RU2003128598A - Способ и устройство для получения синтез-газа - Google Patents

Способ и устройство для получения синтез-газа Download PDF

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RU2003128598A
RU2003128598A RU2003128598/15A RU2003128598A RU2003128598A RU 2003128598 A RU2003128598 A RU 2003128598A RU 2003128598/15 A RU2003128598/15 A RU 2003128598/15A RU 2003128598 A RU2003128598 A RU 2003128598A RU 2003128598 A RU2003128598 A RU 2003128598A
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reforming
heated
reforming unit
catalyst
sections
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RU2354608C2 (ru
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Петер Сайер КРИСТЕНСЕН (DK)
Петер Сайер Кристенсен
Томас РОСТРУП-НИЛЬСЕН (DK)
Томас РОСТРУП-НИЛЬСЕН
Нильс ЭРИКСТРУП (DK)
Нильс ЭРИКСТРУП
Ким ААСБЕРГ-ПЕТЕРСЕН (DK)
Ким Аасберг-Петерсен
Йенс-Хенрик Бак ХАНСЕН (DK)
Йенс-Хенрик Бак ХАНСЕН
Иб ДЮБКЬЯР (DK)
Иб ДЮБКЬЯР
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Хальдор Топсеэ А/С (DK)
Хальдор Топсеэ А/С
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts
    • C01B3/382—Multi-step processes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L3/00—Gaseous fuels; Natural gas; Synthetic natural gas obtained by processes not covered by subclass C10G, C10K; Liquefied petroleum gas
    • C10L3/06—Natural gas; Synthetic natural gas obtained by processes not covered by C10G, C10K3/02 or C10K3/04
    • C10L3/08—Production of synthetic natural gas
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts
    • C01B3/384—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts the catalyst being continuously externally heated
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0205—Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0227—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
    • C01B2203/0233—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being a steam reforming step
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0205—Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0227—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
    • C01B2203/0238—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being a carbon dioxide reforming step
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08—Methods of heating or cooling
    • C01B2203/0805—Methods of heating the process for making hydrogen or synthesis gas
    • C01B2203/0811—Methods of heating the process for making hydrogen or synthesis gas by combustion of fuel
    • C01B2203/0816—Heating by flames
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08—Methods of heating or cooling
    • C01B2203/0805—Methods of heating the process for making hydrogen or synthesis gas
    • C01B2203/0838—Methods of heating the process for making hydrogen or synthesis gas by heat exchange with exothermic reactions, other than by combustion of fuel
    • C01B2203/0844—Methods of heating the process for making hydrogen or synthesis gas by heat exchange with exothermic reactions, other than by combustion of fuel the non-combustive exothermic reaction being another reforming reaction as defined in groups C01B2203/02 - C01B2203/0294
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/10—Catalysts for performing the hydrogen forming reactions
    • C01B2203/1005—Arrangement or shape of catalyst
    • C01B2203/1011—Packed bed of catalytic structures, e.g. particles, packing elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/10—Catalysts for performing the hydrogen forming reactions
    • C01B2203/1005—Arrangement or shape of catalyst
    • C01B2203/1035—Catalyst coated on equipment surfaces, e.g. reactor walls
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14—Details of the flowsheet
    • C01B2203/142—At least two reforming, decomposition or partial oxidation steps in series
    • C01B2203/143—Three or more reforming, decomposition or partial oxidation steps in series
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/141—Feedstock

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  • General Health & Medical Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)

Claims (9)

