NO20080768L - Fremgangsmate for fremstilling av 5-aminolevulinsyre-hydroklorid - Google Patents
Fremgangsmate for fremstilling av 5-aminolevulinsyre-hydrokloridInfo
- Publication number
- NO20080768L NO20080768L NO20080768A NO20080768A NO20080768L NO 20080768 L NO20080768 L NO 20080768L NO 20080768 A NO20080768 A NO 20080768A NO 20080768 A NO20080768 A NO 20080768A NO 20080768 L NO20080768 L NO 20080768L
- Authority
- NO
- Norway
- Prior art keywords
- aminolevulinic acid
- aqueous solution
- acid hydrochloride
- preparation
- solution
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/40—Separation; Purification
- C07C227/42—Crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/40—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
- C07C229/22—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated the carbon skeleton being further substituted by oxygen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Abstract
Fremgangsmåte for fremstilling av 5-aminolevulinsyre-hydrokloridkrystaller som omfatter: å adsorbere 5-aminolevulinsyren inneholdt i en 5-aminolevulinsyre-råoppløsning på en kationbytterharpiks; deretter å desorbere syren med en vandig oppløsning inneholdende ammoniumioner under benyttelse av en endring i den elektriske ledningsevne eller pH i oppløsningen som resulterer fra desorpsjonen som en indeks på utvinning for derved å oppnå en vandig oppløsning av høyren 5-aminolevulinsyre; å tilsette kloridioner til den vandige oppløsningen; og å blande et organisk løsningsmiddel dermed.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2005273398A JP4977349B2 (ja) | 2005-09-21 | 2005-09-21 | 5−アミノレブリン酸塩酸塩の製造方法 |
PCT/JP2006/317570 WO2007034673A1 (ja) | 2005-09-21 | 2006-09-05 | 5-アミノレブリン酸塩酸塩の製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
NO20080768L true NO20080768L (no) | 2008-06-18 |
NO338789B1 NO338789B1 (no) | 2016-10-17 |
Family
ID=37888726
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
NO20080768A NO338789B1 (no) | 2005-09-21 | 2008-02-12 | Fremgangsmåte for fremstilling av 5-aminolevulinsyreoppløsning |
Country Status (10)
Country | Link |
---|---|
US (1) | US8148574B2 (no) |
EP (2) | EP2402306B1 (no) |
JP (1) | JP4977349B2 (no) |
KR (1) | KR101131683B1 (no) |
CN (2) | CN102702002B (no) |
AU (1) | AU2006293300B2 (no) |
CA (1) | CA2618603C (no) |
DK (1) | DK2402306T3 (no) |
NO (1) | NO338789B1 (no) |
WO (1) | WO2007034673A1 (no) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPWO2007052787A1 (ja) * | 2005-11-07 | 2009-04-30 | 協和発酵バイオ株式会社 | 結晶またはアモルファスの洗浄方法および洗浄装置 |
CN101624350B (zh) * | 2009-08-06 | 2012-11-07 | 浙江大学 | 一种5-氨基乙酰丙酸盐酸盐的结晶方法 |
KR102127104B1 (ko) | 2013-03-22 | 2020-06-26 | 네오 Ala 가부시키가이샤 | 5-아미노레불린산 또는 그 염의 제조 방법 |
US20160297747A1 (en) * | 2015-04-08 | 2016-10-13 | Invista North America S.A.R.L. | Materials and methods for the selective recovery of monovalent products from aqueous solutions using continuous ion exchange |
CN108440319B (zh) * | 2018-04-26 | 2021-05-18 | 爱斯特(成都)生物制药股份有限公司 | 一种制备盐酸氨基乙酰丙酸的方法 |
CN111517973B (zh) * | 2019-02-02 | 2023-08-04 | 中国科学院天津工业生物技术研究所 | 一种从发酵液中制备5-氨基乙酰丙酸盐酸盐的生产工艺及其应用 |
CN113149854A (zh) * | 2021-03-23 | 2021-07-23 | 海安艾拉新材料有限公司 | 一种5-氨基乙酰丙酸盐酸盐晶型及其制备方法 |
CN113912508A (zh) * | 2021-08-31 | 2022-01-11 | 新泰市佳禾生物科技有限公司 | 一种从发酵液中分离纯化5-氨基乙酰丙酸的方法 |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3221008A (en) * | 1962-01-30 | 1965-11-30 | Merck & Co Inc | Ion exchange process for the recovery of ionic organic substances |
