RU2012105465A - Гидроксифенилфосфиноксидные смеси и их применение в качестве замедлителей горения для эпоксидных смол - Google Patents
Гидроксифенилфосфиноксидные смеси и их применение в качестве замедлителей горения для эпоксидных смол Download PDFInfo
- Publication number
- RU2012105465A RU2012105465A RU2012105465/05A RU2012105465A RU2012105465A RU 2012105465 A RU2012105465 A RU 2012105465A RU 2012105465/05 A RU2012105465/05 A RU 2012105465/05A RU 2012105465 A RU2012105465 A RU 2012105465A RU 2012105465 A RU2012105465 A RU 2012105465A
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- RU
- Russia
- Prior art keywords
- mixture
- atom
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- respect
- Prior art date
Links
- 239000000203 mixture Substances 0.000 title claims abstract 43
- 239000003822 epoxy resin Substances 0.000 title claims 4
- 229920000647 polyepoxide Polymers 0.000 title claims 4
- 238000002485 combustion reaction Methods 0.000 title 1
- MLCHBQKMVKNBOV-UHFFFAOYSA-N phenylphosphinic acid Chemical compound OP(=O)C1=CC=CC=C1 MLCHBQKMVKNBOV-UHFFFAOYSA-N 0.000 title 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims abstract 15
- 125000004437 phosphorous atom Chemical group 0.000 claims abstract 15
- 125000004464 hydroxyphenyl group Chemical group 0.000 claims abstract 11
- 125000005036 alkoxyphenyl group Chemical group 0.000 claims abstract 9
- MPQXHAGKBWFSNV-UHFFFAOYSA-N oxidophosphanium Chemical class [PH3]=O MPQXHAGKBWFSNV-UHFFFAOYSA-N 0.000 claims abstract 9
- 125000004432 carbon atom Chemical group C* 0.000 claims abstract 6
- 125000000217 alkyl group Chemical group 0.000 claims abstract 5
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract 4
- 239000001257 hydrogen Substances 0.000 claims abstract 4
- FIQMHBFVRAXMOP-UHFFFAOYSA-N triphenylphosphane oxide Chemical class C=1C=CC=CC=1P(C=1C=CC=CC=1)(=O)C1=CC=CC=C1 FIQMHBFVRAXMOP-UHFFFAOYSA-N 0.000 claims abstract 4
- 239000007983 Tris buffer Substances 0.000 claims abstract 3
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims abstract 3
- 238000000034 method Methods 0.000 claims 5
- UHOVQNZJYSORNB-UHFFFAOYSA-N monobenzene Natural products C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims 4
- -1 benzene halide Chemical class 0.000 claims 3
- 239000000047 product Substances 0.000 claims 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims 2
- 229910001508 alkali metal halide Inorganic materials 0.000 claims 2
- 150000008045 alkali metal halides Chemical class 0.000 claims 2
- 150000005224 alkoxybenzenes Chemical class 0.000 claims 2
- 150000001350 alkyl halides Chemical class 0.000 claims 2
- QARVLSVVCXYDNA-UHFFFAOYSA-N bromobenzene Chemical compound BrC1=CC=CC=C1 QARVLSVVCXYDNA-UHFFFAOYSA-N 0.000 claims 2
- GZUXJHMPEANEGY-UHFFFAOYSA-N bromomethane Chemical compound BrC GZUXJHMPEANEGY-UHFFFAOYSA-N 0.000 claims 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 claims 2
- 239000007800 oxidant agent Substances 0.000 claims 2
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 claims 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 150000001340 alkali metals Chemical class 0.000 claims 1
- 239000002585 base Substances 0.000 claims 1
- 239000007795 chemical reaction product Substances 0.000 claims 1
- 239000003431 cross linking reagent Substances 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L magnesium chloride Substances [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims 1
- 229940102396 methyl bromide Drugs 0.000 claims 1
- CGNKSELPNJJTSM-UHFFFAOYSA-N phenylphosphonous acid Chemical compound OP(O)C1=CC=CC=C1 CGNKSELPNJJTSM-UHFFFAOYSA-N 0.000 claims 1
- SNXNZPAIYHZIHA-UHFFFAOYSA-N O=P(C1C=CCCC1)(C1=C=CCCC1)C1=CCCC=C1 Chemical compound O=P(C1C=CCCC1)(C1=C=CCCC1)C1=CCCC=C1 SNXNZPAIYHZIHA-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/49—Phosphorus-containing compounds
- C08K5/51—Phosphorus bound to oxygen
- C08K5/53—Phosphorus bound to oxygen bound to oxygen and to carbon only
