PL150462B1 - Multistage counter-current scrubbing method and system - Google Patents
Multistage counter-current scrubbing method and systemInfo
- Publication number
- PL150462B1 PL150462B1 PL1986263167A PL26316786A PL150462B1 PL 150462 B1 PL150462 B1 PL 150462B1 PL 1986263167 A PL1986263167 A PL 1986263167A PL 26316786 A PL26316786 A PL 26316786A PL 150462 B1 PL150462 B1 PL 150462B1
- Authority
- PL
- Poland
- Prior art keywords
- hydrocyclones
- tank
- upstream
- pressure
- pump
- Prior art date
Links
- 238000005201 scrubbing Methods 0.000 title claims description 9
- 239000007788 liquid Substances 0.000 claims description 76
- 238000011144 upstream manufacturing Methods 0.000 claims description 49
- 238000005406 washing Methods 0.000 claims description 49
- 239000007787 solid Substances 0.000 claims description 37
- 239000013078 crystal Substances 0.000 claims description 25
- 238000000034 method Methods 0.000 claims description 16
- 239000000725 suspension Substances 0.000 claims description 14
- 230000008569 process Effects 0.000 claims description 9
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000005192 partition Methods 0.000 claims description 5
- 230000003247 decreasing effect Effects 0.000 claims description 2
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 15
- 239000002245 particle Substances 0.000 description 13
- 238000002425 crystallisation Methods 0.000 description 8
- 230000008025 crystallization Effects 0.000 description 8
- 239000012535 impurity Substances 0.000 description 8
- 239000002002 slurry Substances 0.000 description 7
- 239000002904 solvent Substances 0.000 description 7
- 229910000831 Steel Inorganic materials 0.000 description 6
- 230000001174 ascending effect Effects 0.000 description 6
- 239000003245 coal Substances 0.000 description 6
- WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 description 6
- 238000011010 flushing procedure Methods 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 239000010959 steel Substances 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 230000009467 reduction Effects 0.000 description 5
- 239000012047 saturated solution Substances 0.000 description 5
- 238000000926 separation method Methods 0.000 description 5
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 239000004215 Carbon black (E152) Substances 0.000 description 4
- 230000008901 benefit Effects 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 229930195733 hydrocarbon Natural products 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- 238000004090 dissolution Methods 0.000 description 3
- 238000005984 hydrogenation reaction Methods 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- GOUHYARYYWKXHS-UHFFFAOYSA-N 4-formylbenzoic acid Chemical compound OC(=O)C1=CC=C(C=O)C=C1 GOUHYARYYWKXHS-UHFFFAOYSA-N 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- 239000011362 coarse particle Substances 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 239000011241 protective layer Substances 0.000 description 2
- 230000002285 radioactive effect Effects 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 230000008439 repair process Effects 0.000 description 2
- 150000003503 terephthalic acid derivatives Chemical class 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 229910052792 caesium Inorganic materials 0.000 description 1
- TVFDJXOCXUVLDH-UHFFFAOYSA-N caesium atom Chemical compound [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- VNNRSPGTAMTISX-UHFFFAOYSA-N chromium nickel Chemical compound [Cr].[Ni] VNNRSPGTAMTISX-UHFFFAOYSA-N 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000009795 derivation Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical class C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000001603 reducing effect Effects 0.000 description 1
- 239000008237 rinsing water Substances 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- KKEYFWRCBNTPAC-UHFFFAOYSA-L terephthalate(2-) Chemical compound [O-]C(=O)C1=CC=C(C([O-])=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-L 0.000 description 1
- 230000008646 thermal stress Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D43/00—Separating particles from liquids, or liquids from solids, otherwise than by sedimentation or filtration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Extraction Or Liquid Replacement (AREA)
- Cyclones (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
