NO810966L - Fremgangsmaate for fremstilling av farvestoffet direkte gult ii i form av konsentrerte stabile opploesninger, opploesningene og deres anvendelse - Google Patents
Fremgangsmaate for fremstilling av farvestoffet direkte gult ii i form av konsentrerte stabile opploesninger, opploesningene og deres anvendelseInfo
- Publication number
- NO810966L NO810966L NO810966A NO810966A NO810966L NO 810966 L NO810966 L NO 810966L NO 810966 A NO810966 A NO 810966A NO 810966 A NO810966 A NO 810966A NO 810966 L NO810966 L NO 810966L
- Authority
- NO
- Norway
- Prior art keywords
- parts
- acid
- toluene
- solutions
- alcohols
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 14
- 238000002360 preparation method Methods 0.000 title description 2
- 239000000243 solution Substances 0.000 claims description 32
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 27
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 18
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 18
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 16
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 11
- 239000002253 acid Substances 0.000 claims description 11
- 150000001298 alcohols Chemical class 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 9
- SBASXUCJHJRPEV-UHFFFAOYSA-N 2-(2-methoxyethoxy)ethanol Chemical compound COCCOCCO SBASXUCJHJRPEV-UHFFFAOYSA-N 0.000 claims description 8
- ZDTXQHVBLWYPHS-UHFFFAOYSA-N 4-nitrotoluene-2-sulfonic acid Chemical compound CC1=CC=C([N+]([O-])=O)C=C1S(O)(=O)=O ZDTXQHVBLWYPHS-UHFFFAOYSA-N 0.000 claims description 8
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 7
- 239000010985 leather Substances 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 5
- 238000004043 dyeing Methods 0.000 claims description 5
- 229920002678 cellulose Polymers 0.000 claims description 4
- 239000001913 cellulose Substances 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 4
- 235000011152 sodium sulphate Nutrition 0.000 claims description 4
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 3
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 230000035484 reaction time Effects 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 125000003158 alcohol group Chemical group 0.000 claims description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 2
- 239000000975 dye Substances 0.000 description 29
- 239000000843 powder Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 6
- 238000003860 storage Methods 0.000 description 6
- 150000003839 salts Chemical class 0.000 description 3
- 239000004753 textile Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 2
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 125000000129 anionic group Chemical group 0.000 description 2
- OIQPTROHQCGFEF-UHFFFAOYSA-L chembl1371409 Chemical compound [Na+].[Na+].OC1=CC=C2C=C(S([O-])(=O)=O)C=CC2=C1N=NC1=CC=C(S([O-])(=O)=O)C=C1 OIQPTROHQCGFEF-UHFFFAOYSA-L 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 229940093476 ethylene glycol Drugs 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- -1 hexafluorosilicic acid Chemical compound 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- XNWFRZJHXBZDAG-UHFFFAOYSA-N 2-METHOXYETHANOL Chemical group COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 description 1
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 229920003043 Cellulose fiber Polymers 0.000 description 1
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 239000007983 Tris buffer Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- BUACSMWVFUNQET-UHFFFAOYSA-H dialuminum;trisulfate;hydrate Chemical compound O.[Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O BUACSMWVFUNQET-UHFFFAOYSA-H 0.000 description 1
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 150000007530 organic bases Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 229910001415 sodium ion Inorganic materials 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0072—Preparations with anionic dyes or reactive dyes
- C09B67/0073—Preparations of acid or reactive dyes in liquid form
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B56/00—Azo dyes containing other chromophoric systems
- C09B56/04—Stilbene-azo dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B69/00—Dyes not provided for by a single group of this subclass
- C09B69/02—Dyestuff salts, e.g. salts of acid dyes with basic dyes
- C09B69/04—Dyestuff salts, e.g. salts of acid dyes with basic dyes of anionic dyes with nitrogen containing compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8006319A FR2478658A1 (fr) | 1980-03-21 | 1980-03-21 | Procede de preparation de colorant jaune direct 11 sous forme de solutions concentrees stables, solutions obtenues et applications |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO810966L true NO810966L (no) | 1981-09-22 |
Family
ID=9239937
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO810966A NO810966L (no) | 1980-03-21 | 1981-03-20 | Fremgangsmaate for fremstilling av farvestoffet direkte gult ii i form av konsentrerte stabile opploesninger, opploesningene og deres anvendelse |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US4310331A (fr) |
