RU94042231A - Усовершенствованный способ производства циклопропилнитрила - Google Patents
Усовершенствованный способ производства циклопропилнитрилаInfo
- Publication number
- RU94042231A RU94042231A RU94042231/04A RU94042231A RU94042231A RU 94042231 A RU94042231 A RU 94042231A RU 94042231/04 A RU94042231/04 A RU 94042231/04A RU 94042231 A RU94042231 A RU 94042231A RU 94042231 A RU94042231 A RU 94042231A
- Authority
- RU
- Russia
- Prior art keywords
- cyclopropyl nitrile
- production
- improved process
- cyclopropyl
- nitrile
- Prior art date
Links
- AUQDITHEDVOTCU-UHFFFAOYSA-N cyclopropyl cyanide Chemical compound N#CC1CC1 AUQDITHEDVOTCU-UHFFFAOYSA-N 0.000 title claims abstract 5
- 238000004519 manufacturing process Methods 0.000 title claims 3
- 238000000034 method Methods 0.000 title abstract 2
- 229910052783 alkali metal Inorganic materials 0.000 claims abstract 2
- 150000001340 alkali metals Chemical class 0.000 claims abstract 2
- 238000010533 azeotropic distillation Methods 0.000 claims abstract 2
- 239000002585 base Substances 0.000 claims abstract 2
- 230000003197 catalytic effect Effects 0.000 claims abstract 2
- 239000007795 chemical reaction product Substances 0.000 claims abstract 2
- 229910017053 inorganic salt Inorganic materials 0.000 claims abstract 2
- 239000002798 polar solvent Substances 0.000 claims abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract 2
- 238000002955 isolation Methods 0.000 claims 1
- 239000000126 substance Substances 0.000 abstract 2
- 230000000694 effects Effects 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
- C07C255/45—Carboxylic acid nitriles having cyano groups bound to carbon atoms of rings other than six-membered aromatic rings
- C07C255/46—Carboxylic acid nitriles having cyano groups bound to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of non-condensed rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
- C07C255/45—Carboxylic acid nitriles having cyano groups bound to carbon atoms of rings other than six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/02—Systems containing only non-condensed rings with a three-membered ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Данное изобретение предлагает усовершенствованный производственный способ получения и выделения циклопропилнитрила. 4-Галобутиронитрил реагирует с основанием щелочного металла в присутствии апротонного полярного растворителя, неорганической соли и каталитического количества воды при повышенной температуре. Реакционный продукт циклопропилнитрил выделяют путем азеотропной перегонки.
Claims (1)
- Данное изобретение предлагает усовершенствованный производственный способ получения и выделения циклопропилнитрила. 4-Галобутиронитрил реагирует с основанием щелочного металла в присутствии апротонного полярного растворителя, неорганической соли и каталитического количества воды при повышенной температуре. Реакционный продукт циклопропилнитрил выделяют путем азеотропной перегонки.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/161.111 | 1993-12-02 | ||
US08/161,111 US5380911A (en) | 1993-12-02 | 1993-12-02 | Process for the manufacture of cyclopropylnitrile |
US08/161,111 | 1993-12-02 |
Publications (2)
Publication Number | Publication Date |
---|---|
RU94042231A true RU94042231A (ru) | 1996-10-10 |
RU2124001C1 RU2124001C1 (ru) | 1998-12-27 |
Family
ID=22579866
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
RU94042231A RU2124001C1 (ru) | 1993-12-02 | 1994-12-01 | Способ получение циклопропилнитрила |
Country Status (24)
Country | Link |
---|---|
US (1) | US5380911A (ru) |
EP (1) | EP0656347B1 (ru) |
JP (1) | JP3615582B2 (ru) |
KR (1) | KR100362481B1 (ru) |
CN (1) | CN1038411C (ru) |
AT (1) | ATE148691T1 (ru) |
AU (1) | AU675365B2 (ru) |
BR (1) | BR9404804A (ru) |
CA (1) | CA2137031C (ru) |
CZ (1) | CZ289825B6 (ru) |
DE (1) | DE69401701T2 (ru) |
DK (1) | DK0656347T3 (ru) |
ES (1) | ES2097602T3 (ru) |
GR (1) | GR3022497T3 (ru) |
HK (1) | HK1001052A1 (ru) |
HU (1) | HU213376B (ru) |
IL (1) | IL111828A (ru) |
PH (1) | PH31598A (ru) |
RU (1) | RU2124001C1 (ru) |
SG (1) | SG47602A1 (ru) |
