TWI307688B - Process for the preparation of cyclic diketones - Google Patents

Process for the preparation of cyclic diketones Download PDF

Info

Publication number
TWI307688B
TWI307688B TW092107861A TW92107861A TWI307688B TW I307688 B TWI307688 B TW I307688B TW 092107861 A TW092107861 A TW 092107861A TW 92107861 A TW92107861 A TW 92107861A TW I307688 B TWI307688 B TW I307688B
Authority
TW
Taiwan
Prior art keywords
group
alkyl
formula
alkoxy
compound
Prior art date
Application number
TW092107861A
Other languages
English (en)
Chinese (zh)
Other versions
TW200307663A (en
Inventor
Hermann Schneider
Christoph Luthy
Andrew Edmunds
Original Assignee
Syngenta Participations Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Syngenta Participations Ag filed Critical Syngenta Participations Ag
Publication of TW200307663A publication Critical patent/TW200307663A/zh
Application granted granted Critical
Publication of TWI307688B publication Critical patent/TWI307688B/zh

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/77—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D307/78—Benzo [b] furans; Hydrogenated benzo [b] furans
    • C07D307/79—Benzo [b] furans; Hydrogenated benzo [b] furans with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to carbon atoms of the hetero ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C315/00—Preparation of sulfones; Preparation of sulfoxides
    • C07C315/04—Preparation of sulfones; Preparation of sulfoxides by reactions not involving the formation of sulfone or sulfoxide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/20—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/22—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and doubly-bound oxygen atoms bound to the same carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/45—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
    • C07C45/455—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation with carboxylic acids or their derivatives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/54—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of compounds containing doubly bound oxygen atoms, e.g. esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/56—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds
    • C07C45/57—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/56—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds
    • C07C45/57—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom
    • C07C45/60—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom in six-membered rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
    • C07C49/703—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups
    • C07C49/723—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups polycyclic
    • C07C49/727—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups polycyclic a keto group being part of a condensed ring system
    • C07C49/733—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups polycyclic a keto group being part of a condensed ring system having two rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D213/44—Radicals substituted by doubly-bound oxygen, sulfur, or nitrogen atoms, or by two such atoms singly-bound to the same carbon atom
    • C07D213/46—Oxygen atoms
    • C07D213/50—Ketonic radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/36—Systems containing two condensed rings the rings having more than two atoms in common
    • C07C2602/44—Systems containing two condensed rings the rings having more than two atoms in common the bicyclo ring system containing eight carbon atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Furan Compounds (AREA)
  • Pyridine Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
TW092107861A 2002-04-09 2003-04-07 Process for the preparation of cyclic diketones TWI307688B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH5982002 2002-04-09

Publications (2)

Publication Number Publication Date
TW200307663A TW200307663A (en) 2003-12-16
TWI307688B true TWI307688B (en) 2009-03-21

Family

ID=28048300

Family Applications (1)

Application Number Title Priority Date Filing Date
TW092107861A TWI307688B (en) 2002-04-09 2003-04-07 Process for the preparation of cyclic diketones

Country Status (19)

Country Link
US (2) US6855831B2 (fr)
EP (1) EP1352901B1 (fr)
JP (1) JP4402363B2 (fr)
KR (1) KR100964481B1 (fr)
CN (1) CN100513381C (fr)
AR (1) AR039386A1 (fr)
AT (1) ATE409690T1 (fr)
AU (1) AU2003203482B2 (fr)
BR (1) BR0300877A (fr)
CA (1) CA2424803C (fr)
DE (1) DE60323778D1 (fr)
ES (1) ES2315441T3 (fr)
IL (1) IL155234A (fr)
MX (1) MXPA03003061A (fr)
PL (1) PL211016B1 (fr)
RU (1) RU2316544C2 (fr)
TW (1) TWI307688B (fr)
UA (1) UA78685C2 (fr)
ZA (1) ZA200302618B (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU2003203482B2 (en) * 2002-04-09 2005-06-02 Syngenta Participations Ag Process for the preparation of cyclic diketones
KR101147632B1 (ko) 2004-04-30 2012-05-23 신젠타 리미티드 사이클릭 디케톤의 제조방법
US20080142375A1 (en) * 2006-12-13 2008-06-19 Francois Doniat Electrolyte formulation for electrochemical mechanical planarization
GB0710223D0 (en) * 2007-05-29 2007-07-11 Syngenta Ltd Novel Herbicides
CN110818542A (zh) * 2019-11-27 2020-02-21 怀化旺达生物科技有限公司 一种1，2-环己二酮的纯化方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2261751C3 (de) * 1972-12-16 1981-12-24 Hoechst Ag, 6000 Frankfurt Verfahren zur Herstellung von Cyclohexandionen-(1,3)
IL77350A (en) 1984-12-20 1991-01-31 Stauffer Chemical Co Production of acylated diketonic compounds
PT1114030E (pt) * 1998-09-15 2005-09-30 Syngenta Participations Ag Piridina cetonas uteis como herbicidas
AU1982600A (en) 1998-12-21 2000-07-12 Syngenta Participations Ag Novel herbicides
SE0000772D0 (sv) * 2000-03-08 2000-03-08 Astrazeneca Ab Chemical compounds
WO2001066522A1 (fr) 2000-03-09 2001-09-13 Syngenta Participations Ag Herbicides phenyl acyle ou pyridine
GT200100103A (es) 2000-06-09 2002-02-21 Nuevos herbicidas
AU2003203482B2 (en) * 2002-04-09 2005-06-02 Syngenta Participations Ag Process for the preparation of cyclic diketones

