SU495829A3 - Способ получени производных фенилгидразона - Google Patents
Способ получени производных фенилгидразонаInfo
- Publication number
- SU495829A3 SU495829A3 SU1919779A SU1919779A SU495829A3 SU 495829 A3 SU495829 A3 SU 495829A3 SU 1919779 A SU1919779 A SU 1919779A SU 1919779 A SU1919779 A SU 1919779A SU 495829 A3 SU495829 A3 SU 495829A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- carbon atoms
- phenylhydrazone
- dichloro
- substituents
- alkyl
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 3
- 125000004432 carbon atom Chemical group C* 0.000 claims 5
- 125000003545 alkoxy group Chemical group 0.000 claims 2
- 125000000217 alkyl group Chemical group 0.000 claims 2
- 125000001424 substituent group Chemical group 0.000 claims 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 1
- 101100490437 Mus musculus Acvrl1 gene Proteins 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 229910052801 chlorine Inorganic materials 0.000 claims 1
- 239000000460 chlorine Substances 0.000 claims 1
- 125000005843 halogen group Chemical group 0.000 claims 1
- 238000002955 isolation Methods 0.000 claims 1
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 8
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- 239000011574 phosphorus Substances 0.000 description 3
- 229910052698 phosphorus Inorganic materials 0.000 description 3
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- -1 phosphorus compound Chemical class 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 description 2
- DGMOBVGABMBZSB-UHFFFAOYSA-N 2-methylpropanoyl chloride Chemical compound CC(C)C(Cl)=O DGMOBVGABMBZSB-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000002828 nitro derivatives Chemical class 0.000 description 1
- LQNUZADURLCDLV-UHFFFAOYSA-N nitrobenzene Substances [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229940067157 phenylhydrazine Drugs 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- LJZPPWWHKPGCHS-UHFFFAOYSA-N propargyl chloride Chemical compound ClCC#C LJZPPWWHKPGCHS-UHFFFAOYSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 235000010288 sodium nitrite Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- HPGGPRDJHPYFRM-UHFFFAOYSA-J tin(iv) chloride Chemical compound Cl[Sn](Cl)(Cl)Cl HPGGPRDJHPYFRM-UHFFFAOYSA-J 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/72—Hydrazones
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7218895A FR2186024A5 (en) | 1972-05-26 | 1972-05-26 | Phenylhydrazone derivs - prepd by chlorination of phenylhydrazides |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU495829A3 true SU495829A3 (ru) | 1975-12-15 |
Family
ID=9099161
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1919779A SU495829A3 (ru) | 1972-05-26 | 1973-05-25 | Способ получени производных фенилгидразона |
| SU751919780D SU578821A3 (ru) | 1972-05-26 | 1973-05-25 | Инсектицидное и акарицидное средство |
| SU1919780A SU496725A3 (ru) | 1972-05-26 | 1973-05-25 | Способ получени производных фенилгидразона |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU751919780D SU578821A3 (ru) | 1972-05-26 | 1973-05-25 | Инсектицидное и акарицидное средство |
| SU1919780A SU496725A3 (ru) | 1972-05-26 | 1973-05-25 | Способ получени производных фенилгидразона |
Country Status (8)
| Country | Link |
|---|---|
| AT (3) | AT324301B (OSRAM) |
| BE (2) | BE800089A (OSRAM) |
| BR (1) | BR7303797D0 (OSRAM) |
| ES (2) | ES415234A1 (OSRAM) |
| FR (1) | FR2186024A5 (OSRAM) |
| HU (1) | HU166620B (OSRAM) |
| SU (3) | SU495829A3 (OSRAM) |
| ZA (2) | ZA733526B (OSRAM) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MY131441A (en) * | 1992-12-29 | 2007-08-30 | American Cyanamid Co | Amidrazones and their use as insecticidal and acaricidal agents |
-
1972
- 1972-05-26 FR FR7218895A patent/FR2186024A5/fr not_active Expired
-
1973
- 1973-05-23 BR BR003797/73A patent/BR7303797D0/pt unknown
- 1973-05-24 HU HURO731A patent/HU166620B/hu unknown
- 1973-05-24 ZA ZA733526A patent/ZA733526B/xx unknown
- 1973-05-24 ZA ZA733527A patent/ZA733527B/xx unknown
- 1973-05-25 AT AT460573A patent/AT324301B/de not_active IP Right Cessation
- 1973-05-25 BE BE131572A patent/BE800089A/xx unknown
- 1973-05-25 AT AT460473A patent/AT324300B/de not_active IP Right Cessation
- 1973-05-25 SU SU1919779A patent/SU495829A3/ru active
- 1973-05-25 SU SU751919780D patent/SU578821A3/ru active
- 1973-05-25 BE BE131571A patent/BE800088A/xx unknown
- 1973-05-25 SU SU1919780A patent/SU496725A3/ru active
- 1973-05-25 AT AT739474A patent/AT325020B/de not_active IP Right Cessation
- 1973-05-26 ES ES415234A patent/ES415234A1/es not_active Expired
- 1973-05-26 ES ES415235A patent/ES415235A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| BR7303797D0 (pt) | 1973-12-20 |
| AT324301B (de) | 1975-08-25 |
| SU496725A3 (ru) | 1975-12-25 |
| HU166620B (OSRAM) | 1975-04-28 |
| ES415235A1 (es) | 1976-02-01 |
| ZA733526B (en) | 1974-04-24 |
| FR2186024A5 (en) | 1974-01-04 |
| ZA733527B (en) | 1974-04-24 |
| AT324300B (de) | 1975-08-25 |
| BE800089A (fr) | 1973-11-26 |
| ES415234A1 (es) | 1976-02-01 |
| AT325020B (de) | 1975-09-25 |
| BE800088A (fr) | 1973-11-26 |
| SU578821A3 (ru) | 1977-10-30 |
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