MX362603B - Procedimiento de preparacion de compuestos de pirazol n-sustituidos. - Google Patents

Procedimiento de preparacion de compuestos de pirazol n-sustituidos.

Info

Publication number
MX362603B
MX362603B MX2013014980A MX2013014980A MX362603B MX 362603 B MX362603 B MX 362603B MX 2013014980 A MX2013014980 A MX 2013014980A MX 2013014980 A MX2013014980 A MX 2013014980A MX 362603 B MX362603 B MX 362603B
Authority
MX
Mexico
Prior art keywords
preparation
pyrazole compounds
substituted pyrazole
oxidant
pyrazole
Prior art date
Application number
MX2013014980A
Other languages
English (en)
Other versions
MX2013014980A (es
Inventor
James Timothy Bristow
Original Assignee
Rotam Agrochem Int Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rotam Agrochem Int Co Ltd filed Critical Rotam Agrochem Int Co Ltd
Publication of MX2013014980A publication Critical patent/MX2013014980A/es
Publication of MX362603B publication Critical patent/MX362603B/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/44—Oxygen and nitrogen or sulfur and nitrogen atoms
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Catalysts (AREA)
  • Cephalosporin Compounds (AREA)

Abstract

Se proporciona un procedimiento de preparación de derivados de sulfinilpirazol de fórmula (I) que comprende oxidar un compuesto amino-4-mercapto-1H-pirazol (II) sustituido con un oxidante en ausencia de ácido trifluoroperacético. El peróxido de hidrógeno es un oxidante particularmente preferido y se lleva a cabo en presencia de wolframato de sodio y ácido clorhídrico como catalizador.
MX2013014980A 2011-09-14 2012-09-12 Procedimiento de preparacion de compuestos de pirazol n-sustituidos. MX362603B (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
BRPI1104747-0A BRPI1104747B1 (pt) 2011-09-14 2011-09-14 Process for the preparation of n-substituted pyrazole compounds
PCT/CN2012/081295 WO2013037291A1 (en) 2011-09-14 2012-09-12 Process for the preparation of n-substituted pyrazole compounds

Publications (2)

Publication Number Publication Date
MX2013014980A MX2013014980A (es) 2014-09-01
MX362603B true MX362603B (es) 2019-01-25

Family

ID=47882617

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2013014980A MX362603B (es) 2011-09-14 2012-09-12 Procedimiento de preparacion de compuestos de pirazol n-sustituidos.

Country Status (9)

Country Link
US (1) US9334241B2 (es)
CN (1) CN103044332B (es)
AR (1) AR087825A1 (es)
BR (1) BRPI1104747B1 (es)
CO (1) CO6870043A2 (es)
EC (1) ECSP13013103A (es)
MX (1) MX362603B (es)
TW (1) TWI564292B (es)
WO (1) WO2013037291A1 (es)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2516446A (en) * 2013-07-22 2015-01-28 Rotam Agrochem Int Co Ltd Process for the preparation of n-substituted pyrazole compounds and products of the same
JP2021502991A (ja) * 2017-11-15 2021-02-04 アダマ・マクテシム・リミテッド ５−アミノ−１−（２，６−ジクロロ−４−トリフルオロメチル−フェニル）−４−エチルスルファニル−１ｈ−ピラゾール−３−カルボニトリル及び関連化合物の合成

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4343832A1 (de) 1993-12-22 1995-06-29 Bayer Ag Substituierte 1-Arylpyrazole
JP4640290B2 (ja) 2005-11-21 2011-03-02 日産自動車株式会社 ワーク移し替えのための方法及びシステム
CN101168529B (zh) * 2006-10-24 2011-03-23 温州大学 氟虫腈、乙虫腈及其衍生物的合成方法
FR2925493B1 (fr) 2007-12-19 2011-09-30 Vetoquinol Procede de preparation du fipronil et d'analogues de celui-ci.
CN101250158B (zh) * 2008-04-02 2011-12-07 湖南化工研究院 一种氟虫腈的制备方法
CN101554607A (zh) 2008-04-13 2009-10-14 李寿海 不缠绕不粘堵柔性物料破碎机
CN101544607B (zh) * 2009-04-30 2011-08-10 宁波中化化学品有限公司 一种含三氟甲基亚磺酰基的1-芳基吡唑化合物的合成方法
CN101628895B (zh) * 2009-07-21 2011-02-09 扬州天和药业有限公司 一种苯基吡唑衍生物氧化成氟虫腈的制备方法
AU2010311536A1 (en) * 2009-10-30 2012-05-31 Basf Se Process for the preparation of 4-sulfinyl-pyrazole derivatives
CN101723898B (zh) * 2009-11-25 2011-08-31 北京颖新泰康国际贸易有限公司 一种5-氨基-3-氰基-1-(2,6-二氯-4-三氟甲基苯基)-4-三氟甲基亚磺酰基吡唑的制备方法
AU2010100310A4 (en) 2010-01-25 2010-05-06 Keki Hormusji Gharda A process for manufacturing 5-amino-1-(2, 6-dichloro-4-trifluoromethyl phenyl) - 3-cyano-4-trifluoromethyl sulphinyl pyrazole
CN101955460B (zh) * 2010-08-25 2012-12-12 北京颖泰嘉和生物科技有限公司 一种制备5-氨基-3-氰基-1-（2,6-二氯-4-三氟甲基苯基）-4-三氟甲基亚磺酰基吡唑的方法

Also Published As

Publication number Publication date
TW201321359A (zh) 2013-06-01
WO2013037291A1 (en) 2013-03-21
MX2013014980A (es) 2014-09-01
AR087825A1 (es) 2014-04-23
ECSP13013103A (es) 2014-01-31
BRPI1104747A2 (pt) 2013-08-13
US20140350267A1 (en) 2014-11-27
CN103044332A (zh) 2013-04-17
BRPI1104747B1 (pt) 2017-11-28
US9334241B2 (en) 2016-05-10
TWI564292B (zh) 2017-01-01
CN103044332B (zh) 2016-08-24
CO6870043A2 (es) 2014-02-20

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