법
JP5793983B2 (ja) ピラゾール化合物の製造方法
JP5915004B2 (ja) ピラゾール化合物の製造方法
JP2013006782A (ja) ピラゾール化合物の製造方法
JP5067780B2 (ja) パーフルオロアルキル基を有するキノリン類の製造方法
JP5790195B2 (ja) ピラゾール化合物の製造方法
JP6349329B2 (ja) 5−フルオロ−1−メチル−3−ジフルオロメチル−1h−ピラゾール−4−カルバルデヒドを調製する方法