SU772469A3 - Способ приготовлени катализатора дл синтеза гидроксиламина - Google Patents
Способ приготовлени катализатора дл синтеза гидроксиламина Download PDFInfo
- Publication number
- SU772469A3 SU772469A3 SU762331207A SU2331207A SU772469A3 SU 772469 A3 SU772469 A3 SU 772469A3 SU 762331207 A SU762331207 A SU 762331207A SU 2331207 A SU2331207 A SU 2331207A SU 772469 A3 SU772469 A3 SU 772469A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- catalyst
- hydroxylamine
- activated carbon
- activity
- temperature
- Prior art date
Links
- 239000003054 catalyst Substances 0.000 title claims abstract description 54
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 title claims description 41
- 238000000034 method Methods 0.000 title claims description 15
- 230000015572 biosynthetic process Effects 0.000 title claims description 13
- 238000003786 synthesis reaction Methods 0.000 title claims description 13
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 77
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229910000510 noble metal Inorganic materials 0.000 claims abstract description 11
- 229910052763 palladium Inorganic materials 0.000 claims abstract description 9
- 239000011148 porous material Substances 0.000 claims abstract description 8
- 238000002360 preparation method Methods 0.000 claims abstract description 6
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 5
- 239000007788 liquid Substances 0.000 claims abstract description 5
- 150000003839 salts Chemical class 0.000 claims abstract description 5
- 230000007062 hydrolysis Effects 0.000 claims abstract description 4
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 4
- 230000000694 effects Effects 0.000 claims description 31
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims description 23
- 238000010438 heat treatment Methods 0.000 claims description 18
- 239000006185 dispersion Substances 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 10
- 239000012153 distilled water Substances 0.000 claims description 8
- 238000006722 reduction reaction Methods 0.000 claims description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 229910052697 platinum Inorganic materials 0.000 claims description 6
- 239000007791 liquid phase Substances 0.000 claims description 5
- PIBWKRNGBLPSSY-UHFFFAOYSA-L palladium(II) chloride Chemical compound Cl[Pd]Cl PIBWKRNGBLPSSY-UHFFFAOYSA-L 0.000 claims description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 4
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 239000003245 coal Substances 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- 239000011521 glass Substances 0.000 claims description 4
- -1 hydroxyl activated carbon Chemical compound 0.000 claims description 4
- 239000002609 medium Substances 0.000 claims description 4
- CLSUSRZJUQMOHH-UHFFFAOYSA-L platinum dichloride Chemical compound Cl[Pt]Cl CLSUSRZJUQMOHH-UHFFFAOYSA-L 0.000 claims description 4
- 239000000243 solution Substances 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
- 229910002651 NO3 Inorganic materials 0.000 claims description 2
- 239000012062 aqueous buffer Substances 0.000 claims description 2
- 239000012736 aqueous medium Substances 0.000 claims description 2
- 230000000737 periodic effect Effects 0.000 claims description 2
- YSVZGWAJIHWNQK-UHFFFAOYSA-N [3-(hydroxymethyl)-2-bicyclo[2.2.1]heptanyl]methanol Chemical compound C1CC2C(CO)C(CO)C1C2 YSVZGWAJIHWNQK-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract description 6
- 229910052751 metal Inorganic materials 0.000 abstract 3
- 239000002184 metal Substances 0.000 abstract 3
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 abstract 2
- 230000003301 hydrolyzing effect Effects 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 2
