KR910006239A - 4급화된 이미다졸린 직물 컨디쇼닝 화합물을 제조하는 방법 - Google Patents

4급화된 이미다졸린 직물 컨디쇼닝 화합물을 제조하는 방법 Download PDF

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KR910006239A
KR910006239A KR1019900014026A KR900014026A KR910006239A KR 910006239 A KR910006239 A KR 910006239A KR 1019900014026 A KR1019900014026 A KR 1019900014026A KR 900014026 A KR900014026 A KR 900014026A KR 910006239 A KR910006239 A KR 910006239A
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quaternizing agent
liquid reaction
reaction mixture
formula
ester compound
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KR1019900014026A
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English (en)
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로사리오-쟌센 테레사
대일 리치텐월터 글렌
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리챠드 챨스 위트
더 프록터 앤드 갬블 캄파니
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Publication of KR910006239A publication Critical patent/KR910006239A/ko

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
    • C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
    • C07D239/06—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/04—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
    • C07D233/06—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, directly attached to ring carbon atoms
    • C07D233/08—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, directly attached to ring carbon atoms with alkyl radicals, containing more than four carbon atoms, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/04—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
    • C07D233/06—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, directly attached to ring carbon atoms
    • C07D233/08—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, directly attached to ring carbon atoms with alkyl radicals, containing more than four carbon atoms, directly attached to ring carbon atoms
    • C07D233/12—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, directly attached to ring carbon atoms with alkyl radicals, containing more than four carbon atoms, directly attached to ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D233/18—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D243/00—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms
    • C07D243/04—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 3

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

내용 없음

Description

4급화된 이미다졸린 직물 컨디쇼닝 화합물을 제조하는 방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (14)

  1. (a)일반식(I)의 이미다졸린 에스테르 화합물의 무수용융물을 형성시키고, (b)언급된 무수 용융물을 일반식 R2X 또는 R2 2X (여기서, R2는 (C1내지 C3)알킬 또는 벤질 그룹이고, X는 할라이드 또는 설페이트이다)의 4급화제와 접촉시켜 액체 반응 혼합불(여기서, 액체 반응 혼합물을 저급 알코올 용매를 함유하지 않은 상태로 유지시킨다)을 형성시킨 후, (c) 언급된 액체 반응 혼합물은 약 50내지 약 100℃의 온도범위에서 실질적으로 모든 언급된 4급화제가 언급된 이미다졸린 에스테르 화합물과 반응되기에 충분한 시간동안 무수 조건하에 유지시켜 일반식(Ⅱ) 또는 일반식(Ⅲ)의 4급화된 이미다졸린 에스테르 화합물 또는 이의 혼합물을 제조함을 특징으로 하여, 이미다졸린 에스테르 화합물을 4급화시키는 방법.
    상기식에서, R 및 R1은 독립적으로 (C11내지 C21)하이드로카르빌 그룹이고, m 및 n은 독립적으로 2내지 4이며, R2및 X는 상기에서 정의한 바와 같다.
  2. 제1항에 있어서, R 및 R1이 독립적으로 (C13내지 C17)알킬 그룹이고 m 및 n은 각각 2인 방법.
  3. 제2항에 있어서, 4급화제가 (C1내지 C3)할라이드인 방법.
  4. 제3항에 있어서, 4급화제가 메틸 클로라이드인 방법.
  5. 제2항에 있어서, 4급화제가 디메틸 설페이트인 방법.
  6. 제4항에 있어서, 액체 반응 혼합물을 약 70내지 약 85℃의 온도 범위에서 약 1 내지 약 4시간동안 유지시키는 방법.
  7. (a)일반식(I) 의 이미다졸린 에스테르 화합물의 무수용융물을 형성시키고, (b) 언급된 무수 용융물을 일반식 R2X 또는 R2 2X (여기서, R2는 (C1내지 C3)알킬 또는 벤질 그룹이고, X는 할라이드 또는 설페이트이다)의 4급화제와 접촉시켜 액체 반응 혼합물(여기서, 액체 반응 혼합물을 저급 알코올 용매를 함유하지 않은 상태로 유지시킨다)을 형성시킨 후, (c) 언급된 액체 반응 혼합물은 약 50내지 약 100℃의 온도범위에서 실질적으로 모든 언급된 4급화제가 언급된 이미다졸린 에스테르 화합물과 반응되기에 충분한 시간동안 무수 조건하에 유지시켜 일반식(Ⅱ) 또는 일반식(Ⅲ)의 4급화된 이미다졸린 에스테르 화합물 또는 이의 혼합물을 제조함을 특징으로 하여, 4급화된 이미다졸린 에스테르 화합물 및 임의의 이미다졸린 에스테르 화합물을 함유하는 반응생성물을 제조하는 방법.
    상기식에서, R 및 R1은 독립적으로 (C11내지 C21)하이드로카르빌 그룹이고, m 및 n은 독립적으로 2내지 4이며, R2및 X는 상기에서 정의한 바와 같다.
  8. 제7항에 있어서, R 및 R1이 독립적으로 (C13내지 C17)알킬 그룹이고 m 및 n은 각각 2인 방법.
  9. 제8항에 있어서, 4급화제가 (C1내지 C3)할라이드인 방법.
  10. 제9항에 있어서, 4급화제가 메틸 클로라이드인 방법.
  11. 제8항에 있어서, 4급화제가 디메틸 실페이트인 방법.
  12. 제10항에 있어서, 액체 반응 혼합물을 약 70내지 약약 85℃의 온도 범위에서 약 1 내지 약 4시간동안 유지시키는 방법.
  13. 제12항에 있어서, 약 30내지 약 90몰 %의 4급화제를 무수 용융물과 접촉시키는 방법.
  14. 제13항에 있어서, 약 40 내지 약 80몰 %의 4급화제를 무수 용융물과 접촉시키는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019900014026A 1989-09-06 1990-09-06 4급화된 이미다졸린 직물 컨디쇼닝 화합물을 제조하는 방법 KR910006239A (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US403541 1989-09-06
US07/403,541 US4954635A (en) 1989-09-06 1989-09-06 Process for preparing quaternized imidazoline fabric conditioning compounds

