KR830006819A - 실리콘체의 연속 화학증기 침전생성물을 위한 복합 가스막 - Google Patents

실리콘체의 연속 화학증기 침전생성물을 위한 복합 가스막 Download PDF

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KR830006819A
KR830006819A KR1019810002705A KR810002705A KR830006819A KR 830006819 A KR830006819 A KR 830006819A KR 1019810002705 A KR1019810002705 A KR 1019810002705A KR 810002705 A KR810002705 A KR 810002705A KR 830006819 A KR830006819 A KR 830006819A
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윌리암 거스췌 헨리
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죤 엘머 마울러
몬산토 캄파니
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    • C30CRYSTAL GROWTH
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    • C30B25/00Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
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    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B25/00Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
    • C30B25/02Epitaxial-layer growth
    • C30B25/18Epitaxial-layer growth characterised by the substrate
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    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
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    • C01B33/027Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material
    • C01B33/035Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material by decomposition or reduction of gaseous or vaporised silicon compounds in the presence of heated filaments of silicon, carbon or a refractory metal, e.g. tantalum or tungsten, or in the presence of heated silicon rods on which the formed silicon is deposited, a silicon rod being obtained, e.g. Siemens process
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    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B25/00Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
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    • C30B25/00Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
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    • C30B25/00Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
    • C30B25/02Epitaxial-layer growth
    • C30B25/14Feed and outlet means for the gases; Modifying the flow of the reactive gases
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S117/00Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
    • Y10S117/906Special atmosphere other than vacuum or inert

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Abstract

내용 없음

Description

실리콘체의 연속 화학증기 침전 생성물을 위한 복합 가스막
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
본 도면은 본 발명을 실행하는데 유용한 장치를 확대항 것으로써 둘 또는 그 이상의 복합 가스막은 본 발명에 따른 연속공정을 실행하기 위해 연속화학 증기 침전실의 벽을 따라 제공되었다.

Claims (4)

