KR920004291A - 실리카 유리 기재의 제조방법 - Google Patents
실리카 유리 기재의 제조방법 Download PDFInfo
- Publication number
- KR920004291A KR920004291A KR1019910014892A KR910014892A KR920004291A KR 920004291 A KR920004291 A KR 920004291A KR 1019910014892 A KR1019910014892 A KR 1019910014892A KR 910014892 A KR910014892 A KR 910014892A KR 920004291 A KR920004291 A KR 920004291A
- Authority
- KR
- South Korea
- Prior art keywords
- glass
- substrate
- silica
- rod
- silica glass
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/10—Non-chemical treatment
- C03B37/12—Non-chemical treatment of fibres or filaments during winding up
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/012—Manufacture of preforms for drawing fibres or filaments
- C03B37/0128—Manufacture of preforms for drawing fibres or filaments starting from pulverulent glass
- C03B37/01282—Manufacture of preforms for drawing fibres or filaments starting from pulverulent glass by pressing or sintering, e.g. hot-pressing
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/012—Manufacture of preforms for drawing fibres or filaments
- C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
- C03B37/01446—Thermal after-treatment of preforms, e.g. dehydrating, consolidating, sintering
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/012—Manufacture of preforms for drawing fibres or filaments
- C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
- C03B37/016—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD] by a liquid phase reaction process, e.g. through a gel phase
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
- Y02P40/57—Improving the yield, e-g- reduction of reject rates
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S65/00—Glass manufacturing
- Y10S65/901—Liquid phase reaction process
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 본 발명의 제1유형의 실시방법을 기술하는 다이어그램.
제2도는 제1유형에 의해서 제조된 석영 유리 기재의 종단면도.
제3도는 기재를 투명한 유리가 되도록 압밀(consolidation)시키므로써 얻어진 광섬유 예비성형체의 단면도.
Claims (11)
- 실리카 유리 기재의 제조방법에 있어서, 실리카를 주재료로 한 막대를 몰드의 공간부로 삽입시키는 단계; 및 실리카 유리 분말을 순수한 물에 분산시키므로써 얻어지는 슬러리를 유리 막대와 몰드의 내측면사이에 있는 몰딩 공간으로 주입시키므로써, 유리 막대 둘레에 다공성 유리 성형 몸체를 형성시키는 단계; 로 구성되는 실리카 유리 기재의 제조방법.
- 제1항에 있어서, 상기 유리 막대는 화학적인 증기 용착 가수분해법에 의해 제조되는 실리카 유리 기재의 제조방법.
- 제2항에 있어서, 상기 유리 막대는 VAD 방법에 의해 제조되는 실리카 유리 기재의 제조방법.
- 제1항에 있어서, 상기 실리카 분말 재료의 평균 입경은 0.6 내지 20㎛ 범위에 속하는 실리카 유리 기재의 제조방법.
- 제1항에 있어서, 비교적 큰 입경을 갖는 유리 분말 재료의 슬러리는 유리 막대와 이 유리 막대에 보다 가깝게 위치하는 몰드의 내측면사이에 있는 몰딩 공간의 중앙부에 주입되고, 비교적 작은 입경을 갖는 유리 분말 재료의 슬러리는 몰딩 공간의 가장자리부로 주입되는 실리카 유리 기재의 제조방법.
- 제5항에 있어서, 상기 보다 큰 입자 유리 분말 재료의 평균 입경은 1 내지 20㎛이고, 상기 보다 작은 입자 유리 분말 재료의 평균 입경은 0.6 내지 1㎛ 범위인 실리카 유리 기재의 제조방법.
- 제1항에 있어서, 상기 다공성 유리 몸체의 양단부 또는 한단부는 원추형 또는 곡률 반경이 성형 몸체의 외경과 동일하거나 보다 큰 3-차원 굴곡면으로 형성되는 실리카 유리 기재의 제조방법.
- 제1항에 있어서, 상기 실리카 유리 기재는 광섬유 예비 성형체를 제조하기 위하여 사용되는 실리카 유리 기재의 제조방법.
