PE14097A1 - Composiciones de extrusion que tienen alto estiramiento y rebordeo sustancialmente reducido - Google Patents

Composiciones de extrusion que tienen alto estiramiento y rebordeo sustancialmente reducido

Info

Publication number
PE14097A1
PE14097A1 PE1995284347A PE28434795A PE14097A1 PE 14097 A1 PE14097 A1 PE 14097A1 PE 1995284347 A PE1995284347 A PE 1995284347A PE 28434795 A PE28434795 A PE 28434795A PE 14097 A1 PE14097 A1 PE 14097A1
Authority
PE
Peru
Prior art keywords
composition
ethylene polymer
sub
ethylene
determined
Prior art date
Application number
PE1995284347A
Other languages
English (en)
Inventor
Lawrence T Kale
David C Kelley
Sharon L Baker
Osborne K Mckinney
Pradeep Jain
Deepak R Parikh
Original Assignee
Dow Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=26991158&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=PE14097(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority claimed from US08/344,262 external-priority patent/US5582923A/en
Application filed by Dow Chemical Co filed Critical Dow Chemical Co
Publication of PE14097A1 publication Critical patent/PE14097A1/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L23/04—Homopolymers or copolymers of ethene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/18—Manufacture of films or sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/022—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the choice of material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00—Layered products comprising a layer of synthetic resin
    • B32B27/32—Layered products comprising a layer of synthetic resin comprising polyolefins
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00—Layered products comprising a layer of synthetic resin
    • B32B27/32—Layered products comprising a layer of synthetic resin comprising polyolefins
    • B32B27/322—Layered products comprising a layer of synthetic resin comprising polyolefins comprising halogenated polyolefins, e.g. PTFE
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L23/04—Homopolymers or copolymers of ethene
    • C08L23/08—Copolymers of ethene
    • C08L23/0807—Copolymers of ethene with unsaturated hydrocarbons only containing more than three carbon atoms
    • C08L23/0815—Copolymers of ethene with aliphatic 1-olefins
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00—Materials not provided for elsewhere
    • C09K3/10—Materials in mouldable or extrudable form for sealing or packing joints or covers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/03—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the shape of the extruded material at extrusion
    • B29C48/06—Rod-shaped
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/03—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the shape of the extruded material at extrusion
    • B29C48/09—Articles with cross-sections having partially or fully enclosed cavities, e.g. pipes or channels
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F110/00—Homopolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F110/02—Ethene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F210/00—Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F210/16—Copolymers of ethene with alpha-alkenes, e.g. EP rubbers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2323/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
    • C08J2323/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
    • C08J2323/04—Homopolymers or copolymers of ethene
    • C08J2323/08—Copolymers of ethene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L23/04—Homopolymers or copolymers of ethene
    • C08L23/06—Polyethene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2314/00—Polymer mixtures characterised by way of preparation
    • C08L2314/06—Metallocene or single site catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Paints Or Removers (AREA)
  • Laminated Bodies (AREA)
  • Extrusion Moulding Of Plastics Or The Like (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)

