MA61721A1 - Procédé de régénération cyclique de déchets de phosphate de fer et application correspondante - Google Patents
Procédé de régénération cyclique de déchets de phosphate de fer et application correspondanteInfo
- Publication number
- MA61721A1 MA61721A1 MA61721A MA61721A MA61721A1 MA 61721 A1 MA61721 A1 MA 61721A1 MA 61721 A MA61721 A MA 61721A MA 61721 A MA61721 A MA 61721A MA 61721 A1 MA61721 A1 MA 61721A1
- Authority
- MA
- Morocco
- Prior art keywords
- iron phosphate
- iron
- precipitant
- preparation
- corresponding application
- Prior art date
Links
- 229910000398 iron phosphate Inorganic materials 0.000 title abstract 10
- WBJZTOZJJYAKHQ-UHFFFAOYSA-K iron(3+) phosphate Chemical compound [Fe+3].[O-]P([O-])([O-])=O WBJZTOZJJYAKHQ-UHFFFAOYSA-K 0.000 title abstract 10
- 238000000034 method Methods 0.000 title abstract 5
- 239000002699 waste material Substances 0.000 title abstract 3
- 230000008929 regeneration Effects 0.000 title abstract 2
- 238000011069 regeneration method Methods 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 abstract 4
- BMTOKWDUYJKSCN-UHFFFAOYSA-K iron(3+);phosphate;dihydrate Chemical compound O.O.[Fe+3].[O-]P([O-])([O-])=O BMTOKWDUYJKSCN-UHFFFAOYSA-K 0.000 abstract 3
- DPTATFGPDCLUTF-UHFFFAOYSA-N phosphanylidyneiron Chemical compound [Fe]#P DPTATFGPDCLUTF-UHFFFAOYSA-N 0.000 abstract 3
- 239000002244 precipitate Substances 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 1
- 238000005265 energy consumption Methods 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/37—Phosphates of heavy metals
- C01B25/375—Phosphates of heavy metals of iron
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
- B09B3/00—Destroying solid waste or transforming solid waste into something useful or harmless
- B09B3/80—Destroying solid waste or transforming solid waste into something useful or harmless involving an extraction step
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G49/00—Compounds of iron
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/005—Preliminary treatment of scrap
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/54—Reclaiming serviceable parts of waste accumulators
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
- H01M2004/028—Positive electrodes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/84—Recycling of batteries or fuel cells
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Crystallography & Structural Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Removal Of Specific Substances (AREA)
- Fertilizers (AREA)
- Compounds Of Iron (AREA)
Abstract
La présente invention concerne un procédé de régénération cyclique de déchets de phosphate de fer et une application correspondante. Le procédé consiste à : mélanger et dissoudre des déchets de phosphate de fer et une liqueur acide pour obtenir une solution de fer-phosphore ; prélever une petite partie de la solution de fer-phosphore pour préparer un précipitant de phosphate de fer ; puis ajouter le précipitant de phosphate de fer dans la solution de fer-phosphore restante pour une réaction afin d'obtenir un précipité de phosphate de fer dihydraté ; utiliser une partie du précipité de phosphate de fer dihydraté en tant que précipitant pour la réaction dans le lot suivant ; et préparer le reste du précipité de phosphate de fer dihydraté en phosphate de fer anhydre. Selon la présente invention, le précipitant de phosphate de fer est préparé pour être utilisé pour la préparation subséquente de phosphate de fer, le phosphate de fer à chaque fois préparé peut être utilisé pour la préparation suivante du phosphate de fer et le procédé est un procédé de préparation simple, n'a besoin de liqueur alcaline que dans un étage de préparation du précipitant, n'utilise pas de liqueur alcaline lors de la production subséquente, est plus respectueux de l'environnement, présente une uniformité de produit élevée, un faible coût, une productivité élevée, une faible consommation d'énergie et est approprié pour une production industrielle à grande échelle.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202110365978.8A CN113044824B (zh) | 2021-04-06 | 2021-04-06 | 磷酸铁废料循环再生的方法及其应用 |