- Pipeline Systems (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3600522 | 1986-01-10 | ||
| DE3606259 | 1986-02-27 | ||
| DE19863639958 DE3639958A1 (de) | 1986-01-10 | 1986-11-22 | Mehrstufige anordnung zur gegenstromwaschung, sowie zugehoerige verfahrensmassnahmen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL263167A1 PL263167A1 (en) | 1987-12-14 |
| PL150462B1 true PL150462B1 (en) | 1990-05-31 |
Family
ID=27193909
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL1986263167A PL150462B1 (en) | 1986-01-10 | 1986-12-22 | Multistage counter-current scrubbing method and system |
Country Status (17)
| Country | Link |
|---|---|
| US (2) | US4707274A (forum.php) |
| EP (1) | EP0229356B1 (forum.php) |
| KR (1) | KR880005957A (forum.php) |
| AR (1) | AR245019A1 (forum.php) |
| BG (1) | BG48454A3 (forum.php) |
| BR (1) | BR8700098A (forum.php) |
| DE (2) | DE3639958A1 (forum.php) |
| ES (1) | ES2034958T3 (forum.php) |
| GR (1) | GR3006336T3 (forum.php) |
| IL (1) | IL81220A (forum.php) |
| MX (1) | MX168672B (forum.php) |
| PH (1) | PH24878A (forum.php) |
| PL (1) | PL150462B1 (forum.php) |
| PT (1) | PT84076B (forum.php) |
| SU (1) | SU1679972A3 (forum.php) |
| TR (1) | TR23582A (forum.php) |
| YU (1) | YU2887A (forum.php) |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1376325A1 (ru) * | 1986-07-10 | 1990-08-23 | Научно-производственное объединение по крахмалопродуктам | Многоступенчата мультициклонна установка |
| US5794791A (en) * | 1987-11-30 | 1998-08-18 | Genesis Research Corporation | Coal cleaning process |
| CA1327342C (en) * | 1987-11-30 | 1994-03-01 | James Kelly Kindig | Process for beneficiating particulate solids |
| GB8803138D0 (en) * | 1988-02-11 | 1988-03-09 | Atomic Energy Authority Uk | Fluidic contactors |
| US4960525A (en) * | 1988-09-26 | 1990-10-02 | The United States Of America, As Represented By The Secretary Of Agriculture | Hydrocyclone for washing particles in liquid suspension |
| US5492622A (en) * | 1990-09-28 | 1996-02-20 | Broussard; Paul C. | Water clarification apparatus |
| US5158678A (en) * | 1990-09-28 | 1992-10-27 | Broussard Paul C Sr | Water clarification method and apparatus |
| US5472094A (en) * | 1993-10-04 | 1995-12-05 | Electric Power Research Institute | Flotation machine and process for removing impurities from coals |
| JP3808672B2 (ja) * | 1999-11-26 | 2006-08-16 | 東洋製罐株式会社 | 回収ポリエチレンテレフタレート粉砕品からのテレフタル酸の工業的回収方法 |
| CN1230235C (zh) * | 2000-10-02 | 2005-12-07 | 三菱瓦斯化学株式会社 | 晶析方法 |
| US7276625B2 (en) * | 2002-10-15 | 2007-10-02 | Eastman Chemical Company | Process for production of a carboxylic acid/diol mixture suitable for use in polyester production |
| DE10251792A1 (de) * | 2002-11-07 | 2004-05-19 | Industriebetriebe Heinrich Meyer-Werke Breloh Gmbh & Co. Kg | Verfahren zur Regenerierung von Filtermitteln, insbesondere Kieselgur |
| US7132566B2 (en) * | 2003-09-22 | 2006-11-07 | Eastman Chemical Company | Process for the purification of a crude carboxylic acid slurry |
| US7161027B2 (en) | 2002-12-09 | 2007-01-09 | Eastman Chemical Company | Process for the oxidative purification of terephthalic acid |
| US7074954B2 (en) * | 2002-12-09 | 2006-07-11 | Eastman Chemical Company | Process for the oxidative purification of terephthalic acid |
| BR0316462A (pt) * | 2002-12-09 | 2005-10-11 | Eastman Chem Co | Processos para reduzir uma suspensão de ácido carboxìlico purificado, para purificar um produto de oxidação em estágios, para produzir um produto de ácido carboxìlico purificado, e, suspensão de ácido carboxìlico purificado |
| US7193109B2 (en) | 2003-03-06 | 2007-03-20 | Eastman Chemical Company | Process for production of a carboxylic acid/diol mixture suitable for use in polyester production |
| US20050059709A1 (en) * | 2003-09-15 | 2005-03-17 | Meythaler Jay M. | Treatment of a neuropathy with rapid release aminopyridine |
| US7214760B2 (en) * | 2004-01-15 | 2007-05-08 | Eastman Chemical Company | Process for production of a carboxylic acid/diol mixture suitable for use in polyester production |
| SE529771C2 (sv) * | 2005-04-29 | 2007-11-20 | Gl & V Man Hungary Kft Hermina | Hydrocyklonenhet och metod för separering av en fibermassasuspension innehållande relativt tunga föroreningar |
| ITRM20050329A1 (it) * | 2005-06-24 | 2006-12-25 | Guido Fragiacomo | Procedimento per il trattamento di sospensioni abrasive esauste per il recupero delle loro componenti riciclabili e relativo impianto. |
| US20070179312A1 (en) * | 2006-02-02 | 2007-08-02 | O'meadhra Ruairi Seosamh | Process for the purification of a crude carboxylic axid slurry |