US3846490A (en) * | 1972-02-24 | 1974-11-05 | N Aronova | Method of producing zeta-aminolevulinic acid hydrochloride |
JPS4892328A (no) * | 1972-03-17 | 1973-11-30 | ||
JPS60139656A (ja) * | 1983-12-27 | 1985-07-24 | Ajinomoto Co Inc | リジン製造法 |
JPH0676355B2 (ja) * | 1985-07-29 | 1994-09-28 | 三井東圧化学株式会社 | グリシンとl−セリンの分離方法 |
JPS62111954A (ja) | 1985-11-09 | 1987-05-22 | Japan Spectroscopic Co | アミノレブリン酸の合成法 |
JPH01148193A (ja) * | 1987-12-04 | 1989-06-09 | Daicel Chem Ind Ltd | 5−アミノレブリン酸の製造法 |
JPH0267256A (ja) * | 1988-09-02 | 1990-03-07 | Bio-Le Kk | カルニチンおよびカルニチンニトリルの単離精製法 |
JPH0276841A (ja) | 1988-09-09 | 1990-03-16 | Osaka Organic Chem Ind Ltd | アミノレブリン酸類の製造法 |
JPH0655147B2 (ja) * | 1989-03-31 | 1994-07-27 | 株式会社クボタ | 5―アミノレブリン酸の製法 |
JPH05184376A (ja) * | 1992-01-17 | 1993-07-27 | Shimizu Corp | 5−アミノレブリン酸の生産方法 |
DE4228084C1 (de) | 1992-08-24 | 1993-12-23 | Suedzucker Ag | Verfahren zur Herstellung von N-Acylderivaten der 5-Aminolävulinsäure sowie des Hydrochlorids der freien Säure |
JPH06277081A (ja) * | 1992-11-19 | 1994-10-04 | Shimizu Corp | メタン生成細菌による5−アミノレブリン酸の生産方法 |
JPH07188133A (ja) | 1993-12-27 | 1995-07-25 | Asahi Chem Ind Co Ltd | δ−アミノレブリン酸またはその同族体の製造法 |
JPH09316041A (ja) | 1996-05-24 | 1997-12-09 | Sagami Chem Res Center | δ−アミノレブリン酸の製造法および5−ニトロ−4−オキソペンタン酸 |
JP3026190B2 (ja) | 1997-05-27 | 2000-03-27 | 株式会社コスモ総合研究所 | 5−アミノレブリン酸生産微生物及びこれを用いた5−アミノレブリン酸の製造法 |
WO2005100300A1 (ja) * | 2004-03-30 | 2005-10-27 | Cosmo Oil Co., Ltd. | 5-アミノレブリン酸塩、その製造方法及びその用途 |
KR100655041B1 (ko) * | 2005-05-09 | 2006-12-06 | 주식회사 라이트팜텍 | 감마-아미노레불리닉 엑시드 염산염의 신규한 제조 방법 |
-
2005
- 2005-09-21 JP JP2005273398A patent/JP4977349B2/ja active Active
-
2006
- 2006-09-05 US US12/063,883 patent/US8148574B2/en not_active Expired - Fee Related
- 2006-09-05 EP EP11183090.7A patent/EP2402306B1/en not_active Not-in-force
- 2006-09-05 CN CN201210159974.5A patent/CN102702002B/zh not_active Expired - Fee Related
- 2006-09-05 EP EP06797470.9A patent/EP1927586B1/en not_active Not-in-force
- 2006-09-05 CN CN2006800344722A patent/CN101268036B/zh not_active Expired - Fee Related
- 2006-09-05 WO PCT/JP2006/317570 patent/WO2007034673A1/ja active Application Filing
- 2006-09-05 CA CA2618603A patent/CA2618603C/en not_active Expired - Fee Related
- 2006-09-05 AU AU2006293300A patent/AU2006293300B2/en not_active Ceased
- 2006-09-05 KR KR1020087003548A patent/KR101131683B1/ko active IP Right Grant
- 2006-09-05 DK DK11183090.7T patent/DK2402306T3/da active
-
2008
- 2008-02-12 NO NO20080768A patent/NO338789B1/no not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
KR20080045680A (ko) | 2008-05-23 |
JP4977349B2 (ja) | 2012-07-18 |
JP2007084466A (ja) | 2007-04-05 |
EP1927586A4 (en) | 2010-04-14 |
AU2006293300B2 (en) | 2012-06-14 |
EP2402306B1 (en) | 2014-05-21 |
EP1927586A1 (en) | 2008-06-04 |
US8148574B2 (en) | 2012-04-03 |
CA2618603A1 (en) | 2007-03-29 |
CN101268036B (zh) | 2013-01-09 |
AU2006293300A1 (en) | 2007-03-29 |
CA2618603C (en) | 2013-04-09 |
NO338789B1 (no) | 2016-10-17 |
CN101268036A (zh) | 2008-09-17 |
EP2402306A1 (en) | 2012-01-04 |
US20090036709A1 (en) | 2009-02-05 |
KR101131683B1 (ko) | 2012-03-28 |
EP1927586B1 (en) | 2016-04-27 |
CN102702002A (zh) | 2012-10-03 |
WO2007034673A1 (ja) | 2007-03-29 |
CN102702002B (zh) | 2015-10-21 |
DK2402306T3 (da) | 2014-06-30 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
CHAD | Change of the owner's name or address (par. 44 patent law, par. patentforskriften) |
Owner name: COSMO ALA CO., JP |
|
MM1K | Lapsed by not paying the annual fees |