  1. 가스성 실리콘 화합물을 분해시킬 수 있는 온도까지 하나 또는 그 이상의 실리콘 세봉(Silm rod)을 가열시키며; 가열시킨 실리콘 세봉을 화학중기 침전실로 통과시키며; 실리콘 세봉의 표면온도를 가열기구로 약 1000℃ 내지 1300℃까지 유지시키며; 실리콘 세봉을 일반식 SikHmXn의 반응가스와 접촉시키며; 화학증기 침전실 내벽을 따라 첫번째 가스막을 형성시켜, 이 첫번째 막이 반응가스와 역류로 흐르며 반응가스의 입구점에서부터 반대끝으로 실에 들어가도록 하며 ; 반응가스 입구 부근에 내벽실을 따라 두번째 가스막을 분해실까지 형성시키며, 봉이 분해실을 통해 움직이므로써 봉의 표면상에 실리콘을 침전시키며; 및 분해실로부터 생성된 확장 결정성 실리콘체를 회수시킴을 특징으로 하여 결정성 실리콘체를 연속적으로 제조하는 방법.
    상기식에서
    k는 1 내지 2의 수이고, m은 0 내지 6의 수이고, n은 0내지 6의 수이고, X는 할로겐이다.
  2. 용융 실리콘원의 시이드(Seed)결정 작용으로부터 예인실(Pulling chamber)내의 처녀세봉을 예인시키며, 가스성 실리콘 화합물을 분해시킬 수 있는 온도까지 단일결정실리콘 세봉을 가열시키며; 가열된 단일 결정실리콘 세봉을 화학증기 침전실가지 통과시키며; 단일 결정세봉의 표면온도를 가열기루로 약 1000℃내지 1300℃까지 유지시키며, 단일결정 세봉을 일반식 SikHmXn의 반응가스와 접촉시키며; 수소, 헬륨, 네온, 아르곤, 크립톤, 세논 및 라돈을 구성하는 그룹으로부터 선택된 첫번째 가스막을 화학증기 침전실 내벽을 따라 형성시켜, 첫번째 가스막이 역류로 흐르도록 하여 반응가스 입구와 반대역으로 들어가도록 하며; 반응가스 입구부근의 내벽을 따라 수소-염소막을 분해실가지 형성시키며, 봉이 분해실을 통해 움직임으로써 단일 결정실리콘봉의 표면상에 실리콘을 침전시키며 및 분해실로부터 생성된 확장셜정성 실리콘체를 회수시킴을 특징으로 하여 단일결정 실리콘을 연속적으로 제조하는 방법.
    상기식에서
    k는 1내지 2의 수이고, m은 0내지 6의수이고, n은 0내지 6의 수이고, X는 할로겐이다.
  3. 하나 또는 그 이상의 시이드 결정과 용융실리콘 원의 반응으로부터 예인실내의 하나 또는 그 이상의 처녀 실리콘 세봉을 예인시키며, 실리콘세봉을 예열시켜 화학증기 침전실로 도입시키며; 가스성 화합물을 함유하는 실리콘을 분해시킬 수 있는 온도까지 도임된 세봉을 동시에 가열시켜 세봉과 가스성 화합물을 접촉시키며; 수소, 헬륨, 네온, 아르곤, 크립톤, 세논 및 라돈을 구성하는 그룹으로부터 선택된 첫번째 가스막을 화학증기 침전실 내벽을 따라 형성시켜, 첫번재 가스막이 반응가스 흐름과 역류로 흐르도록 하여 반응가스의 도입점으로부터 실의 반대끝으로 도입시키며; 반응가스입구부근의 내벽실을 따라 수소 염소 두번째 가스막을 분해실가지 형성시키며; 봉이 분해실을 통해 움직임으로서 봉의 표면상에 실리콘을 침전시키며; 및 분해실로부터 생성된 확장 결정성 실리콘체를 회수시킴을 특징으로 하여 다결정 실리콘체를 연속적으로 제조하는 방법.
  4. 성장실로부터 세봉을 화학증기 칩전실로 통과하도록 충분한 직경의 좁은 통로를 통하여 증기침전실 하부와 연결된 사웁 끝과 용융 실리콘 원과 연결된 성장실과 저부 끝을 세봉성장실 ; 화학증기 침전실을 통하여 성장실 안으로 아래에 확장되는 회수성 예인기구; 성장실 세봉 가열기구; 화학증기 침전실벽주위에 방사선을 집중시킬 수 있는 기하학적인 노 및 역을 집중시킬 수 있는 투명한 실벽; 가스압력원 기구를 넣을 수 있는 성장실; 반응가스를 화학증기 침전실가지 넣고 내보낼 수 있는 기구; 첫번째 가스막이 반응가스 입구에서부터 실의 반대끝에 위치한 화학증기 침전실을 따라 가스를 흐르도록 하는 안내기구; 반응가스 입구 부근의 화학증기 침전실 내벽을 따라 가스막을 제공하는 두번째 가스막 입구흐름 안내기구; 및 가스봉임장치를 구성하는 화학증기 침전실 상부 끝으로부터 생성되는 실리콘체를 위한 출구기구를 특징으로 하여 결정성 실리콘체를 연속적으로 성장시키기 위한 장치.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019810002705A 1980-07-28 1981-07-25 실리콘 결정체의 연속적 제조방법 KR850001943B1 (ko)

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US06/172,509 US4444812A (en) 1980-07-28 1980-07-28 Combination gas curtains for continuous chemical vapor deposition production of silicon bodies
US172509 1980-07-28

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US4033286A (en) * 1976-07-12 1977-07-05 California Institute Of Technology Chemical vapor deposition reactor
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KR850001943B1 (ko) 1985-12-31
US4444812A (en) 1984-04-24
DE3169538D1 (en) 1985-05-02
EP0045599B1 (en) 1985-03-27
EP0045599A1 (en) 1982-02-10
JPS5751112A (en) 1982-03-25
CA1178179A (en) 1984-11-20

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