| US8614350B2 (en) | 2008-01-15 | 2013-12-24 | Eastman Chemical Company | Carboxylic acid production process employing solvent from esterification of lignocellulosic material |
| US8455680B2 (en) | 2008-01-15 | 2013-06-04 | Eastman Chemical Company | Carboxylic acid production process employing solvent from esterification of lignocellulosic material |
| AU2017274307A1 (en) * | 2016-06-01 | 2019-01-24 | Keller Technologies, Inc. | Refiner for lactose and high lactose products |
| US11015156B1 (en) * | 2020-05-22 | 2021-05-25 | Franzenburg | Protein concentration methods |
| EP4249096A4 (en) * | 2020-11-20 | 2024-11-20 | Nippon Shokubai Co., Ltd. | Method for purifying compound |
| CN113144660B (zh) * | 2021-02-05 | 2023-03-03 | 成都思达能环保设备有限公司 | 一种结晶方法及系统 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE855098C (de) * | 1949-11-01 | 1952-11-10 | Metallgesellschaft Ag | Verfahren und Vorrichtung zur kontinuierlichen Gegenstrom-Extraktion von Fluessigkeiten mit Fluessigkeiten |
| DE878043C (de) * | 1951-09-01 | 1953-05-28 | Westfalia Separator Ag | Gegenstromextraktionsanlage |
| DE1263697B (de) * | 1964-06-08 | 1968-03-21 | Maerkische Oelwerke Wittenberg | Verfahren zur kontinuierlichen, stufenweisen Gegenstromextraktion von Feststoffen mit fluessigen Loesungsmitteln |
| US3952052A (en) * | 1974-04-15 | 1976-04-20 | Phillips Petroleum Company | Process for producing alkali metal salts of aromatic polycarboxylic acids |
| US4053506A (en) * | 1975-05-02 | 1977-10-11 | Standard Oil Company (Indiana) | Production of fiber-grade terephthalic acid |
| US4455224A (en) * | 1979-03-19 | 1984-06-19 | Clark & Vicario Corporation | Apparatus for treating a papermaking suspension |
| US4285706A (en) * | 1979-03-20 | 1981-08-25 | Dehne Manfred F | Particulate filtration device |
| DE3044617C2 (de) | 1980-11-27 | 1985-09-26 | Dynamit Nobel Ag, 5210 Troisdorf | Verfahren zur Herstellung von Terephthalsäure aus Dimethylterephthalat als Zwischenprodukt |
| AU567503B2 (en) * | 1982-08-23 | 1987-11-26 | Ok Tedi Mining Ltd. | Process and apparatus for the elution of values from solid particles |
| DE3410143A1 (de) * | 1984-03-20 | 1985-10-03 | Deutsche Babcock Werke AG, 4200 Oberhausen | Vorrichtung zum entstauben von unter druck stehendem gas |
-
1986
- 1986-11-22 DE DE19863639958 patent/DE3639958A1/de not_active Withdrawn
- 1986-12-18 EP EP86117650A patent/EP0229356B1/de not_active Expired - Lifetime
- 1986-12-18 DE DE8686117650T patent/DE3687165D1/de not_active Expired - Fee Related
- 1986-12-18 ES ES198686117650T patent/ES2034958T3/es not_active Expired - Lifetime
- 1986-12-19 AR AR86306271A patent/AR245019A1/es active
- 1986-12-22 PL PL1986263167A patent/PL150462B1/pl unknown
- 1986-12-24 PH PH34663A patent/PH24878A/en unknown
- 1986-12-25 BG BG077722A patent/BG48454A3/xx unknown
- 1986-12-31 US US06/948,049 patent/US4707274A/en not_active Expired - Fee Related
-
1987
- 1987-01-08 TR TR22/87A patent/TR23582A/xx unknown
- 1987-01-08 PT PT84076A patent/PT84076B/pt not_active IP Right Cessation
- 1987-01-09 YU YU00028/87A patent/YU2887A/xx unknown
- 1987-01-09 MX MX004898A patent/MX168672B/es unknown
- 1987-01-09 SU SU874028783A patent/SU1679972A3/ru active
- 1987-01-09 IL IL81220A patent/IL81220A/xx unknown
- 1987-01-10 KR KR870000207A patent/KR880005957A/ko not_active Ceased
- 1987-01-12 BR BR8700098A patent/BR8700098A/pt not_active IP Right Cessation
- 1987-07-31 US US07/080,746 patent/US4755295A/en not_active Expired - Fee Related
-
1992
- 1992-11-26 GR GR920402451T patent/GR3006336T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| GR3006336T3 (forum.php) | 1993-06-21 |
| EP0229356A2 (de) | 1987-07-22 |
| DE3639958A1 (de) | 1987-07-16 |
| PH24878A (en) | 1990-12-26 |
| US4755295A (en) | 1988-07-05 |
| IL81220A (en) | 1991-03-10 |
| PL263167A1 (en) | 1987-12-14 |
| MX168672B (es) | 1993-06-02 |
| AR245019A1 (es) | 1993-12-30 |
| BG48454A3 (en) | 1991-02-15 |
| DE3687165D1 (de) | 1993-01-07 |
| BR8700098A (pt) | 1987-12-01 |
| EP0229356A3 (en) | 1988-06-22 |
| SU1679972A3 (ru) | 1991-09-23 |
| ES2034958T3 (es) | 1993-04-16 |
| EP0229356B1 (de) | 1992-11-25 |
| US4707274A (en) | 1987-11-17 |
| PT84076A (de) | 1987-02-01 |
| PT84076B (pt) | 1993-03-31 |
| KR880005957A (ko) | 1988-07-21 |
| YU2887A (en) | 1989-04-30 |
| IL81220A0 (en) | 1987-08-31 |
| TR23582A (tr) | 1990-04-06 |
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