SK (1) | SK279899B6 (ru) |
TW (1) | TW381074B (ru) |
UA (1) | UA27906C2 (ru) |
ZA (1) | ZA949582B (ru) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5502234A (en) * | 1995-07-17 | 1996-03-26 | Eastman Chemical Company | Process for the preparation and separation of cyclopropanecarbonitrile |
EP1243578A1 (en) | 2001-02-23 | 2002-09-25 | Kuraray Co., Ltd. | Process for producing cyclopropanecarbonitrile |
CZ2008352A3 (cs) * | 2008-06-09 | 2009-09-09 | Lucební závody Draslovka a. s. Kolín | Zpusob výroby cykloalkankarbonitrilu |
CN101993393B (zh) * | 2009-08-26 | 2013-11-27 | 浙江华海药业股份有限公司 | 一种人工合成环丙基腈的方法 |
CN102489323B (zh) * | 2011-11-23 | 2013-04-10 | 北京化工大学 | 基于光催化分解水制备氢气的水滑石光催化剂及其制备方法 |
CN106242997B (zh) * | 2016-07-29 | 2018-12-11 | 西安近代化学研究所 | 一种环丙腈的合成方法 |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3847985A (en) * | 1970-08-28 | 1974-11-12 | Exxon Research Engineering Co | Process for the preparation of cyclopropylmethyl alkyl amines |
US3853942A (en) * | 1973-09-13 | 1974-12-10 | Ciba Geigy Corp | Process for the manufacture of cyclopropa-necarbonitrile |
US3843709A (en) * | 1973-10-15 | 1974-10-22 | Gulf Research Development Co | Preparation of cyclopropyl cyanide from 4-hlorobutyronitrile |
US3974199A (en) * | 1975-06-16 | 1976-08-10 | The Dow Chemical Company | Process for production of cyclopropylcyanide |
CH624662A5 (en) * | 1976-03-01 | 1981-08-14 | Ciba Geigy Ag | Process for the preparation of cyclopropanecarbonitrile |
CH624663A5 (en) * | 1976-03-02 | 1981-08-14 | Ciba Geigy Ag | Process for the preparation of cyclopropanecarbonitrile |
US4205009A (en) * | 1979-02-07 | 1980-05-27 | Velsicol Chemical Corporation | Process for the preparation of cyclopropylcyanide |
US4974199A (en) * | 1984-06-28 | 1990-11-27 | Westinghouse Electric Corp. | Digital IC-microcomputer interface |
US4622065A (en) * | 1984-11-01 | 1986-11-11 | Ppg Industries, Inc. | Sulfamoyl urea derivatives |
US5107023A (en) * | 1990-06-22 | 1992-04-21 | American Cyanamid Company | 0-Aminophenyl cyclopropyl ketone intermediate |
US5009699A (en) * | 1990-06-22 | 1991-04-23 | American Cyanamid Company | 1-{[O-(cyclopropylcarbonyl)phenyl]sulfamoyl}-3-(4,6-dimethoxy-2-pyrimidinyl)urea herbicidal composition and use |
-
1993
- 1993-12-02 US US08/161,111 patent/US5380911A/en not_active Expired - Lifetime
-
1994
- 1994-09-26 TW TW083108908A patent/TW381074B/zh not_active IP Right Cessation
- 1994-11-09 EP EP94117654A patent/EP0656347B1/en not_active Expired - Lifetime
- 1994-11-09 DE DE69401701T patent/DE69401701T2/de not_active Expired - Lifetime
- 1994-11-09 AT AT94117654T patent/ATE148691T1/de active
- 1994-11-09 ES ES94117654T patent/ES2097602T3/es not_active Expired - Lifetime
- 1994-11-09 SG SG1996003063A patent/SG47602A1/en unknown
- 1994-11-09 DK DK94117654.7T patent/DK0656347T3/da active
- 1994-11-23 CZ CZ19942885A patent/CZ289825B6/cs not_active IP Right Cessation
- 1994-11-28 CN CN94117826A patent/CN1038411C/zh not_active Expired - Fee Related
- 1994-11-28 JP JP31759294A patent/JP3615582B2/ja not_active Expired - Fee Related
- 1994-11-30 IL IL111828A patent/IL111828A/xx not_active IP Right Cessation
- 1994-11-30 CA CA002137031A patent/CA2137031C/en not_active Expired - Lifetime
- 1994-11-30 SK SK1466-94A patent/SK279899B6/sk not_active IP Right Cessation
- 1994-12-01 PH PH49476A patent/PH31598A/en unknown
- 1994-12-01 UA UA94129107A patent/UA27906C2/uk unknown
- 1994-12-01 ZA ZA949582A patent/ZA949582B/xx unknown
- 1994-12-01 KR KR1019940032459A patent/KR100362481B1/ko not_active IP Right Cessation
- 1994-12-01 AU AU79171/94A patent/AU675365B2/en not_active Ceased
- 1994-12-01 HU HU9403453A patent/HU213376B/hu not_active IP Right Cessation
- 1994-12-01 RU RU94042231A patent/RU2124001C1/ru not_active IP Right Cessation
- 1994-12-01 BR BR9404804A patent/BR9404804A/pt not_active IP Right Cessation
-
1997
- 1997-02-06 GR GR960402149T patent/GR3022497T3/el unknown
-
1998
- 1998-01-05 HK HK98100070A patent/HK1001052A1/xx unknown
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
MM4A | The patent is invalid due to non-payment of fees |
Effective date: 20131202 |