PCT/CN2021/142510 WO2022213676A1 (fr) | 2021-04-06 | 2021-12-29 | Procédé de régénération cyclique de déchets de phosphate de fer et application correspondante |
Publications (1)
Publication Number | Publication Date |
---|---|
MA61721A1 true MA61721A1 (fr) | 2024-01-31 |
Family
ID=76517451
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MA61721A MA61721A1 (fr) | 2021-04-06 | 2021-12-29 | Procédé de régénération cyclique de déchets de phosphate de fer et application correspondante |
Country Status (9)
Country | Link |
---|---|
US (1) | US20240021903A1 (fr) |
CN (1) | CN113044824B (fr) |
DE (1) | DE112021006151T5 (fr) |
ES (1) | ES2950678R1 (fr) |
GB (1) | GB2620057A (fr) |
HU (1) | HUP2200267A2 (fr) |
MA (1) | MA61721A1 (fr) |
MX (1) | MX2023011731A (fr) |
WO (1) | WO2022213676A1 (fr) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113044824B (zh) * | 2021-04-06 | 2023-04-11 | 广东邦普循环科技有限公司 | 磷酸铁废料循环再生的方法及其应用 |
CN113428848A (zh) * | 2021-07-19 | 2021-09-24 | 四川大学 | 一种电池级磷酸铁的循环制备工艺 |
CN116675197B (zh) * | 2022-02-23 | 2024-09-03 | 中国科学院过程工程研究所 | 一种从废磷酸铁锂正极粉提锂后铁磷渣制备磷酸铁的方法 |
CN114852983A (zh) * | 2022-04-14 | 2022-08-05 | 湖北大学 | 一种从回收废旧锂电池的副产物磷铁废渣中提取电池级磷酸铁的方法 |
CN114524572B (zh) * | 2022-04-24 | 2022-07-12 | 深圳永清水务有限责任公司 | 一种磷酸铁生产所产生的废水综合处理方法 |
CN115367722B (zh) * | 2022-08-03 | 2023-10-27 | 宜都兴发化工有限公司 | 磷铁矿制备磷酸铁的方法 |
CN115490219B (zh) * | 2022-09-02 | 2024-03-12 | 广东邦普循环科技有限公司 | 磷酸铁及其合成工艺、系统以及应用 |
CN115676790B (zh) * | 2022-10-28 | 2024-04-02 | 贵州川恒化工股份有限公司 | 一种高振实球形电池级磷酸铁的制备方法 |
CN115650192A (zh) * | 2022-11-02 | 2023-01-31 | 四川顺应动力电池材料有限公司 | 一种红土镍矿高铁渣制备高纯磷酸铁的方法 |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106684485B (zh) * | 2016-12-19 | 2020-04-21 | 天齐锂业股份有限公司 | 酸浸法回收处理废旧磷酸铁锂正极材料的方法 |
CN108101014A (zh) * | 2018-01-31 | 2018-06-01 | 贵州仁聚业科技股份有限公司 | 用黄磷副产磷铁渣制备磷酸铁的方法 |
CN109761209A (zh) * | 2019-03-06 | 2019-05-17 | 深圳海纳百川科技有限公司 | 一种磷酸铁的生产工艺及其生产设备 |
CN110683528B (zh) * | 2019-10-17 | 2021-03-23 | 湖南雅城新材料有限公司 | 一种磷酸铁废料的再生方法 |
CN112357899B (zh) * | 2020-11-23 | 2022-04-22 | 湖南金源新材料股份有限公司 | 一种废旧磷酸铁锂电池的综合回收利用方法 |
CN112499609A (zh) * | 2020-12-03 | 2021-03-16 | 广东邦普循环科技有限公司 | 利用废磷酸铁锂正极粉提锂渣制备磷酸铁的方法和应用 |
CN112520718B (zh) * | 2020-12-04 | 2022-08-26 | 南昌航空大学 | 一种从提锂渣酸浸液中选择性回收电池级磷酸铁的方法 |
CN113044824B (zh) * | 2021-04-06 | 2023-04-11 | 广东邦普循环科技有限公司 | 磷酸铁废料循环再生的方法及其应用 |
-
2021
- 2021-04-06 CN CN202110365978.8A patent/CN113044824B/zh active Active
- 2021-12-29 ES ES202390110A patent/ES2950678R1/es active Pending
- 2021-12-29 MX MX2023011731A patent/MX2023011731A/es unknown
- 2021-12-29 GB GB2315158.2A patent/GB2620057A/en active Pending
- 2021-12-29 WO PCT/CN2021/142510 patent/WO2022213676A1/fr active Application Filing
- 2021-12-29 HU HU2200267A patent/HUP2200267A2/hu unknown
- 2021-12-29 DE DE112021006151.8T patent/DE112021006151T5/de active Pending
- 2021-12-29 MA MA61721A patent/MA61721A1/fr unknown
-
2023
- 2023-09-28 US US18/373,966 patent/US20240021903A1/en active Pending
Also Published As
Publication number | Publication date |
---|---|
GB202315158D0 (en) | 2023-11-15 |
GB2620057A (en) | 2023-12-27 |
ES2950678R1 (es) | 2024-07-31 |
HUP2200267A2 (hu) | 2023-01-28 |
CN113044824B (zh) | 2023-04-11 |
DE112021006151T5 (de) | 2023-09-28 |
US20240021903A1 (en) | 2024-01-18 |
CN113044824A (zh) | 2021-06-29 |
MX2023011731A (es) | 2023-12-15 |
ES2950678A2 (es) | 2023-10-11 |
WO2022213676A1 (fr) | 2022-10-13 |
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