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KR910006239A true KR910006239A (ko) 1991-04-27

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Country Link
US (1) US4954635A (ko)
EP (1) EP0416686B1 (ko)
JP (1) JPH03135959A (ko)
KR (1) KR910006239A (ko)
CN (1) CN1050716A (ko)
AU (1) AU648512B2 (ko)
BR (1) BR9004422A (ko)
CA (1) CA2023877A1 (ko)
DE (1) DE69013826D1 (ko)
ES (1) ES2063248T3 (ko)
NZ (1) NZ235164A (ko)
PE (1) PE4391A1 (ko)

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CN105829600A (zh) * 2013-12-27 2016-08-03 陶氏环球技术有限责任公司 适用于改进水分管理且提供抗微生物保护的包括衍生自直链四胺的季双咪唑啉化合物的纺织品处理组合物
JP2019535692A (ja) 2016-11-09 2019-12-12 コベストロ、ドイチュラント、アクチエンゲゼルシャフトＣｏｖｅｓｔｒｏ Ｄｅｕｔｓｃｈｌａｎｄ Ａｇ トリアリール−有機ボレートを製造するための方法
KR102489809B1 (ko) 2016-11-09 2023-01-20 코베스트로 도이칠란트 아게 트리아릴 유기보레이트의 제조 방법
TW201833122A (zh) 2016-11-09 2018-09-16 德商科思創德意志股份有限公司 製備三芳基有機硼酸鹽的方法

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BR9004422A (pt) 1991-09-10
CA2023877A1 (en) 1991-03-07
AU6222590A (en) 1991-03-14
AU648512B2 (en) 1994-04-28
EP0416686A2 (en) 1991-03-13
EP0416686A3 (en) 1991-03-20
ES2063248T3 (es) 1995-01-01
US4954635A (en) 1990-09-04
CN1050716A (zh) 1991-04-17
DE69013826D1 (de) 1994-12-08
JPH03135959A (ja) 1991-06-10
PE4391A1 (es) 1991-02-05
EP0416686B1 (en) 1994-11-02
NZ235164A (en) 1992-06-25

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