SU433682A3 - Способ получшия эшроамидов тиофосфорной кислоты - Google Patents
Способ получшия эшроамидов тиофосфорной кислотыInfo
- Publication number
- SU433682A3 SU433682A3 SU1691583A SU1691583A SU433682A3 SU 433682 A3 SU433682 A3 SU 433682A3 SU 1691583 A SU1691583 A SU 1691583A SU 1691583 A SU1691583 A SU 1691583A SU 433682 A3 SU433682 A3 SU 433682A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- acid
- obtaining
- thyophosphoric
- echroamides
- methyl
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 12
- 239000002253 acid Substances 0.000 title description 5
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 15
- 229910052739 hydrogen Inorganic materials 0.000 description 7
- 239000001257 hydrogen Substances 0.000 description 7
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 125000000217 alkyl group Chemical group 0.000 description 4
- 239000000741 silica gel Substances 0.000 description 4
- 229910002027 silica gel Inorganic materials 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 229910052736 halogen Inorganic materials 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 239000011541 reaction mixture Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- RYYWUUFWQRZTIU-UHFFFAOYSA-N Thiophosphoric acid Chemical compound OP(O)(S)=O RYYWUUFWQRZTIU-UHFFFAOYSA-N 0.000 description 2
- 150000002431 hydrogen Chemical class 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 159000000000 sodium salts Chemical class 0.000 description 2
- 150000003580 thiophosphoric acid esters Chemical class 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- NQCPECCCWDWTJJ-UHFFFAOYSA-N 2-diethylamino-6-methylpyrimidin-4(1H)-one Chemical compound CCN(CC)C1=NC(=O)C=C(C)N1 NQCPECCCWDWTJJ-UHFFFAOYSA-N 0.000 description 1
- WDYVUKGVKRZQNM-UHFFFAOYSA-N 6-phosphonohexylphosphonic acid Chemical compound OP(O)(=O)CCCCCCP(O)(O)=O WDYVUKGVKRZQNM-UHFFFAOYSA-N 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 230000000895 acaricidal effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- -1 halogen hydride Chemical class 0.000 description 1
- 150000002367 halogens Chemical group 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000011814 protection agent Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000004809 thin layer chromatography Methods 0.000 description 1
- 150000003581 thiophosphoric acid halides Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/645—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having two nitrogen atoms as the only ring hetero atoms
- C07F9/6509—Six-membered rings
- C07F9/6512—Six-membered rings having the nitrogen atoms in positions 1 and 3
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH1189370A CH535264A (de) | 1970-08-07 | 1970-08-07 | Verfahren zur Herstellung neuer Phosphorsäureamidester |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU433682A3 true SU433682A3 (ru) | 1974-06-25 |
Family
ID=4377905
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1691583A SU433682A3 (ru) | 1970-08-07 | 1971-08-05 | Способ получшия эшроамидов тиофосфорной кислоты |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US3808333A (en:Method) |
| AU (1) | AU3210271A (en:Method) |
| BR (1) | BR7105055D0 (en:Method) |
| CH (1) | CH535264A (en:Method) |
| DD (1) | DD102065A5 (en:Method) |
| DE (1) | DE2139246A1 (en:Method) |
| ES (1) | ES393943A1 (en:Method) |
| FR (1) | FR2104014A5 (en:Method) |
| GB (1) | GB1350133A (en:Method) |
| IL (1) | IL37458A (en:Method) |
| IT (1) | IT945925B (en:Method) |
| RO (1) | RO62391A (en:Method) |
| SU (1) | SU433682A3 (en:Method) |
| ZA (1) | ZA715247B (en:Method) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4048172A (en) * | 1973-03-29 | 1977-09-13 | Imperial Chemical Industries Limited | Carbonylmethylpyrimidin-6-yl phosphates and phosphorothionates |
| GB1418784A (en) * | 1973-03-29 | 1975-12-24 | Ici Ltd | Phosphorus containing pyrimidine compounds and pesticidal compositions comprising them |
| DE2352995A1 (de) * | 1973-10-23 | 1975-04-30 | Bayer Ag | O-pyrazolopyrimidin-thiono-phosphorsaeureesteramide, verfahren zu ihrer herstellung sowie ihre verwendung als insektizide und akarizide |
| US4489068A (en) * | 1983-04-28 | 1984-12-18 | The Dow Chemical Company | Method and composition for enhancing the insecticidal activity of certain organophosphorus compounds |
-
1970
- 1970-08-07 CH CH1189370A patent/CH535264A/de not_active IP Right Cessation
-
1971
- 1971-07-27 GB GB3509171A patent/GB1350133A/en not_active Expired
- 1971-08-03 US US00168764A patent/US3808333A/en not_active Expired - Lifetime
- 1971-08-05 ES ES393943A patent/ES393943A1/es not_active Expired
- 1971-08-05 DE DE19712139246 patent/DE2139246A1/de active Pending
- 1971-08-05 IL IL37458A patent/IL37458A/xx unknown
- 1971-08-05 FR FR7128762A patent/FR2104014A5/fr not_active Expired
- 1971-08-05 SU SU1691583A patent/SU433682A3/ru active
- 1971-08-05 DD DD156959A patent/DD102065A5/xx unknown
- 1971-08-05 IT IT27223/71A patent/IT945925B/it active
- 1971-08-06 BR BR5055/71A patent/BR7105055D0/pt unknown
- 1971-08-06 RO RO7100067922A patent/RO62391A/ro unknown
- 1971-08-06 ZA ZA715247A patent/ZA715247B/xx unknown
- 1971-08-06 AU AU32102/71A patent/AU3210271A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US3808333A (en) | 1974-04-30 |
| BR7105055D0 (pt) | 1973-04-17 |
| ES393943A1 (es) | 1974-07-01 |
| IL37458A0 (en) | 1971-11-29 |
| DD102065A5 (en:Method) | 1973-12-05 |
| IT945925B (it) | 1973-05-10 |
| CH535264A (de) | 1973-03-31 |
| FR2104014A5 (en:Method) | 1972-04-14 |
| RO62391A (fr) | 1978-02-15 |
| AU3210271A (en) | 1973-02-08 |
| IL37458A (en) | 1974-07-31 |
| GB1350133A (en) | 1974-04-18 |
| ZA715247B (en) | 1973-03-28 |
| DE2139246A1 (de) | 1972-02-17 |
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