KR960705905A - 이형제, 이 이형제로부터 수득되는 경화피막 및 이 이형제를 사용한 성형방법(mold-release agent, cured coating film prepared therefrom, and method of molding with said agent) - Google Patents

이형제, 이 이형제로부터 수득되는 경화피막 및 이 이형제를 사용한 성형방법(mold-release agent, cured coating film prepared therefrom, and method of molding with said agent)

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Publication number
KR960705905A
KR960705905A KR1019960702691A KR19960702691A KR960705905A KR 960705905 A KR960705905 A KR 960705905A KR 1019960702691 A KR1019960702691 A KR 1019960702691A KR 19960702691 A KR19960702691 A KR 19960702691A KR 960705905 A KR960705905 A KR 960705905A
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South Korea
Prior art keywords
carbon atoms
group
release agent
silicon
containing compound
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KR1019960702691A
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English (en)
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KR100254839B1 (ko
Inventor
마사유끼 야마나
도모히로 호소미
히로또시 사까시따
마사또 가시와기
Original Assignee
이노우에 노리유끼
다이낑고오교 가부시끼가이샤
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Publication of KR960705905A publication Critical patent/KR960705905A/ko
Application granted granted Critical
Publication of KR100254839B1 publication Critical patent/KR100254839B1/ko

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    • C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
    • C10M105/76—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing silicon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C33/00—Moulds or cores; Details thereof or accessories therefor
    • B29C33/56—Coatings, e.g. enameled or galvanised; Releasing, lubricating or separating agents
    • B29C33/60—Releasing, lubricating or separating agents
    • B29C33/62—Releasing, lubricating or separating agents based on polymers or oligomers
    • B29C33/64—Silicone
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Abstract

식:R1 nSiR2 4-n〔식 중, R1은
(여기서, R3, R4는 각각 탄소원자수 1~4의 탄화수소기이다), R2는 탄소원자수 1~4의 탄화수소기 또는 할로겐화 탄화수소기, n은 3 또는 4를 나타낸다]로 표시되는 규소함유 화합물과, 1분자내에 수산기 또는 알콕시기를 2개 이상 갖는 규소 및/또는 불소함유 화합물로 이루어지는 이형제로서, 이형성능이 뛰어나고, 이형수명이 긴 동시에, 성형품의 표면 마무리성을 양호하게 하고, 성형품의 2차 가공성에 영향을 미치지 않는 이형제를 제공한다.

Description

이형제, 이 이형제로부터 수득되는 경화피막 및 이 이형제를 사용한 성형방법(MOLDRELESE AGENT, CURED COATING FILM PREPARED THEREFROM, AND METHOD OF MOLDING WITH SAID AGENT)
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (7)

