SU906383A3 - Способ получени поверхностно активного вещества - Google Patents
Способ получени поверхностно активного вещества Download PDFInfo
- Publication number
- SU906383A3 SU906383A3 SU752184053A SU2184053A SU906383A3 SU 906383 A3 SU906383 A3 SU 906383A3 SU 752184053 A SU752184053 A SU 752184053A SU 2184053 A SU2184053 A SU 2184053A SU 906383 A3 SU906383 A3 SU 906383A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- reaction
- sucrose
- fatty acid
- catalyst
- surfactant
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 18
- 239000004094 surface-active agent Substances 0.000 title claims abstract description 12
- 229930006000 Sucrose Natural products 0.000 claims abstract description 20
- 239000005720 sucrose Substances 0.000 claims abstract description 20
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 19
- 239000003054 catalyst Substances 0.000 claims abstract description 14
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 8
- 239000000194 fatty acid Substances 0.000 claims abstract description 8
- 229930195729 fatty acid Natural products 0.000 claims abstract description 8
- 150000004665 fatty acids Chemical class 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 7
- 238000005809 transesterification reaction Methods 0.000 claims description 7
- 125000004432 carbon atom Chemical group C* 0.000 claims description 5
- 150000005690 diesters Chemical class 0.000 claims description 2
- -1 sucrose fatty acid Chemical class 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims 2
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 abstract description 18
- 239000002904 solvent Substances 0.000 abstract description 5
- 238000002156 mixing Methods 0.000 abstract description 4
- 239000007787 solid Substances 0.000 abstract description 3
- 239000011149 active material Substances 0.000 abstract 2
- 125000004169 (C1-C6) alkyl group Chemical group 0.000 abstract 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 abstract 1
- 150000008041 alkali metal carbonates Chemical class 0.000 abstract 1
- 150000004703 alkoxides Chemical class 0.000 abstract 1
- 230000032050 esterification Effects 0.000 abstract 1
- 238000005886 esterification reaction Methods 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 description 12
- 125000005907 alkyl ester group Chemical group 0.000 description 10
- 239000000047 product Substances 0.000 description 10
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 8
- 229910000027 potassium carbonate Inorganic materials 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- 239000003925 fat Substances 0.000 description 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
- 150000003626 triacylglycerols Chemical class 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 2
- 239000002385 cottonseed oil Substances 0.000 description 2
- 235000012343 cottonseed oil Nutrition 0.000 description 2
- 239000000944 linseed oil Substances 0.000 description 2
- 235000021388 linseed oil Nutrition 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 235000019198 oils Nutrition 0.000 description 2
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 description 1
- WHBHBVVOGNECLV-OBQKJFGGSA-N 11-deoxycortisol Chemical compound O=C1CC[C@]2(C)[C@H]3CC[C@](C)([C@@](CC4)(O)C(=O)CO)[C@@H]4[C@@H]3CCC2=C1 WHBHBVVOGNECLV-OBQKJFGGSA-N 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 240000007817 Olea europaea Species 0.000 description 1
- 235000019482 Palm oil Nutrition 0.000 description 1
- 235000021314 Palmitic acid Nutrition 0.000 description 1
- 235000019483 Peanut oil Nutrition 0.000 description 1
- 235000021355 Stearic acid Nutrition 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 150000005215 alkyl ethers Chemical class 0.000 description 1
- 150000007514 bases Chemical class 0.000 description 1
- OGBUMNBNEWYMNJ-UHFFFAOYSA-N batilol Chemical class CCCCCCCCCCCCCCCCCCOCC(O)CO OGBUMNBNEWYMNJ-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000001642 boronic acid derivatives Chemical group 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000000543 intermediate Substances 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 150000004702 methyl esters Chemical class 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000021313 oleic acid Nutrition 0.000 description 1
- 150000002889 oleic acids Chemical class 0.000 description 1
- 150000007530 organic bases Chemical group 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- 150000002943 palmitic acids Chemical class 0.000 description 1
