KR840006365A - 용배부제 실리콘 조절된 박리 조성물 - Google Patents

용배부제 실리콘 조절된 박리 조성물 Download PDF

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KR840006365A
KR840006365A KR1019830004258A KR830004258A KR840006365A KR 840006365 A KR840006365 A KR 840006365A KR 1019830004258 A KR1019830004258 A KR 1019830004258A KR 830004258 A KR830004258 A KR 830004258A KR 840006365 A KR840006365 A KR 840006365A
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composition
base
viscosity
silanol
functional
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KR1019830004258A
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KR860000603B1 (ko
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폴 엑크베르그 리차드 (외 1)
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삼손 헬프 고트
제너럴 일렉트릭 캄파니
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
    • C08L83/04—Polysiloxanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/49—Phosphorus-containing compounds
    • C08K5/51—Phosphorus bound to oxygen
    • C08K5/52—Phosphorus bound to oxygen only
    • C08K5/524—Esters of phosphorous acids, e.g. of H3PO3
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • C08G77/08—Preparatory processes characterised by the catalysts used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/32—Post-polymerisation treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/01—Hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/06—Ethers; Acetals; Ketals; Ortho-esters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/10—Esters; Ether-esters
    • C08K5/11—Esters; Ether-esters of acyclic polycarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/20—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for coatings strippable as coherent films, e.g. temporary coatings strippable as coherent films
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • C08G77/10—Equilibration processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/14—Polysiloxanes containing silicon bound to oxygen-containing groups
    • C08G77/16—Polysiloxanes containing silicon bound to oxygen-containing groups to hydroxyl groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Silicon Polymers (AREA)
  • Paints Or Removers (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Adhesive Tapes (AREA)
  • Detergent Compositions (AREA)
  • Compression, Expansion, Code Conversion, And Decoders (AREA)
  • Optical Communication System (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Paper (AREA)

Abstract

내용 없음

Description

용매부제 실리콘 조절된 박리 조성물
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (10)

  1. (1) SiH기 또는 실라놀-작용기를 중량비로 20%까지 가지며, 25℃에서 점도가 약 50내지 약 100,000인 디오 가노폴리실옥산 염기성 폴리머
    (2) 불포화 유기반응 희석제에 분산된, R3SiO½및 SiO½ 단위의 공중합체(여기에서 R은 같거나 다른 탄수 2이하의 일가 탄화수소 래디칼)
    (3) SiH기를 중량비로 100비를 가지며, 25℃에서 점도 25내지 1000CPS인 폴리메틸 하이드로겐실옥산 유체 가교 결합제
    (4) 상기한 공중합체, 상기한 첨가제 및 상기한 가교 결합제 사이에서 첨가 경화 하이드로실레이션 반응을 축진시키는 효율적인 량의 귀금속 촉매
    (5) 상기한 실리콘 조절된 박리 조성물의 열 경화 온도 이하의 온도에서 상기한 하이드로실레이션 반응을 효율적으로 수행하기 위한 불포화 탄소-탄소를 포함하는 상당한 량의 디알킬 카복실 에스테르로 구성되는 것을 특징으로 한 용매부재 실리콘 조절된 박리 조성물.
  2. 제1항에 있어서, 상기한 염기성 폴리머가 비닐-쇄 정지된 폴리디메틸비닐실옥산 공중합체인 조성물.
  3. 제1항에 있어서, 상기한 공중합체 성분(2)은 응축되지 않은 실리콘 MQ수지이고 상기한 반응 희석제는 디부틸말리에이트, 데실비닐에테르, 도데실비닐에테르, 캄펜, C(16내지 18) 알파-올레핀 및 메타-비스이소프로페닐벤젠으로 구성된 그룹에서 선택한 반응희석제인 조성물.
  4. 제1항에 있어서, 상기한 공중합체 성분(2)이 C(16내지 18) 알파-올레핀에 분산시킨 비닐 실리콘 MQ수지인 조성물.
  5. 제1항에 있어서, 소량의 비닐-함유 폴리실옥산 고무를 함께 포함하는 조성물.
  6. 제1항에 있어서, 염기성 폴리머가 실라놀 작용기이고 옥타메틸사이클로테트라실옥산 및 물의 KOH-촉매 평형에 의해서 제조되고, 소량의 트리스(2-클로로에틸) 포스파이트의 부가에 의하여 중화된 조성물.
  7. 사이클릭폴리실옥산 단량체 및 물의 염기-촉매 평형에 의하여 제조되고, 상기한 염기를 트리스)2-클로로에틸) 포스파이트의 부가로 중화하여 25℃에서 점도 약 50내지 100,000 CPS이며 SiOH기가 중량비 약 20%이하인 것을 특징으로 하는 잠재 응축 촉매없는 실라놀-작용기 디오가노폴리실옥산 조성물.
  8. 제7항에 있어서, 상기한 염기가 KOH이고 상기한 사이클릭 폴리실옥산 단량체는 옥타메틸사이클로 테트라실옥산인 살라놀 작용기 디오가노폴리실옥산 조성물.
  9. (a)염기 존재하에 사이클릭 폴리실옥산 단량체 및 물의 평형시키고 (b)트리스(2-클로로에틸) 포스파이트로 염기를 중화시킴을 특징으로 하는 SiOH작용기가 20중량%이하이고 25℃에서 점도50내지 100,000CPS인 잠재 응축 촉매없는 실라놀-작용기 디오가노폴리실옥산의 제조방법.
  10. 제9항에 있어서, 상기한 사이클릭 폴리실옥산 단량체인 기본적으로 옥타메틸사이클로 테트라실옥산이고 상기한 염기가 KOH인 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019830004258A 1982-09-10 1983-09-10 용매부재 실리콘 조절된 박리 조성물 KR860000603B1 (ko)

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US41657682A 1982-09-10 1982-09-10
US416,576 1989-10-03

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KR860000603B1 KR860000603B1 (ko) 1986-05-22

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JP (2) JPS5984953A (ko)
KR (1) KR860000603B1 (ko)
AT (2) ATE33847T1 (ko)
BR (1) BR8305030A (ko)
DE (2) DE3376429D1 (ko)
FI (1) FI833113A (ko)

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EP0216376A1 (en) 1987-04-01
EP0216376B1 (en) 1991-08-07
BR8305030A (pt) 1984-04-24
JPH032889B2 (ko) 1991-01-17
DE3382370D1 (de) 1991-09-12
DE3376429D1 (en) 1988-06-01
JPH0138414B2 (ko) 1989-08-14
EP0108208B1 (en) 1988-04-27
FI833113A (fi) 1984-03-11
KR860000603B1 (ko) 1986-05-22
FI833113A0 (fi) 1983-09-01
EP0108208A3 (en) 1984-07-18
JPH0243223A (ja) 1990-02-13
JPS5984953A (ja) 1984-05-16
EP0108208A2 (en) 1984-05-16
ATE33847T1 (de) 1988-05-15
ATE66008T1 (de) 1991-08-15

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