Abstract

ESTA REFERIDA A UNA COMPOSICION DE EXTRUSION DE UN POLIMERO DE ETILENO COMPUESTA POR 75% A 95% DEL PESO DE LA COMPOSICION TOTAL, DE POR LO MENOS UNA COMPOSICION DE INTERPOLIMERO DE ETILENO/O-OLEFINA SELECCIONADA DEL GRUPO CONFORMADO POR EL POLIMERO DE ETILENO SUSTANCIALMENTE LINEAL, UNA COMPOSICION DE POLIMERO DE ETILENO LINEAL HOMOGENEAMENTE RAMIFICADO, EN DONDE EL INTERPOLIMERO DE ETILENO/O-OLEFINA SE CARACTERIZA POR TENER UNA DENSIDAD QUE VARIA ENTRE 0,85 g/cm3 Y O,940 g/cm3 Y DE 5% A 25%, DEL PESO DE LA COMPOSICION TOTAL, DE POR LO MENOS UN POLIMERO DE ETILENO DE ALTA PRESION CARACTERIZADO POR TENER UN INDICE DE FUSION I(SUB)2, MENOR A 6,0 g/10 MINUTOS, UNA DENSIDAD DE POR LO MENOS 0,916 g/cm3, UNA RESISTENCIA A LA FUSION DE POR LO MENOS 9 cN COMO SE DETERMINA USANDO UNA UNIDAD GOTTFERT RHEOTENS A 190�C, UN RATIO M(SUB)W/M(SUB)N DE POR LO MENOS 7,0 DETERMINADO MEDIANTE CROMATOGRAFIA DE PERMEACION DE GEL Y UNA DISTRIBUCION DE PESO MOLECULAR BIDIMODAL DETERMINADA POR EL METODO ANTICIPADO, EN DONDE LA COMPOSICION DE EXTRUSION DEL POLIMERO DE ETILENO TIENE UN INDICE DE FUSION I(SUB)2 DE POR LO MENOS 1,0 g/10 MINUTOS. EN PERFILES, RECUBRIMIENTOS O PELICULAS, LA COMPOSICION PUEDE SER USADA COMO CAPA SELLANTE, ADHESIVA O DE RESISTENCIA AL ESTIRAMIENTO
PE1995284347A 1994-11-14 1995-11-13 Composiciones de extrusion que tienen alto estiramiento y rebordeo sustancialmente reducido PE14097A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US33836694A 1994-11-14 1994-11-14
US08/344,262 US5582923A (en) 1991-10-15 1994-11-23 Extrusion compositions having high drawdown and substantially reduced neck-in

Publications (1)

Publication Number Publication Date
PE14097A1 true PE14097A1 (es) 1997-05-07

Family

ID=26991158

Family Applications (1)

Application Number Title Priority Date Filing Date
PE1995284347A PE14097A1 (es) 1994-11-14 1995-11-13 Composiciones de extrusion que tienen alto estiramiento y rebordeo sustancialmente reducido

Country Status (18)

Country Link
EP (1) EP0792318B1 (es)
JP (1) JP3582836B2 (es)
KR (1) KR100396958B1 (es)
AR (1) AR000687A1 (es)
AT (1) ATE185829T1 (es)
AU (1) AU691386B2 (es)
BR (1) BR9510328A (es)
CA (1) CA2205116C (es)
DE (1) DE69512932T2 (es)
ES (1) ES2137558T3 (es)
FI (1) FI117976B (es)
IL (1) IL115911A0 (es)
MX (1) MX9703565A (es)
MY (1) MY112741A (es)
NO (1) NO319158B1 (es)
NZ (1) NZ297629A (es)
PE (1) PE14097A1 (es)
WO (1) WO1996016119A1 (es)

Families Citing this family (48)