- 순수한 물에 실리카 유리 분말 재료를 분산시키므로써 얻어진 슬러리를 유리 막대와 몰드의 내측면사이에 있는 몰딩 공간으로 주입시키므로써, 다공성 유리 성형 몸체가 유리 막대 둘레에 형성되며, 유리 막대와 다공성 유리몸체를 포함하는, 실리카 유리 기재의 처리 방법에 있어서, 기재 원료를 탈수 및 정제시키는 단계; 이 기재를 He 가스로 충전시키기 위하여 He가스로 노출시키는 단계; 및 이 기재를 He을 함유하는 분위기에서 압밀시키는 단계; 로 구성되는 실리카 유리 기재의 처리방법.
- 제9항에 있어서, 탈수-정제 공정과 기재를 He으로 충전시키기 위한 공정 중간에 전공하에 기재를 가열시키면서 공기를 제거시키는 단계를 포함하는 실리카 유리 기재의 처리방법.
- 제9항에 있어서, 광섬유 예비성형체는 상기 실리카 유리 기재로부터 얻어지는 실리카 유리 기재의 처리방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2-224732 | 1990-08-27 | ||
JP22473290 | 1990-08-27 | ||
JP3-92028 | 1991-04-23 | ||
JP3092028A JPH04321531A (ja) | 1991-04-23 | 1991-04-23 | 光ファイバ用母材の製造方法 |
JP3122752A JPH04325429A (ja) | 1991-04-25 | 1991-04-25 | 光ファイバ用母材の製造方法 |
JP3-122695 | 1991-04-25 | ||
JP3-122752 | 1991-04-25 | ||
JP3122695A JPH04325432A (ja) | 1991-04-25 | 1991-04-25 | 光ファイバ用母材の製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR920004291A true KR920004291A (ko) | 1992-03-27 |
KR940005065B1 KR940005065B1 (ko) | 1994-06-10 |
Family
ID=27467974
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019910014892A KR940005065B1 (ko) | 1990-08-27 | 1991-08-27 | 실리카 유리 기재의 제조방법 |
Country Status (7)
Country | Link |
---|---|
US (1) | US5185020A (ko) |
EP (1) | EP0473104B1 (ko) |
KR (1) | KR940005065B1 (ko) |
AU (1) | AU632240B2 (ko) |
BR (1) | BR9103682A (ko) |
CA (1) | CA2049898C (ko) |
DE (1) | DE69123313T2 (ko) |
Families Citing this family (39)
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US5244485A (en) * | 1991-04-30 | 1993-09-14 | The Furukawa Electric Co., Ltd. | Method of manufacturing a silica glass preform |
CA2088238C (en) * | 1992-01-30 | 1998-08-18 | Masato Oku | Method of manufacturing optical fiber preform |
US5314520A (en) * | 1992-02-12 | 1994-05-24 | The Furukawa Electric Co., Ltd. | Method for manufacturing optical fiber preform |
GB9210327D0 (en) * | 1992-05-14 | 1992-07-01 | Tsl Group Plc | Heat treatment facility for synthetic vitreous silica bodies |
FR2692052A1 (fr) * | 1992-06-09 | 1993-12-10 | Alcatel Cable | Procédé de fabrication d'une multiferrule pour fibres optiques. |
JP2917729B2 (ja) * | 1993-03-03 | 1999-07-12 | 住友電気工業株式会社 | 光ファイバ母材の製造方法 |
US5356447A (en) * | 1993-03-11 | 1994-10-18 | At&T Bell Laboratories | Manufacture of high proof-test optical fiber using sol-gel |
US5344475A (en) * | 1993-03-11 | 1994-09-06 | At&T Bell Laboratories | Manufacture of high proof-test optical fiber using sol-gel |
FR2707285B1 (fr) * | 1993-07-06 | 1995-08-11 | Alcatel Fibres Optiques | Préforme pour fibre optique, procédé de fabrication d'une telle préforme et fibre optique obtenue à partir de cette préforme. |
FR2712278B1 (fr) * | 1993-11-08 | 1995-12-29 | Alcatel Cable Interface | Procédé de réalisation d'une ébauche pour multiférule en verre de silice, et ébauche ainsi obtenue. |
DE69514867D1 (de) * | 1994-06-10 | 2000-03-09 | Ceramoptec Gmbh | Verfahren zur Herstellung Mikroporöse Siliziumdioxyd-Faser mit Siliziumdioxyd Mantel |
US5531956A (en) * | 1995-04-27 | 1996-07-02 | Institute Of Gas Technology | Ribbed electrodes for molten carbonate fuel cells |
ITNO990004A1 (it) | 1999-03-08 | 2000-09-08 | Gel Design And Engineering S R | Processo sol-gel per la produzione di manufatti contenenti e aderentiad un inserto cilindrico incomprimibile e manufatti cosi' ottenuti. |