- 239000003638 chemical reducing agent Substances 0.000 abstract 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 abstract 1
- 235000017557 sodium bicarbonate Nutrition 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- VNWKTOKETHGBQD-AKLPVKDBSA-N carbane Chemical class [15CH4] VNWKTOKETHGBQD-AKLPVKDBSA-N 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G35/00—Reforming naphtha
- C10G35/04—Catalytic reforming
- C10G35/06—Catalytic reforming characterised by the catalyst used
- C10G35/085—Catalytic reforming characterised by the catalyst used containing platinum group metals or compounds thereof
- C10G35/09—Bimetallic catalysts in which at least one of the metals is a platinum group metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1418—Preparation by catalytic reduction of nitrogen oxides or nitrates with hydrogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL7502968A NL7502968A (nl) | 1975-03-13 | 1975-03-13 | Werkwijze voor het bereiden van edelmetaal- katalysatoren. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU772469A3 true SU772469A3 (ru) | 1980-10-15 |
Family
ID=19823356
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU762331207A SU772469A3 (ru) | 1975-03-13 | 1976-03-11 | Способ приготовлени катализатора дл синтеза гидроксиламина |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4052336A (enExample) |
| JP (1) | JPS51115294A (enExample) |
| BE (1) | BE839524A (enExample) |
| CA (1) | CA1071617A (enExample) |
| DE (1) | DE2610486A1 (enExample) |
| FR (1) | FR2303598A1 (enExample) |
| GB (1) | GB1531595A (enExample) |
| IT (1) | IT1078732B (enExample) |
| NL (1) | NL7502968A (enExample) |
| SU (1) | SU772469A3 (enExample) |
Families Citing this family (31)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL8104025A (nl) * | 1981-08-29 | 1983-03-16 | Stamicarbon | Werkwijze voor de bereiding van ethercarboxylaten. |
| US4415479A (en) * | 1981-10-29 | 1983-11-15 | Standard Oil Company (Indiana) | Palladium on carbon catalyst for purification of crude terephthalic acid |
| US4394299A (en) * | 1981-10-29 | 1983-07-19 | Standard Oil Company (Indiana) | Palladium-rhodium catalyst for purification of crude terephthalic acid |
| IT1156324B (it) * | 1982-09-10 | 1987-02-04 | Montepolimeri Spa | Metodo per la preparazione di catalizzatori supportati e catalizzatori supportati cosi' ottenuti |
| DE4022851A1 (de) * | 1990-07-18 | 1992-01-23 | Basf Ag | Platin-graphittraeger-katalysatoren und deren verwendung |
| DE4022853A1 (de) * | 1990-07-18 | 1992-01-23 | Basf Ag | Platin-graphittraeger-katalysatoren und deren verwendung |
| IT1256800B (it) * | 1992-01-31 | 1995-12-15 | Novamont Spa | Procedimento per la produzione di polioli inferiori e nuovo catalizzatore a base di rutenio utilizzato in tale procedimento. |
| NL9201176A (nl) * | 1992-07-02 | 1994-02-01 | Dsm Nv | Werkwijze voor het bereiden en zuiveren van een hydroxylammoniumzoutoplossing. |
| TW322432B (enExample) * | 1993-06-14 | 1997-12-11 | Degussa | |
| US6103393A (en) * | 1998-02-24 | 2000-08-15 | Superior Micropowders Llc | Metal-carbon composite powders, methods for producing powders and devices fabricated from same |
| US6660680B1 (en) | 1997-02-24 | 2003-12-09 | Superior Micropowders, Llc | Electrocatalyst powders, methods for producing powders and devices fabricated from same |
| US6780350B1 (en) | 1997-02-24 | 2004-08-24 | Superior Micropowders Llc | Metal-carbon composite powders, methods for producing powders and devices fabricated from same |
| US6338809B1 (en) * | 1997-02-24 | 2002-01-15 | Superior Micropowders Llc | Aerosol method and apparatus, particulate products, and electronic devices made therefrom |
| US6967183B2 (en) | 1998-08-27 | 2005-11-22 | Cabot Corporation | Electrocatalyst powders, methods for producing powders and devices fabricated from same |