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JP3431706B2 (ja) * 1994-12-16 2003-07-28 新日本石油化学株式会社 積層体・不織布または織布並びにそれらを用いた強化積層体
US5879768A (en) † 1995-10-06 1999-03-09 The Dow Chemical Company Pouches for packaging flowable materials
US5858515A (en) * 1995-12-29 1999-01-12 Kimberly-Clark Worldwide, Inc. Pattern-unbonded nonwoven web and process for making the same
AU3403097A (en) * 1996-06-21 1998-01-07 Dow Chemical Company, The Peelable-seal compositions and sealant film layers
US5718974A (en) * 1996-06-24 1998-02-17 Union Carbide Chemicals & Plastics Technology Corporation Cable jacket
US5849823A (en) * 1996-09-04 1998-12-15 The Dow Chemical Company Homogeneously branched ethylene α-olefin interpolymer compositions for use in gasket applications
GB9620651D0 (en) * 1996-10-02 1996-11-20 Norester S A A laminate
JP4008973B2 (ja) * 1996-11-27 2007-11-14 出光興産株式会社 包装袋用フィルム
JP4233126B2 (ja) * 1996-11-27 2009-03-04 出光興産株式会社 包装袋用多層フィルム
US6485662B1 (en) 1996-12-03 2002-11-26 Union Carbide Chemicals & Plastics Technology Corporation Process for preparing a simulated in situ polyethylene blend
WO1998024842A1 (en) * 1996-12-03 1998-06-11 Union Carbide Chemicals & Plastics Technology Corporation Process for preparing a simulated in situ polyethylene blend
FI111166B (fi) 1997-01-10 2003-06-13 Borealis Polymers Oy Ekstruusiopäällystysrakenne
US6416833B1 (en) * 1997-08-22 2002-07-09 Dupont Canada Inc. Interpolymer film pouch
GB9800245D0 (en) * 1998-01-07 1998-03-04 Bp Chem Int Ltd Novel polymers
EP1047723A1 (en) * 1998-01-21 2000-11-02 Eastman Chemical Company Modified polyester with improved processability and adhesion in extrusion coating applications
JP2002523310A (ja) * 1998-08-21 2002-07-30 デュポン カナダ インコーポレイテッド 改良された漏出部頻度性能を有する液体パッケージ
US6632911B1 (en) * 1999-11-05 2003-10-14 Japan Polychem Corporation Ethylene/α-olefin copolymer and film made thereof
EP1457518A1 (en) * 1999-12-03 2004-09-15 Dow Global Technologies, Inc. Grafted thermoplastic compositions and fabricated articles therefrom
US6395791B1 (en) 1999-12-03 2002-05-28 The Dow Chemical Company Grafted thermoplastic compositions and fabricated articles therefrom
FI111954B (fi) 2000-02-21 2003-10-15 Borealis Tech Oy Menetelmä polyeteenipäällysteen valmistamiseksi substraatille
JP2002105253A (ja) * 2000-09-29 2002-04-10 Asahi Kasei Corp 重包装袋用ポリエチレン樹脂組成物
JP4749539B2 (ja) * 2000-12-18 2011-08-17 三井化学株式会社 ポリプロピレン用シーラント材およびそれを用いた易開封性密封容器
GB0126147D0 (en) * 2001-10-31 2002-01-02 Borealis Tech Oy Process
US7846552B2 (en) * 2002-09-23 2010-12-07 Dow Global Technologies Inc. Polymer compositions for extrusion coating
US7776987B2 (en) * 2003-09-05 2010-08-17 Dow Global Technologies, Inc. Resin compositions for extrusion coating
JP4765277B2 (ja) * 2004-07-30 2011-09-07 東ソー株式会社 積層体
CA2585376C (en) * 2004-11-16 2013-06-25 Dow Global Technologies Inc. Elastomeric compositions with improved resistance to necking for high speed sheet extrusion applications
DE602005001055T2 (de) 2005-10-18 2007-12-27 Borealis Technology Oy Polyethylenmischungskomponente und diese enthaltende Mischungen
US8653193B2 (en) 2009-09-28 2014-02-18 Exxonmobil Chemical Patents Inc. Polyolefin compositions and products made therefrom
US8679639B2 (en) * 2009-11-24 2014-03-25 Dow Global Technologies Llc Extrusion coating composition
US8784996B2 (en) 2009-11-24 2014-07-22 Dow Global Technologies Llc Extrusion coating composition