DE19943103A1 (de) | 1999-09-09 | 2001-03-15 | Wacker Chemie Gmbh | Hochgefüllte SiO2-Dispersion, Verfahren zu ihrer Herstellung und Verwendung |
DE10131494A1 (de) * | 2001-07-02 | 2003-05-28 | Nanogate Technologies Gmbh | Partikuläre Beschichtung |
US7125912B2 (en) * | 2001-10-09 | 2006-10-24 | Simax Technologies, Inc. | Doped sol-gel materials and method of manufacture utilizing reduced mixing temperatures |
US7026362B2 (en) * | 2001-10-09 | 2006-04-11 | Simax Technologies, Inc. | Sol-gel process utilizing reduced mixing temperatures |
JP4117641B2 (ja) * | 2001-11-26 | 2008-07-16 | ジャパンスーパークォーツ株式会社 | 合成石英粉の処理方法およびその石英ガラス製品 |
AU2002224966A1 (en) * | 2001-12-21 | 2003-07-09 | Pirelli & C. S.P.A. | Process for manufacturing a micro-structured optical fibre |
US20030147606A1 (en) * | 2002-02-01 | 2003-08-07 | Shiho Wang | Sol-gel-based optical preforms and methods of manufacture |
US20040194511A1 (en) * | 2002-02-01 | 2004-10-07 | Chih-Hsing Cheng | Sol-gel-derived halogen-doped glass |
US6928220B2 (en) * | 2002-02-01 | 2005-08-09 | Simax Technologies, Inc. | Sol-gel-derived optical fiber preform and method of manufacture |
US7001568B2 (en) * | 2002-02-01 | 2006-02-21 | Simax Technologies, Inc. | Method of removing liquid from pores of a sol-gel monolith |
US7000885B2 (en) * | 2002-02-01 | 2006-02-21 | Simax Technologies, Inc. | Apparatus and method for forming a sol-gel monolith utilizing multiple casting |
US6829908B2 (en) * | 2002-02-27 | 2004-12-14 | Corning Incorporated | Fabrication of inclusion free homogeneous glasses |
US20040226319A1 (en) * | 2003-05-15 | 2004-11-18 | Macchesney John Burnette | Chemical powder deposition method for the manufacture of optical fiber preforms and optical fibers |
ATE499330T1 (de) * | 2003-05-30 | 2011-03-15 | Prysmian Spa | Verfahren und vorrichtung zur bildung einer vorform für eine mikrostrukturierte lichtleitfaser |
KR100617713B1 (ko) * | 2004-02-12 | 2006-08-28 | 삼성전자주식회사 | 다공 광섬유의 제조방법 |
DE102004052312A1 (de) * | 2004-08-23 | 2006-03-02 | Heraeus Quarzglas Gmbh & Co. Kg | Beschichtetes Bauteil aus Quarzglas sowie Verfahren zur Herstellung des Bauteils |
CN101052599B (zh) * | 2004-08-28 | 2012-05-16 | 赫罗伊斯石英玻璃股份有限两合公司 | 用于接合部件的接合剂、用于接合由硅酸含量高的材料制备的部件的方法,和根据该方法获得的部件组件 |
DE102004054392A1 (de) | 2004-08-28 | 2006-03-02 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren zum Verbinden von Bauteilen aus hochkieselsäurehaltigem Werkstoff, sowie aus derartigen Bauteilen zusammengefügter Bauteil-Verbund |
US8578736B2 (en) * | 2008-09-23 | 2013-11-12 | Corning Incorporated | Soot radial pressing for optical fiber overcladding |
US8904828B2 (en) * | 2008-10-30 | 2014-12-09 | Corning Incorporated | Methods for forming cladding portions of optical fiber preform assemblies |
EP2226301A1 (en) * | 2009-02-22 | 2010-09-08 | Silitec Fibers SA | Method for producing and processing a preform, preform and optical fiber |
US10011517B2 (en) * | 2013-06-06 | 2018-07-03 | Corning Incorporated | Optical preforms and methods for forming the same |