- C08K5/5397—Phosphine oxides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/02—Polycondensates containing more than one epoxy group per molecule
- C08G59/04—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof
- C08G59/06—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K21/00—Fireproofing materials
- C09K21/06—Organic materials
- C09K21/12—Organic materials containing phosphorus
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/249921—Web or sheet containing structurally defined element or component
- Y10T428/249924—Noninterengaged fiber-containing paper-free web or sheet which is not of specified porosity
- Y10T428/24994—Fiber embedded in or on the surface of a polymeric matrix
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Fireproofing Substances (AREA)
- Epoxy Resins (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US24156209P | 2009-09-11 | 2009-09-11 | |
| US61/241,562 | 2009-09-11 | ||
| PCT/US2010/048235 WO2011031834A1 (en) | 2009-09-11 | 2010-09-09 | Hydroxyphenyl phosphine oxide mixtures and their use as flame retardants for epoxy resins |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RU2012105465A true RU2012105465A (ru) | 2013-08-27 |
Family
ID=42988502
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2012105465/05A RU2012105465A (ru) | 2009-09-11 | 2010-09-09 | Гидроксифенилфосфиноксидные смеси и их применение в качестве замедлителей горения для эпоксидных смол |
Country Status (12)
| Country | Link |
|---|---|
| US (2) | US20110065838A1 (https=) |
| EP (1) | EP2475716B1 (https=) |
| JP (1) | JP5559322B2 (https=) |
| KR (1) | KR20120089450A (https=) |
| CN (1) | CN102471534B (https=) |
| BR (1) | BR112012001128A2 (https=) |
| CA (1) | CA2767940A1 (https=) |
| IL (1) | IL218156A0 (https=) |
| IN (1) | IN2012DN00987A (https=) |
| RU (1) | RU2012105465A (https=) |
| TW (1) | TW201125873A (https=) |
| WO (2) | WO2011031421A1 (https=) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9388340B2 (en) * | 2009-09-11 | 2016-07-12 | Chemtura Corporation | Preparation of hydroxyphenyl phosphine oxide mixtures |
| US20110065838A1 (en) * | 2009-09-11 | 2011-03-17 | Chemtura Corporation | Hydroxyphenyl Phosphine Oxide Mixtures and their use as Flame Retardants for Epoxy Resins |
| US8865862B2 (en) * | 2009-09-11 | 2014-10-21 | Chemtura Corporation | Hydroxyphenyl phosphine oxide mixtures and their use as flame retardants for epoxy resins |
| US9145488B2 (en) * | 2011-05-19 | 2015-09-29 | Chemtura Corporation | Aluminum phosphorus acid salts as epoxy resin cure inhibitors |
| CN104004015A (zh) * | 2014-06-06 | 2014-08-27 | 清华大学 | 二烃基次膦酸的制备方法 |
| US9534108B2 (en) | 2015-03-13 | 2017-01-03 | Chemtura Corporation | Flame retardant epoxy resins comprising phosphorus containing flame retardants |
| CN112409572A (zh) * | 2019-08-22 | 2021-02-26 | 苏州巨峰新材料科技有限公司 | 含磷阻燃低热膨胀系数环氧树脂及其制备方法和所涉及的中间产物以及应用 |
| WO2022040633A1 (en) * | 2020-08-21 | 2022-02-24 | The University Of Southern Mississippi | Phenylphosphine oxide and oxygen stable epoxy polymers and methods of synthesis |
| CN118496702B (zh) * | 2023-02-15 | 2026-04-07 | 江苏冠军科技集团股份有限公司 | 一种基于耐热苯基氧化膦的高闪点防火涂料及其制备方法 |
| TWI860749B (zh) | 2023-06-14 | 2024-11-01 | 南亞塑膠工業股份有限公司 | 磷系耐燃劑、製品及其製造方法 |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4345059A (en) | 1981-05-18 | 1982-08-17 | Fmc Corporation | Fire retardant epoxy resins containing 3-hydroxyalkylphosphine oxides |
| JPS61134395A (ja) | 1984-12-03 | 1986-06-21 | Sumitomo Chem Co Ltd | リン含有エポキシ化合物およびその製法 |
| EP0384940B1 (de) | 1989-03-03 | 1994-06-22 | Siemens Aktiengesellschaft | Epoxidharzmischungen |
| EP0384939B1 (de) | 1989-03-03 | 1994-06-22 | Siemens Aktiengesellschaft | Epoxidharz-Formmassen |
| FI902943A7 (fi) | 1989-07-19 | 1991-01-20 | Siemens Ag | Kuumassa kovettuvia reaktiohartsiseoksia |
| DE4237132C1 (de) | 1992-11-03 | 1994-07-07 | Siemens Ag | UV-aktiviert thermisch härtendes einkomponentiges Reaktionsharzsystem |
