KR880007590A - 플루오렌-함유 비스페놀의 글리시딜에테르 - Google Patents

플루오렌-함유 비스페놀의 글리시딜에테르 Download PDF

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Publication number
KR880007590A
KR880007590A KR870013977A KR870013977A KR880007590A KR 880007590 A KR880007590 A KR 880007590A KR 870013977 A KR870013977 A KR 870013977A KR 870013977 A KR870013977 A KR 870013977A KR 880007590 A KR880007590 A KR 880007590A
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South Korea
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phenyl
fluorene
epoxypropoxy
substituted
ortho
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KR870013977A
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English (en)
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죤 슐츠 윌리암
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도날드 밀러 셀
미네소타 마이닝 앤드 매뉴 팩츄 어링 컴패니
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Publication of KR880007590A publication Critical patent/KR880007590A/ko

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/02—Polycondensates containing more than one epoxy group per molecule
    • C08G59/04—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof
    • C08G59/06—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols
    • C08G59/063—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols with epihalohydrins
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
    • C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
    • C07D303/24—Ethers with hydroxy compounds containing no oxirane rings with polyhydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
    • C08G59/22—Di-epoxy compounds
    • C08G59/24—Di-epoxy compounds carbocyclic
    • C08G59/245—Di-epoxy compounds carbocyclic aromatic

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Epoxy Resins (AREA)
  • Epoxy Compounds (AREA)

Abstract

내용 없음.

Description

플루오렌-함유 비스페놀의 글리시딜에테르
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (10)

  1. 오르토-치환된-4-히드록시페닐플루오렌의 글리시딜에테르.
  2. 제1항에 있어서, 하기식(Ⅰ)의 글리시딜에테르.
    상기식에서 n은 0내지 3, R은 하기식의 2가 유기기인데
    상기식에서 R0은 각각 수소와 에폭시기-함유 화합물의 중합에 불황성인가, 1-6 탄소원자의 직쇄와 측쇄알킬, 페닐, 니트로, 아세틸과 트리메틸실릴에서 선택되며 ; R1, R2, R3과 R4각각은 수소, 1-6탄소 원자의 직쇄 또는 측쇄알킬, 페닐과 할로겐에서 선택되는데 R1. R2, R3과 R4중 최소한 하나가 1-6탄소 원자의 직쇄 또는 측쇄 알킬, 페닐 또는 할로겐 일때 디글리시딜 에테르의 에폭시당량은 최대가 약 500이다.
  3. 제2항에 있어서, R0이 할로겐, 1-6 탄소원자의 직쇄 또는 측쇄 알킬기, 페닐, 니트로, 아세틸 또는 트리메틸 실릴인 글리시딜 에테르.
  4. 제1항 내지 제3항의 어느 한항에 있어서, 9,9-비스[3-메틸-4-(2,3-에폭시프로폭시)페닐] 플루오렌, 9,9-비스[3,5-디메틸-4-(2,3-에폭시프로폭시)페닐] 플루오렌, 9,9-비스[3-클로로-4-(2,3-에폭시프로폭시)페닐] 플로오렌, 9-[4-(2,3-에폭시프로폭시)페닐]-9-[3-메틸-4-(2,3-에폭시프로폭시)페닐]플루오렌, 9-[3-메틸-4-(2,3-에폭시프로폭시)페닐]-9-[3,5-디메틸-4-(2.3-에폭시프로폭시)페닐]플루오렌과 9,9-비스[3,5-디브로모-4-(2,3-에폭시프로폭시)페닐]플루오렌에서 선택된 글리시딜에테르.
  5. a) 최소한 25중량 %가 제1항내지 제4항에 따른 오르토-치환된-4-히드록시페닐플루오렌의 최소한 하나의 글리시딜 에테르인 최소한 하나의 경화성에 폭시수지. b) 에폭시수지 경화제 c) 그외의 방향족 폴리에폭사이드가 75 중량%로 구성된 경화성 에폭시 수지 조성물.
  6. 제5항에 있이서, 방향족 폴리에폭사이드가 폴리히드릭페놀의 폴리글리시딜에테르, 방향족 카르복실산의 글리시딘 에스테르, 글리시딜아미노벤젠과 글리시딜아미노-글리시딜옥시-벤젠 중 최소한 하나인 조성물.
  7. 제6항에 있어서, 폴리히드릭페놀의 폴리글리시딜 에테르가 최소한 하나의 펜단트 카르복실기를 함유하는 비스페놀의 디글리시딜에테르인 조성물.
  8. a) 최소한 하나의 오르토-치환된 페놀과 선택적으로 비치환 된 페놀을 플루오 레논 또는 치환된 플루오레논으로 축합하여 최소한 하나의 오르토-치환된 비스페놀을 제조하고 b) 생성된 오르토-치환된 비스페놀을 과량의 에피클로 히드린과 반응시켜 9,9-비스(오르토-치환된-4-히드록시-페닐)플루오렌의 최소한 하나의 디글리시딜 에테르를 제조하고 c) 생성된 9,9-비스(오르토-치환된-4-히드록시-페닐) 플루오렌의 최소한 하나의 디글리시딜 에테르를 분리하는 것으로 구성된 특허청구범위 제1내지 제7항의 화합물의 제조방법.
  9. 제5항 내지 제7항의 경화성 수지 조성물의 경화된 수지.
  10. 제5항 내지 제7항과 제9항중 어느 한항의 경화성 또는 경화된 수지의 층을 함유하거나 그로서 함침된 기관.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR870013977A 1986-12-09 1987-12-08 플루오렌-함유 비스페놀의 글리시딜에테르 KR880007590A (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US939574 1986-12-09
US06/939,574 US4707534A (en) 1986-12-09 1986-12-09 Glycidylethers of fluorene-containing bisphenols

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KR880007590A true KR880007590A (ko) 1988-08-27

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Country Status (6)

Country Link
US (1) US4707534A (ko)
EP (1) EP0274209A1 (ko)
JP (1) JPS63165378A (ko)
KR (1) KR880007590A (ko)
AU (1) AU596241B2 (ko)
CA (1) CA1273949A (ko)

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CA1273949A (en) 1990-09-11
AU596241B2 (en) 1990-04-26
US4707534A (en) 1987-11-17
AU8127687A (en) 1988-06-09
JPS63165378A (ja) 1988-07-08
EP0274209A1 (en) 1988-07-13

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