US10494291B2 (en) | 2014-10-23 | 2019-12-03 | Corning Incorporated | Hygroscopic additives for silica soot compacts and methods for forming optical quality glass |
WO2016138052A1 (en) | 2015-02-27 | 2016-09-01 | Corning Incorporated | Methods for strengthening silica soot compacts with nanoparticles |
WO2017011002A1 (en) | 2015-07-15 | 2017-01-19 | Heraeus Quartz America Llc | Process for joining opaque fused quartz to clear fused quartz |
US10562804B2 (en) | 2016-03-18 | 2020-02-18 | Corning Incorporated | Burner design for particle generation |
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US2288661A (en) * | 1939-09-07 | 1942-07-07 | Hartford Empire Co | Method of slip casting composite refractories |
US2290671A (en) * | 1940-03-26 | 1942-07-21 | Gen Electric | Insulated conducting member and method of applying the insulation |
CA1058814A (en) * | 1973-11-13 | 1979-07-24 | Sumitomo Electric Industries, Ltd. | Method for producing a tubular multi-layered porous barrier |
JPS55100231A (en) * | 1979-01-19 | 1980-07-31 | Hitachi Ltd | Production of optical fiber base material |
US4419115A (en) * | 1981-07-31 | 1983-12-06 | Bell Telephone Laboratories, Incorporated | Fabrication of sintered high-silica glasses |
US4605428A (en) * | 1984-08-03 | 1986-08-12 | At&T Bell Laboratories | Sintered high-silica glass and articles comprising same |
JPS62288130A (ja) * | 1986-06-04 | 1987-12-15 | Seiko Epson Corp | 石英系光フアイバ用母材の製造方法 |
DE3765887D1 (de) * | 1986-08-29 | 1990-12-06 | American Telephone & Telegraph | Verfahren zum bekleiden von optischen vorformen mit glasruss. |
US4789389A (en) * | 1987-05-20 | 1988-12-06 | Corning Glass Works | Method for producing ultra-high purity, optical quality, glass articles |
US4775401A (en) * | 1987-06-18 | 1988-10-04 | American Telephone And Telegraph Company, At&T Bell Laboratories | Method of producing an optical fiber |
JPH0764574B2 (ja) * | 1987-08-26 | 1995-07-12 | 古河電気工業株式会社 | 棒状石英系ガラス母材の製造方法 |
JPH0615162B2 (ja) * | 1988-04-22 | 1994-03-02 | トヨタ自動車株式会社 | スリップキャスティング成形方法 |
JP2653828B2 (ja) * | 1988-05-20 | 1997-09-17 | 日本電信電話株式会社 | 光ファイバ母材の製造方法 |
US4940675A (en) * | 1988-06-17 | 1990-07-10 | Corning Incorporated | Method for making low-expansion glass article of complex shape |
-
1991
- 1991-08-26 AU AU82720/91A patent/AU632240B2/en not_active Ceased
- 1991-08-26 US US07/749,900 patent/US5185020A/en not_active Expired - Fee Related
- 1991-08-26 CA CA002049898A patent/CA2049898C/en not_active Expired - Fee Related
- 1991-08-27 EP EP91114336A patent/EP0473104B1/en not_active Expired - Lifetime
- 1991-08-27 BR BR919103682A patent/BR9103682A/pt not_active IP Right Cessation
- 1991-08-27 KR KR1019910014892A patent/KR940005065B1/ko not_active IP Right Cessation
- 1991-08-27 DE DE69123313T patent/DE69123313T2/de not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
AU8272091A (en) | 1992-03-19 |
AU632240B2 (en) | 1992-12-17 |
CA2049898C (en) | 1996-06-25 |
KR940005065B1 (ko) | 1994-06-10 |
BR9103682A (pt) | 1992-05-19 |
EP0473104B1 (en) | 1996-11-27 |
CA2049898A1 (en) | 1992-02-28 |
DE69123313T2 (de) | 1997-04-24 |
EP0473104A1 (en) | 1992-03-04 |
DE69123313D1 (de) | 1997-01-09 |
US5185020A (en) | 1993-02-09 |
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