| JP (1) | JPS56145956A (fr) |
| AU (1) | AU6859681A (fr) |
| BE (1) | BE887894A (fr) |
| BR (1) | BR8101666A (fr) |
| DE (1) | DE3110261A1 (fr) |
| DK (1) | DK127681A (fr) |
| ES (1) | ES8206603A1 (fr) |
| FI (1) | FI810868L (fr) |
| FR (1) | FR2478658A1 (fr) |
| GB (1) | GB2072213B (fr) |
| IT (1) | IT1144320B (fr) |
| NL (1) | NL8101367A (fr) |
| NO (1) | NO810966L (fr) |
| SE (1) | SE8101802L (fr) |
| ZA (1) | ZA811876B (fr) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3462916D1 (en) * | 1983-03-04 | 1987-05-07 | Ciba Geigy Ag | Concentrated storage-stable aqueous solutions of yellow to greenish yellow stilbene azo or stilbene azoxy dyes |
| US4502864A (en) * | 1984-04-25 | 1985-03-05 | Ciba-Geigy Corporation | Crown ether complexes of direct yellow 11 and dyestuff containing same |
| US4617381A (en) * | 1984-09-11 | 1986-10-14 | Ciba-Geigy Corporation | Process for the preparation of concentrated stable liquid dye solutions of CI Direct Yellow 11 utilizing an alkanol/water solvent in a desalting procedure |
| CH692246A5 (de) * | 1996-12-13 | 2002-04-15 | Basf Ag | Verfahren zur Herstellung von Aminsalzen von 4-Nitrotoluol-2-sulfonsäure. |
| DE60012915T2 (de) * | 1999-06-02 | 2005-07-14 | Ciba Speciality Chemicals Holding Inc. | Gelbe azo- und azoxystilbenfarbstoffe |
| DE502004011476D1 (de) * | 2003-12-22 | 2010-09-16 | Basf Se | Flüssigformulierungen von Direktfarbstoffen |
| CN101805527A (zh) * | 2010-04-14 | 2010-08-18 | 天津大学 | 4-硝基甲苯-2-磺酸自缩聚染料液体色浆的制备方法 |
| WO2012120543A1 (fr) | 2011-03-09 | 2012-09-13 | Council Of Scientific & Industrial Research | Procédé en une seule étape pour la synthèse du colorant yellow dye 11 de ton uniforme |
| CN104292876B (zh) * | 2014-09-12 | 2016-04-06 | 沈阳化工大学 | 利用微波加热制备直接染料黄11的方法 |
| CN104312207B (zh) * | 2014-09-12 | 2016-08-24 | 沈阳化工大学 | 一种提高直接黄11上染率的方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE631379A (fr) * | ||||
| US2821550A (en) * | 1956-12-27 | 1958-01-28 | Gen Aniline & Film Corp | Process of preparing 4-nitro-2-stilbene sulfonic acid salts |
| US3122529A (en) * | 1959-11-16 | 1964-02-25 | Gen Aniline & Film Corp | Preparation of stilbene azo dyes |
| US3905949A (en) * | 1965-04-29 | 1975-09-16 | Du Pont | Stilbene azo lithium salt dyes |
| US3557079A (en) * | 1967-02-01 | 1971-01-19 | Allied Chem | Production of stilbene azo dyes |
| US3547774A (en) * | 1967-06-30 | 1970-12-15 | Toms River Chemical Corp | Process for forming a solubilized stilbene dye and a process for forming colored paper therewith |
| BE757179A (fr) * | 1970-10-07 | 1971-04-07 | Althouse Tertre | Compositions tinctoriales pour papier |
| US3953419A (en) * | 1972-03-09 | 1976-04-27 | Sandoz Ltd. | Salts of stilbene-azo and stilbene-azoxy dyes and process for their preparation |
| GB1409326A (en) * | 1973-01-09 | 1975-10-08 | Ici Ltd | Preparation of stilbene-azo dyes |
| DE2451219C3 (de) * | 1974-10-29 | 1978-06-22 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung konzentrierter Lösungen von Farbstoffen und Farbstoffzwischenprodukten und Verwendung der Lösungen |
| DE2527703A1 (de) * | 1975-06-21 | 1977-01-13 | Bayer Ag | Verfahren zur herstellung konzentrierter loesungen anionischer farbstoffe |
| DE2820487A1 (de) * | 1978-05-10 | 1979-11-15 | Bayer Ag | Farbstoffloesungen von stilbenazofarbstoffen |
-
1980
- 1980-03-21 FR FR8006319A patent/FR2478658A1/fr active Granted
-
1981
- 1981-02-23 US US06/237,566 patent/US4310331A/en not_active Expired - Fee Related
- 1981-03-11 BE BE0/204084A patent/BE887894A/fr not_active IP Right Cessation
- 1981-03-17 DE DE19813110261 patent/DE3110261A1/de not_active Withdrawn
- 1981-03-18 GB GB8108397A patent/GB2072213B/en not_active Expired
- 1981-03-20 NL NL8101367A patent/NL8101367A/nl not_active Application Discontinuation
- 1981-03-20 NO NO810966A patent/NO810966L/no unknown
- 1981-03-20 AU AU68596/81A patent/AU6859681A/en not_active Abandoned
- 1981-03-20 DK DK127681A patent/DK127681A/da not_active Application Discontinuation
- 1981-03-20 JP JP3968581A patent/JPS56145956A/ja active Pending
- 1981-03-20 SE SE8101802A patent/SE8101802L/ not_active Application Discontinuation
- 1981-03-20 FI FI810868A patent/FI810868L/fi not_active Application Discontinuation
- 1981-03-20 ES ES500580A patent/ES8206603A1/es not_active Expired
- 1981-03-20 BR BR8101666A patent/BR8101666A/pt unknown
- 1981-03-20 IT IT67382/81A patent/IT1144320B/it active
- 1981-03-20 ZA ZA00811876A patent/ZA811876B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| IT1144320B (it) | 1986-10-29 |
| JPS56145956A (en) | 1981-11-13 |
| ZA811876B (en) | 1982-04-28 |
| US4310331A (en) | 1982-01-12 |
| SE8101802L (sv) | 1981-09-22 |
| GB2072213B (en) | 1983-06-02 |
| NL8101367A (nl) | 1981-10-16 |
| DE3110261A1 (de) | 1982-02-18 |
| AU6859681A (en) | 1981-09-24 |
| DK127681A (da) | 1981-09-22 |
| ES500580A0 (es) | 1982-08-16 |
| FR2478658A1 (fr) | 1981-09-25 |
| ES8206603A1 (es) | 1982-08-16 |
| FR2478658B1 (fr) | 1983-10-07 |
| IT8167382A0 (it) | 1981-03-20 |
| BE887894A (fr) | 1981-09-11 |
| FI810868L (fi) | 1981-09-22 |
| BR8101666A (pt) | 1981-09-22 |
| GB2072213A (en) | 1981-09-30 |
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