US9493641B2 (en) * 2011-06-10 2016-11-15 Dow Global Technologies Llc Resin compositions for extrusion coating
MX354789B (es) * 2011-07-08 2018-03-21 Dow Global Technologies Llc Composicion de mezcla de polietileno adecuada para pelicula soplada, metodo para producir la misma y peliculas hechas a partir de la misma.
EP2782960B1 (en) 2011-11-23 2016-11-09 Dow Global Technologies LLC Low density ethylene-based polymers with extracts at lower molecular weights
US9228036B2 (en) 2011-11-23 2016-01-05 Dow Global Technologies Llc Low density ethylene-based polymers with broad molecular weight distributions and low extractables
EP2631268A1 (en) 2012-02-22 2013-08-28 Borealis AG Extrusion coating polyethylene with improved drawdown
EP2831187B1 (en) 2012-03-28 2017-11-15 Borealis AG Extrusion coated polymer layer with reduced coefficient of friction
CN104781289B (zh) * 2012-09-28 2018-04-10 陶氏环球技术有限公司 乙烯基聚合物和其制造方法
ES2640018T3 (es) 2012-11-20 2017-10-31 Dow Global Technologies Llc Polímeros a base de etileno de baja densidad con alta resistencia en estado fundido
CN105189639B (zh) 2013-05-22 2018-02-06 陶氏环球技术有限责任公司 具有改进的熔体强度、产量以及机械特性的低密度乙烯类组合物
BR112015027619B1 (pt) 2013-05-22 2021-05-18 Dow Global Technologies Llc composições contendo polímeros à base de etileno de baixa densidade, artigo e filme
AR102954A1 (es) * 2014-12-19 2017-04-05 Dow Global Technologies Llc Una estructura de capa múltiple, un método para producir la misma, y un envasado que comprende la misma
KR102397059B1 (ko) 2015-06-30 2022-05-12 다우 글로벌 테크놀로지스 엘엘씨 개선된 압출 코팅을 위한 에틸렌계 폴리머 조성물
WO2018118362A1 (en) 2016-12-22 2018-06-28 Dow Global Technologies Llc Process to make high density ethylene-based polymer compositions with high melt strength
EP3453727A1 (en) * 2017-09-08 2019-03-13 Borealis AG Process for preparing polypropylene composition
CA3198297A1 (en) * 2020-11-20 2022-05-27 Dow Global Technologies Llc Multilayer structures and articles with coating layers
CN112595715B (zh) * 2020-12-07 2023-04-14 武汉科技大学 一种高温熔渣中自由基相对含量的检测方法
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US5278272A (en) * 1991-10-15 1994-01-11 The Dow Chemical Company Elastic substantialy linear olefin polymers
US5395471A (en) * 1991-10-15 1995-03-07 The Dow Chemical Company High drawdown extrusion process with greater resistance to draw resonance
ATE148905T1 (de) * 1992-09-16 1997-02-15 Exxon Chemical Patents Inc Weiche filme mit verbesserten physikalischen eigenschaften
EP0601495B1 (en) * 1992-12-07 2002-04-24 Mitsubishi Chemical Corporation Resin composition for extruded forms

Also Published As

Publication number Publication date
ES2137558T3 (es) 1999-12-16
BR9510328A (pt) 1998-06-02
WO1996016119A1 (en) 1996-05-30
MY112741A (en) 2001-08-30
NO972203L (no) 1997-07-14
FI117976B (fi) 2007-05-15
FI972032A (fi) 1997-07-11
KR100396958B1 (ko) 2003-12-01
DE69512932T2 (de) 2000-03-09
AU691386B2 (en) 1998-05-14
ATE185829T1 (de) 1999-11-15
EP0792318B1 (en) 1999-10-20
NO319158B1 (no) 2005-06-27
CA2205116A1 (en) 1996-05-30
EP0792318A1 (en) 1997-09-03
IL115911A0 (en) 1996-01-31
NZ297629A (en) 2000-01-28
DE69512932D1 (de) 1999-11-25
NO972203D0 (no) 1997-05-13
CA2205116C (en) 2003-07-29
FI972032A0 (fi) 1997-05-13
MX9703565A (es) 1997-08-30
AU4283096A (en) 1996-06-17
AR000687A1 (es) 1997-08-06
KR970707228A (ko) 1997-12-01
JP3582836B2 (ja) 2004-10-27
JPH10509200A (ja) 1998-09-08

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