1. Способ получения синтез-газа каталитическим реформингом с водяным паром и/или CO2 углеводородного сырья, включающий следующие стадии:
(а) нагревание реакционной смеси углеводорода и водяного пара и/или CO2 в нагретой водяным паром реформинг-установке, объединенной с секцией отходящего газа, содержащего бросовое тепло, трубчатой реформинг-установки с огневым обогревом, в которой происходит реформинг реакционной смеси при контакте с твердым катализатором реформинга,
(б) подача частично подвергнутой реформингу с водяным паром смеси в трубчатую реформинг-установку с огневым обогревом и затем реформинг этой смеси до желаемых состава и температуры, при этом реформинг-установка с нагретым водяным паром включает трубную систему, содержащую реакционные секции с твердым катализатором реформинга, включающим гранулы катализатора и/или каталитические структурированные элементы, причем трубная система является частью трубной системы для перерабатываемого газа, объединенной с секцией отходящего газа, содержащего бросовое тепло.
2. Способ по п.1, где реформинг-установка с нагретым водяным паром включает секции нагрева с твердым катализатором реформинга или без него и адиабатические реакционные секции, содержащие каталитические структурированные элементы, покрытые слоем катализатора реформинга с водяным паром, причем обе секции являются частью трубной системы для перерабатываемого газа, объединенной с секцией отходящего газа, содержащего бросовое тепло.
3. Способ по п.1, где реформинг-установка с нагретым водяным паром включает нагреваемые реакционные секции с гранулами катализатора, причем нагреваемые секции являются частью трубной системы для перерабатываемого газа, объединенной с секцией отходящего газа, содержащего бросовое тепло.
4. Способ по п.2 или 3, где реакционную смесь углеводорода и водяного пара и/или CO2 подвергают предварительному реформингу перед стадией нагревания (а).
5. Способ по пп.1, 2 или 3, где структурированный элемент представляет собой монолит или складчатую структуру.
6. Способ по п.2, где водяной пар и/или диоксид углерода добавляют в адиабатические реакционные секции.
7. Способ по пп.1, 2, 3 или 4, где реакционные секции также содержат катализатор реформинга с водяным паром, прикрепленный к стенке
трубы, или катализатор, прикрепленный к структурам, прикрепленным к стенке трубы.
8. Устройство для получения синтез-газа по п.1, включающее следующее:
(а) установку адиабатического предварительного реформинга для необязательного предварительного реформинга смеси углеводорода и водяного пара и/или СО2,
(б) трубчатую реформинг-установку с огневым обогревом с секцией отходящего газа, содержащего бросовое тепло, для нагревания смеси углеводорода и водяного пара и/или CO2 или смеси, подвергнутой предварительному реформингу,
(в) реформинг-установку с нагретым водяным паром, объединенную с секцией отходящего газа, содержащего бросовое тепло, трубчатой реформинг-установки с огневым обогревом, где реформинг-установка с нагретым водяным паром включает трубную систему, содержащую реакционные секции с твердым катализатором реформинга, включающим гранулы катализатора и/или каталитические структурированные элементы, причем трубная система является частью трубной системы для перерабатываемого газа, объединенной с секцией отходящего газа, содержащего бросовое тепло.
9. Устройство по п.8, где твердый катализатор помещают в нагреваемые реакционные секции и/или в адиабатические реакционные секции реформинг-установки с нагретым водяным паром.
RU2003128598/04A 2002-09-26 2003-09-25 Способ и устройство для получения синтез-газа RU2354608C2 (ru)

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US7547332B2 (en) 2009-06-16
NO336969B1 (no) 2015-12-07
CN1496956A (zh) 2004-05-19
JP2004269345A (ja) 2004-09-30
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RU2354608C2 (ru) 2009-05-10
US20060143984A1 (en) 2006-07-06
JP4959105B2 (ja) 2012-06-20
ES2405587T3 (es) 2013-05-31
CN1328153C (zh) 2007-07-25
KR20040027456A (ko) 2004-04-01
AU2003248394A1 (en) 2004-04-22
US7094363B2 (en) 2006-08-22
KR101044621B1 (ko) 2011-06-29
US20040065014A1 (en) 2004-04-08
ZA200307449B (en) 2004-07-06
NO20034283L (no) 2004-03-29
AU2003248394B2 (en) 2010-03-11
CA2442493A1 (en) 2004-03-26
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CA2442493C (en) 2011-05-03
NO20034283D0 (no) 2003-09-25

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