- 239000000312 peanut oil Substances 0.000 description 1
- 239000000546 pharmaceutical excipient Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000007127 saponification reaction Methods 0.000 description 1
- 150000004760 silicates Chemical group 0.000 description 1
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
- C07H13/06—Fatty acids
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/34—Higher-molecular-weight carboxylic acid esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
- C11C1/002—Sources of fatty acids, e.g. natural glycerides, characterised by the nature, the quantities or the distribution of said acids
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S516/00—Colloid systems and wetting agents; subcombinations thereof; processes of
- Y10S516/01—Wetting, emulsifying, dispersing, or stabilizing agents
- Y10S516/02—Organic and inorganic agents containing, except water
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Microbiology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biotechnology (AREA)
- Wood Science & Technology (AREA)
- Materials Engineering (AREA)
- Saccharide Compounds (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB45122/74A GB1499989A (en) | 1974-10-17 | 1974-10-17 | Production of a surface active material containing sucrose esters |
| GB1622275 | 1975-04-18 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU906383A3 true SU906383A3 (ru) | 1982-02-15 |
Family
ID=26251906
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU752184053A SU906383A3 (ru) | 1974-10-17 | 1975-10-17 | Способ получени поверхностно активного вещества |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US4032702A (en, 2012) |
| JP (1) | JPS5165704A (en, 2012) |
| AR (1) | AR212161A1 (en, 2012) |
| AT (1) | AT347410B (en, 2012) |
| BR (1) | BR7506830A (en, 2012) |
| CA (1) | CA1045130A (en, 2012) |
| CH (1) | CH606074A5 (en, 2012) |
| CU (1) | CU34398A (en, 2012) |
| DE (1) | DE2546716C3 (en, 2012) |
| DK (1) | DK142148B (en, 2012) |
| ES (1) | ES441908A2 (en, 2012) |
| FR (1) | FR2288143A2 (en, 2012) |
| GB (1) | GB1499989A (en, 2012) |
| IE (1) | IE42171B1 (en, 2012) |
| IT (1) | IT1048249B (en, 2012) |
| NL (1) | NL172761B (en, 2012) |
| NO (1) | NO140983C (en, 2012) |
| SE (1) | SE430339B (en, 2012) |
| SU (1) | SU906383A3 (en, 2012) |
| TR (1) | TR18880A (en, 2012) |
| ZA (1) | ZA756573B (en, 2012) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1593856A (en) * | 1976-11-17 | 1981-07-22 | Gist Brocades Nv | Process for the treatment of fruit and vegetables |
| JPS6037085B2 (ja) * | 1978-09-22 | 1985-08-24 | 花王株式会社 | 棒状化粧料 |
| JPS5547610A (en) * | 1978-09-29 | 1980-04-04 | Kao Corp | Hair cosmetic |
| JPS6026368B2 (ja) * | 1978-09-29 | 1985-06-24 | 花王株式会社 | 粉末圧縮型化粧料 |
| JPS6037086B2 (ja) * | 1978-09-26 | 1985-08-24 | 花王株式会社 | 化粧料 |
| JPS6037087B2 (ja) * | 1978-09-28 | 1985-08-24 | 花王株式会社 | 化粧料 |
| EP0010975B1 (en) * | 1978-11-06 | 1983-05-18 | TATE & LYLE PUBLIC LIMITED COMPANY | Gramophone record composition and gramophone records produced therefrom |
| EP0011419A1 (en) * | 1978-11-09 | 1980-05-28 | TATE & LYLE PUBLIC LIMITED COMPANY | P.V.C. compositions for extrusion moulding |
| IE50028B1 (en) * | 1979-12-19 | 1986-02-05 | Tate & Lyle Plc | Process for the production of a surfactant containing sucrose esters |
| US4518772A (en) * | 1983-06-23 | 1985-05-21 | The Proctor & Gamble Company | Synthesis of higher polyol fatty acid polyesters using high soap:polyol ratios |
| US4517360A (en) * | 1983-06-23 | 1985-05-14 | The Procter & Gamble Company | Synthesis of higher polyol fatty acid polyesters using carbonate catalysts |
| JPS6115893A (ja) * | 1984-06-29 | 1986-01-23 | Dai Ichi Kogyo Seiyaku Co Ltd | シヨ糖脂肪酸エステルの精製法 |
| NL8601904A (nl) * | 1986-07-23 | 1988-02-16 | Unilever Nv | Werkwijze voor de bereiding van polyol-vetzuurpolyesters. |
| JPS63179884A (ja) * | 1987-01-17 | 1988-07-23 | Mitsubishi Kasei Corp | シヨ糖脂肪酸エステルの製造方法 |
| ATE143664T1 (de) * | 1989-12-21 | 1996-10-15 | Unilever Nv | Verfahren zur raffinierung von seife enthaltendem rohprodukt aus einem polyol-fettsäure- veresterungsgemisch |
| ES2095326T3 (es) | 1990-09-11 | 1997-02-16 | Procter & Gamble | Sintesis de poliesteres de poliol. |
| CA2111479C (en) * | 1991-04-12 | 1998-07-07 | Robert J. Sarama | Process for improving oxidative stability of polyol fatty acid polyesters |