| DE4303824A1 (de) | 1993-02-10 | 1994-08-11 | Ruetgerswerke Ag | Epoxidharzsystem |
| DE4340834A1 (de) | 1993-03-15 | 1994-09-22 | Siemens Ag | Phosphormodifizierte Epoxidharze, Verfahren zu ihrer Herstellung sowie ihre Verwendung |
| HU214503B (hu) | 1993-03-15 | 1998-03-30 | Hoechst Aktiengesellschaft | Foszforral módosított epoxigyanták, eljárás előállításukra, és az ilyen gyantákkal előállított termékek |
| DE4308187A1 (de) | 1993-03-15 | 1994-09-22 | Siemens Ag | Epoxidharzmischungen |
| TW294694B (https=) | 1994-09-09 | 1997-01-01 | Siemens Ag | |
| TW297034B (https=) | 1994-09-09 | 1997-02-01 | Siemens Ag | |
| EP0754728A1 (de) | 1995-07-14 | 1997-01-22 | Hoechst Aktiengesellschaft | Flammwidrige Epoxidharz-Formmassen |
| US6162929A (en) * | 1997-12-23 | 2000-12-19 | Hoffmann-La Roche Inc. | Process for the manufacture of bisphosphine oxide and bisphosphonate compounds |
| JP2000186186A (ja) | 1998-12-22 | 2000-07-04 | Sumitomo Bakelite Co Ltd | 難燃性樹脂組成物並びにこれを用いた半導体封止材料および積層板 |
| US6403220B1 (en) * | 1999-12-13 | 2002-06-11 | The Dow Chemical Company | Phosphorus element-containing crosslinking agents and flame retardant phosphorus element-containing epoxy resin compositions prepared therewith |
| TW587094B (en) | 2000-01-17 | 2004-05-11 | Sumitomo Bakelite Co | Flame-retardant resin composition comprising no halogen-containing flame retardant, and prepregs and laminates using such composition |
| US6887950B2 (en) * | 2001-02-15 | 2005-05-03 | Pabu Services, Inc. | Phosphine oxide hydroxyaryl mixtures with novolac resins for co-curing epoxy resins |
| CN100432081C (zh) * | 2001-02-15 | 2008-11-12 | 帕布服务公司 | 双（羟苯基）氧化膦、缩水甘油醚和环氧组合物及由其衍生的复合材料和层压材料 |
| AU2003226414A1 (en) * | 2002-05-30 | 2003-12-19 | Dow Global Technologies, Inc. | Halogen free ignition resistant thermoplastic resin compositions |
| JP2006001876A (ja) * | 2004-06-17 | 2006-01-05 | Songwon Industrial Co Ltd | 機能性有機りん化合物およびその製造方法 |
| US20110065838A1 (en) * | 2009-09-11 | 2011-03-17 | Chemtura Corporation | Hydroxyphenyl Phosphine Oxide Mixtures and their use as Flame Retardants for Epoxy Resins |
-
2010
- 2010-08-17 US US12/857,994 patent/US20110065838A1/en not_active Abandoned
- 2010-08-18 WO PCT/US2010/045849 patent/WO2011031421A1/en not_active Ceased
- 2010-09-01 TW TW99129530A patent/TW201125873A/zh unknown
- 2010-09-09 CN CN2010800325605A patent/CN102471534B/zh active Active
- 2010-09-09 WO PCT/US2010/048235 patent/WO2011031834A1/en not_active Ceased
- 2010-09-09 JP JP2012521886A patent/JP5559322B2/ja active Active
- 2010-09-09 RU RU2012105465/05A patent/RU2012105465A/ru not_active Application Discontinuation
- 2010-09-09 IN IN987DEN2012 patent/IN2012DN00987A/en unknown
- 2010-09-09 CA CA 2767940 patent/CA2767940A1/en not_active Abandoned
- 2010-09-09 KR KR1020127005333A patent/KR20120089450A/ko not_active Withdrawn
- 2010-09-09 BR BR112012001128A patent/BR112012001128A2/pt not_active IP Right Cessation
- 2010-09-09 EP EP10757661.3A patent/EP2475716B1/en active Active
- 2010-09-10 US US12/807,642 patent/US8404161B2/en active Active
-
2012
- 2012-02-16 IL IL218156A patent/IL218156A0/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| WO2011031421A1 (en) | 2011-03-17 |
| IN2012DN00987A (https=) | 2015-04-10 |
| CN102471534B (zh) | 2013-10-16 |
| JP5559322B2 (ja) | 2014-07-23 |
| TW201125873A (en) | 2011-08-01 |
| US20110065869A1 (en) | 2011-03-17 |
| EP2475716A1 (en) | 2012-07-18 |
| US20110065838A1 (en) | 2011-03-17 |
| CN102471534A (zh) | 2012-05-23 |
| KR20120089450A (ko) | 2012-08-10 |
| WO2011031834A1 (en) | 2011-03-17 |
| CA2767940A1 (en) | 2011-03-17 |
| US8404161B2 (en) | 2013-03-26 |
| EP2475716B1 (en) | 2017-04-19 |
| IL218156A0 (en) | 2012-07-31 |
| JP2013500272A (ja) | 2013-01-07 |
| BR112012001128A2 (pt) | 2017-10-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FA92 | Acknowledgement of application withdrawn (lack of supplementary materials submitted) |
Effective date: 20150121 |