| US7094370B2 (en) * | 1998-02-24 | 2006-08-22 | Cabot Corporation | Method for the production of metal-carbon composite powders |
| US6753108B1 (en) | 1998-02-24 | 2004-06-22 | Superior Micropowders, Llc | Energy devices and methods for the fabrication of energy devices |
| US7138354B2 (en) * | 1998-02-24 | 2006-11-21 | Cabot Corporation | Method for the fabrication of an electrocatalyst layer |
| US7659225B2 (en) * | 2001-09-17 | 2010-02-09 | Basf Catalysts Llc | Precious metal catalyst for debenzylation |
| US6992037B2 (en) * | 2001-09-17 | 2006-01-31 | Engelhard Corporation | Precious metal catalyst for debenzylation |
| US6706658B2 (en) * | 2001-12-21 | 2004-03-16 | Engelhard Corporation | Catalyst for purification of aromatic acids |
| JP5138584B2 (ja) * | 2006-03-31 | 2013-02-06 | トヨタ自動車株式会社 | 燃料電池用電極触媒の製造方法 |
| US20070298961A1 (en) * | 2006-06-22 | 2007-12-27 | Rice Gordon L | Method of producing electrodes |
| US7696122B2 (en) * | 2006-07-05 | 2010-04-13 | Cabot Corporation | Electrocatalyst inks for fuel cell applications |
| JP5157216B2 (ja) * | 2007-03-29 | 2013-03-06 | Ｔｄｋ株式会社 | 活物質の製造方法及び活物質 |
| JP5211527B2 (ja) * | 2007-03-29 | 2013-06-12 | Ｔｄｋ株式会社 | 全固体リチウムイオン二次電池及びその製造方法 |
| JP5211526B2 (ja) | 2007-03-29 | 2013-06-12 | Ｔｄｋ株式会社 | 全固体リチウムイオン二次電池及びその製造方法 |
| EP2181177A4 (en) * | 2007-08-01 | 2012-10-10 | Nagarjuna Energy Private Ltd | PROCESS FOR PREVENTING THE POLYMERIZATION OF VOLATILE CRYSTALLING PRODUCTS DURING PYROLYSIS AND GASIFICATION |
| WO2011162339A1 (ja) | 2010-06-23 | 2011-12-29 | 旭硝子株式会社 | ２，３，３，３－テトラフルオロプロペンの製造方法 |
| US9018127B2 (en) * | 2012-01-12 | 2015-04-28 | Bioamber International S.A.R.L. | Preparation of catalyst for selective hydrogenation of hydrogenatable precursors |
| CN112661126B (zh) * | 2021-01-05 | 2022-03-11 | 浙江锦华新材料股份有限公司 | 一种固体盐酸羟胺的制备方法 |
| CN113058590B (zh) * | 2021-03-16 | 2022-10-11 | 河北广祥制药有限公司 | 一种湿基碳载纳米贵金属催化剂的制备方法与应用 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3138560A (en) * | 1959-12-17 | 1964-06-23 | Engelhard Ind Inc | Process for producing palladium on carbon catalysts |
| DE1667045A1 (de) * | 1967-05-13 | 1971-06-03 | Bayer Ag | Verfahren zur Herstellung eines besonders fuer die NO-Hydrierung zu Hydroxylamin geeigneten Platinkatalysators |
| US3736266A (en) * | 1971-08-18 | 1973-05-29 | Dart Ind Inc | Preparation of carbon supported palladium catalysts |
| SE392045B (sv) * | 1972-08-17 | 1977-03-14 | Hoechst Ag | Sett att framstella en av finkornigt berarmaterial och palladium bestaende katalysator |
| US3804779A (en) * | 1972-10-02 | 1974-04-16 | Dart Ind Inc | Carbon supported palladium catalyst |
-
1975
- 1975-03-13 NL NL7502968A patent/NL7502968A/xx not_active Application Discontinuation
-
1976
- 1976-03-09 US US05/665,442 patent/US4052336A/en not_active Expired - Lifetime
- 1976-03-09 CA CA247,496A patent/CA1071617A/en not_active Expired
- 1976-03-11 GB GB9836/76A patent/GB1531595A/en not_active Expired
- 1976-03-11 SU SU762331207A patent/SU772469A3/ru active
- 1976-03-12 IT IT48560/76A patent/IT1078732B/it active
- 1976-03-12 DE DE19762610486 patent/DE2610486A1/de not_active Withdrawn
- 1976-03-12 JP JP51027014A patent/JPS51115294A/ja active Granted
- 1976-03-12 FR FR7607179A patent/FR2303598A1/fr active Granted
- 1976-03-12 BE BE165129A patent/BE839524A/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| NL7502968A (nl) | 1976-09-15 |
| US4052336A (en) | 1977-10-04 |
| BE839524A (nl) | 1976-09-13 |
| JPS5323274B2 (enExample) | 1978-07-13 |
| JPS51115294A (en) | 1976-10-09 |
| FR2303598B1 (enExample) | 1981-12-24 |
| DE2610486A1 (de) | 1976-09-30 |
| FR2303598A1 (fr) | 1976-10-08 |
| CA1071617A (en) | 1980-02-12 |
| IT1078732B (it) | 1985-05-08 |
| GB1531595A (en) | 1978-11-08 |
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