Also Published As

Publication number Publication date
US20030199708A1 (en) 2003-10-23
EP1352901B1 (fr) 2008-10-01
EP1352901A2 (fr) 2003-10-15
IL155234A0 (en) 2003-11-23
CN1450047A (zh) 2003-10-22
ZA200302618B (en) 2003-10-06
TW200307663A (en) 2003-12-16
AU2003203482B2 (en) 2005-06-02
AR039386A1 (es) 2005-02-16
IL155234A (en) 2010-05-17
PL359520A1 (en) 2003-10-20
CA2424803C (fr) 2011-01-25
AU2003203482A1 (en) 2003-10-23
ATE409690T1 (de) 2008-10-15
KR100964481B1 (ko) 2010-06-21
US7135574B2 (en) 2006-11-14
CA2424803A1 (fr) 2003-10-09
DE60323778D1 (de) 2008-11-13
KR20030081064A (ko) 2003-10-17
US20050159314A1 (en) 2005-07-21
RU2316544C2 (ru) 2008-02-10
JP4402363B2 (ja) 2010-01-20
UA78685C2 (en) 2007-04-25
PL211016B1 (pl) 2012-03-30
CN100513381C (zh) 2009-07-15
EP1352901A3 (fr) 2004-03-24
ES2315441T3 (es) 2009-04-01
MXPA03003061A (es) 2003-10-14
US6855831B2 (en) 2005-02-15
JP2003313161A (ja) 2003-11-06
BR0300877A (pt) 2004-08-17

Similar Documents

Publication Publication Date Title
CN101889009A (zh) c-fms激酶抑制剂
JP7052798B2 (ja) アゾールで置換されたピリジン化合物
JPH09505294A (ja) プロテアーゼ阻害剤および抗ウイルス剤としての５，６−ジヒドロピロン誘導体
CN107814785A (zh) 雄激素受体拮抗剂及其制备方法和用途
IL296920A (en) Indole derivatives as alpha-1-antitrypsin modulators for the treatment of alpha-1-antitrypsin deficiency (aatd)
TWI361688B (en) Process for the preparation of isothiazole derivatives
TWI307688B (en) Process for the preparation of cyclic diketones
TW200901980A (en) Benzimidazole cannabinoid agonists
HUT75225A (en) 5,6-dihydropyrone derivatives as protease inhibitors and antiviral agents
JP4971141B2 (ja) 環式ジケトンの製造方法
US9988361B2 (en) Anti-enterovirus 71 thiadiazolidine derivative
JP2020536944A (ja) ３−（５−フルオロベンゾフラン−３−イル）−４−（５−メチル−５Ｈ−［１，３］ジオキソロ［４，５−ｆ］インドール−７−イル）ピロール−２，５−ジオンの固体形態
WO2001007401A1 (fr) Composes tricycliques et compositions medicamenteuses les contenant
JP5740042B2 (ja) 化合物、化合物の製造方法、及び化合物の精製方法
TW200306304A (en) Process for the preparation of bicyclic diketone salts
JP4819798B2 (ja) 環式ジケトンの製造方法
KR101348304B1 (ko) ((2Ｚ)-3-[(6-메틸피리딘-3-일)메틸-1,3-티아졸리딘-2-이리덴]시아나미드, 티아클로프리드(Ｔｈｉａｃｌｏｐｒｉｄ))의 제조방법
KR100576339B1 (ko) 피리다진-4-온 유도체, 그 제조방법 및 약제학적 조성물
TW202021971A (zh) 雙環雜芳香環衍生物
TW201936597A (zh) 製備經取代之（１ｈ－１，２，４－三唑－１－基）醇類之方法
JP2687811B2 (ja) エーテル類の製造法

Legal Events

Date Code Title Description
MM4A Annulment or lapse of patent due to non-payment of fees