| US5767257A (en) * | 1996-07-19 | 1998-06-16 | The Procter & Gamble Company | Methods for producing polyol fatty acid polyesters using atmospheric or superatmospheric pressure |
| US5945529A (en) * | 1996-07-19 | 1999-08-31 | The Procter & Gamble Company | Synthesis of polyol fatty acid polyesters using column with inert gas stripping |
| CA2263104C (en) * | 1996-08-08 | 2003-06-17 | Roger Stephen Berger | Polyol polyester synthesis |
| US6121440A (en) * | 1998-01-29 | 2000-09-19 | The Procter & Gamble Company | Process for synthesis of polyol fatty acid polyesters |
| AU4911300A (en) * | 1999-06-01 | 2000-12-18 | Astion Development Aps | A method of producing organic emulsifiers and organic surfactants, products produced by said method, and the use of such products |
| GB0608512D0 (en) | 2006-04-28 | 2006-06-07 | Vincent Processes Ltd | Process for the production of esters of sugars and sugar derivatives |
| EP3031443A1 (de) | 2014-12-12 | 2016-06-15 | Basf Se | Zusammensetzung enthaltend Kohlehydratpartialester |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1200276B (de) * | 1959-10-08 | 1965-09-09 | Bayer Ag | Verfahren zum Herstellen von Carbonsaeureestern nichtreduzierender Zucker |
| DE1643795A1 (de) * | 1967-08-04 | 1971-07-01 | Cassella Farbwerke Mainkur Ag | Verfahren zur Herstellung von Zuckerestern |
| US3597417A (en) * | 1968-07-23 | 1971-08-03 | Procter & Gamble | Process for the preparation of fatty acid esters of sugar glycosides |
| DE2004899C2 (de) * | 1969-02-05 | 1984-07-26 | Dai-Ichi Kogyo Seiyaku Co.,Ltd., Kyoto | Verfahren zur Abtrennung von Verunreinigungen aus Saccharosefettsäureester-Rohprodukten |
| US3714144A (en) * | 1969-05-29 | 1973-01-30 | Us Agriculture | Process for the production of sucrose esters of fatty acids |
| GB1399053A (en) * | 1973-03-16 | 1975-06-25 | Tate & Lyle Ltd | Process for the production of surface active agents comprising sucrose esters |
-
1974
- 1974-10-17 GB GB45122/74A patent/GB1499989A/en not_active Expired
-
1975
- 1975-04-18 TR TR18880A patent/TR18880A/xx unknown
- 1975-10-15 US US05/622,495 patent/US4032702A/en not_active Expired - Lifetime
- 1975-10-15 AR AR260811A patent/AR212161A1/es active
- 1975-10-16 SE SE7511612A patent/SE430339B/xx unknown
- 1975-10-16 DK DK465675AA patent/DK142148B/da not_active IP Right Cessation
- 1975-10-16 IT IT69587/75A patent/IT1048249B/it active
- 1975-10-16 NO NO753492A patent/NO140983C/no unknown
- 1975-10-17 DE DE2546716A patent/DE2546716C3/de not_active Expired
- 1975-10-17 CA CA237,872A patent/CA1045130A/en not_active Expired
- 1975-10-17 ZA ZA00756573A patent/ZA756573B/xx unknown
- 1975-10-17 CH CH1354075A patent/CH606074A5/xx not_active IP Right Cessation
- 1975-10-17 FR FR7531806A patent/FR2288143A2/fr active Granted
- 1975-10-17 NL NLAANVRAGE7512252,A patent/NL172761B/xx not_active IP Right Cessation
- 1975-10-17 AT AT793375A patent/AT347410B/de not_active IP Right Cessation
- 1975-10-17 JP JP50124459A patent/JPS5165704A/ja active Pending
- 1975-10-17 IE IE2270/75A patent/IE42171B1/en unknown
- 1975-10-17 BR BR7506830A patent/BR7506830A/pt unknown
- 1975-10-17 SU SU752184053A patent/SU906383A3/ru active
- 1975-10-17 ES ES441908A patent/ES441908A2/es not_active Expired
- 1975-11-12 CU CU34398A patent/CU34398A/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DK142148C (en, 2012) | 1981-02-02 |
| DK465675A (en, 2012) | 1976-04-18 |
| AR212161A1 (es) | 1978-05-31 |
| NO753492L (en, 2012) | 1976-04-21 |
| ATA793375A (de) | 1978-05-15 |
| IT1048249B (it) | 1980-11-20 |
| CU34398A (en, 2012) | 1977-06-08 |
| CH606074A5 (en, 2012) | 1978-10-13 |
| CA1045130A (en) | 1978-12-26 |
| IE42171L (en) | 1976-04-17 |
| TR18880A (tr) | 1977-10-13 |
| DE2546716C3 (de) | 1983-11-17 |
| US4032702A (en) | 1977-06-28 |
| FR2288143B2 (en, 2012) | 1979-02-02 |
| FR2288143A2 (fr) | 1976-05-14 |
| SE7511612L (sv) | 1976-04-20 |
| NL172761B (nl) | 1983-05-16 |
| JPS5165704A (en, 2012) | 1976-06-07 |
| AT347410B (de) | 1978-12-27 |
| NO140983C (no) | 1979-12-19 |
| AU8582875A (en) | 1977-04-21 |
| ZA756573B (en) | 1976-09-29 |
| IE42171B1 (en) | 1980-06-18 |
| BR7506830A (pt) | 1976-08-31 |
| NO140983B (no) | 1979-09-10 |
| SE430339B (sv) | 1983-11-07 |
| NL7512252A (nl) | 1976-04-21 |
| DE2546716A1 (de) | 1976-04-29 |
| ES441908A2 (es) | 1977-07-01 |
| GB1499989A (en) | 1978-02-01 |
| DK142148B (da) | 1980-09-08 |
| DE2546716B2 (de) | 1981-04-09 |
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