  1. (A)로서의 일반식(Ⅰ) :
    R1 nSiR2 4-n(I)
    〔식 중, R1은(여기서, R3R4는 각각 탄소원자수 1~4의 탄화수소기이다), R2는 탄소원자수 1~4의 탄화수소기 또는 할로겐화 탄화수소기, n은 3 또는 4를 나타낸다.]로 표시되는 규소화합물, (B)로서 1분자내에 수산기 또는 알콕시기를 2개 이상 갖는 규소 및/또는 불소함유 화합물로 이루어지는 이형제.
  2. 제1항에 있어서, 규소함유 화합물(A)와 규소 및/또는 불소함유 화합물(B)와의 중량비가 1/99~80/20인 이형제.
  3. 제1항 또는 2항에 있어서, 규소함유 화합물(A)이 일반식(Ⅱ) :
    R1 nSiR2 4-n(Ⅱ)
    〔식 중, R1은(여기서, R R는 각각 탄소원자수 1~4의 탄화수소기이다), R는 탄소원자수 1~4의 탄화수소기 또는 할로겐화 탄화수소기, n은 3 또는 4를 나타낸다.]로 표시되는 화합물인 이형제.
  4. 제1항 내지 3항 중 어느 하나에 있어서, 규소 및/또는 불소함유 화합물(B)이 일반식(Ⅲ)
    RfA4A5(Ⅲ)
    (식 중, Rf는 탄소원자수 6~21의 퍼플루오로 알킬기, A4는 탄소원자수 1~6의 알킬렌기, A5는을 나타낸다)로 표시되는 화합물 20중량% 이상과 일반식(Ⅳ) :
    A6OA7A8(Ⅳ)
    (식 중, A6은 수소원자 또는 탄소원자수 1~4의 단화수소기, A7은 1~6의 알킬렌기, A8은을 나타낸다)로 표시되는 화합물 20중량% 이상을 공중합 성분으로서 함유하여 이루어지는 수평균 분자량이 1000 이상인 공중합체, 일반식(Ⅴ):
    〔식 중, j는 양의 정수, k는 0 또는 양의 정수, j+k의 평균은 10 이상, 바람직하게는 20~5000, X1, X2는 -OH, OR12, -R13NH2-R14OH, -R15COOH, -R15SH 또는 -R12, X3는 -OH, -OR12, R13NH2, -R14OH, -R15COOH 또는 -R15SH(단, k가 0일 때 X1, X2는 함께 -OH 또는 -OR12, k가 0이 아닐 때 X1, X2, X3의 적어도 2개는 -OH 또는 -OR12, R12는 탄소원자수 1~4의 알킬기, 할로겐화 알킬기 또는 페닐기, R13은 탄소원자수 1~10의 알킬렌기 또는 R16NHCH2CH2-(R16은 탄소원자수 1~4의 알킬렌기), R14는
    (단, a는 0 또는 1~15의 정수, b는 0 또는 1~15의 정수, c는 1~10의 정수, d는 1~5의 정수), R15는 탄소원자수 1~10의 알킬렌기), R5, R6, R7, R8, R16, R11은 탄소원자수 1~4의 알킬기, 할로겐화 알킬기 또는 페닐기를 나타낸다〕로 표시되는 화합물, 일반식(Ⅵ):
    Y1OCH2R16O-R18-R17CH2OY2(Ⅵ)
    〔식 중, Y1, Y2는 각각 수소원자 또는 탄소원자수 1~4의 탄화수소기, R16은 -CF2-, -CF2CF2- 또는, R17은 -CF2-, -CF2CF2- 또는, R18은로 이루어지는 군으로부터 선택된 구조단위의 적어도 1종(R16은또는 -CF2CF2CF2-, s1+s2+s3은 평균이 5 이상, 바람직하게 10~200이다)을 나타낸다〕로 표시되는 화합물 및 일반식(Ⅶ)
    RfA1Si(OA2)s6A3-s6(Ⅶ)
    (식중, Rf는 탄소원자수 6~21의 퍼플루오로알킬기, A1는 탄소원자수 2~6의 알킬렌기, A2는 수소원자 또는 탄소원자수 1~4의 알킬기, A3은 탄소원자수 1~4의 알킬기, S은 2또는 3을 나타내다)로 표시되는 화합물로 이루어지는 군으로부터 선택된 적어도 1종인 이형제
  5. 제1항 내지 4항 중 어느 한 항에 있어서, 규소 및/또는 불소 함유 화합물(B)이 일반식(Ⅷ)
    (식 중, R5, R6은 각각 탄소원자수 1~4의 알킬기 또는 할로겐화 알킬기 또는 페닐기, X4,X5는 함께 수소원자 또는 탄소원자수 1~4의 알킬기, m은 평균이 10이상, 바람직하게는 20~5000을 나타낸다)로 표시되는 화합물인 이형제.
  6. 제1항 내지 제5항 중 어느 한 항에 기재된 규소함유 화합물과 규소 및/또는 불소함유 화합물을 형내면에 도포하여 경화시킴으로써 수득되는 경화피막.
  7. 제1항 내지 제5항 중 어느 한 항에 기재된 규소함유 화합물과 규소 및/또는 불소함유 화합물을 형내면에 도포하여 경화시킴으로써 수득되는 경화피막을 형성시킨 후, 이 형내에 성형용 조성물을 충전하여 성형품을 성형하고, 이 형으로부터 성형품을 이형하는 것으로 이루어지는 성형방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019960702691A 1993-11-22 1994-11-18 이형제, 이 이형제로부터 수득되는 경화피막 및 이이형제를 사용한 성형방법 KR100254839B1 (ko)

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