KR20240006654A - 황색도 지수 감소 및 안정화를 위한 불포화 에스테르 함유 첨가제 - Google Patents

황색도 지수 감소 및 안정화를 위한 불포화 에스테르 함유 첨가제 Download PDF

Info

Publication number
KR20240006654A
KR20240006654A KR1020237042646A KR20237042646A KR20240006654A KR 20240006654 A KR20240006654 A KR 20240006654A KR 1020237042646 A KR1020237042646 A KR 1020237042646A KR 20237042646 A KR20237042646 A KR 20237042646A KR 20240006654 A KR20240006654 A KR 20240006654A
Authority
KR
South Korea
Prior art keywords
alkyl
meth
ppm
acrylate
composition
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
KR1020237042646A
Other languages
English (en)
Korean (ko)
Inventor
플로리안 츠슌케
플로리안 츠šœ케
안드레아 비트코브스키
아이사 벨라이드 아이트
루돌프 부르크하르트
다니엘 헬무트 쾨니히
슈테펜 크릴
안드레아스 뤼흘링
스펜 발크
브루노 켈러
Original Assignee
룀 게엠베하
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 룀 게엠베하 filed Critical 룀 게엠베하
Publication of KR20240006654A publication Critical patent/KR20240006654A/ko
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/62Use of additives, e.g. for stabilisation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/04Oxygen-containing compounds
    • C08K5/07Aldehydes; Ketones
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54Acrylic acid esters; Methacrylic acid esters
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F20/00Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
    • C08F20/02Monocarboxylic acids having less than ten carbon atoms, Derivatives thereof
    • C08F20/10Esters
    • C08F20/12Esters of monohydric alcohols or phenols
    • C08F20/14Methyl esters, e.g. methyl (meth)acrylate
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/04Oxygen-containing compounds
    • C08K5/13Phenols; Phenolates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/04Oxygen-containing compounds
    • C08K5/13Phenols; Phenolates
    • C08K5/132Phenols containing keto groups, e.g. benzophenones
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/014Additives containing two or more different additives of the same subgroup in C08K

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
KR1020237042646A 2021-05-10 2022-04-29 황색도 지수 감소 및 안정화를 위한 불포화 에스테르 함유 첨가제 Pending KR20240006654A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP21172931 2021-05-10
EP21172931.4 2021-05-10
PCT/EP2022/061442 WO2022238144A1 (de) 2021-05-10 2022-04-29 Ungesättigte ester, enthaltend ein additiv zur reduktion und stabilisierung des gelbwertes

Publications (1)

Publication Number Publication Date
KR20240006654A true KR20240006654A (ko) 2024-01-15

Family

ID=76180846

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020237042646A Pending KR20240006654A (ko) 2021-05-10 2022-04-29 황색도 지수 감소 및 안정화를 위한 불포화 에스테르 함유 첨가제

Country Status (8)

Country Link
US (1) US20250282929A1 (https=)
EP (1) EP4337633A1 (https=)
JP (1) JP2024518080A (https=)
KR (1) KR20240006654A (https=)
CN (1) CN117279885A (https=)
BR (1) BR112023023281A2 (https=)
TW (1) TW202311223A (https=)
WO (1) WO2022238144A1 (https=)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI845945B (zh) * 2021-05-20 2024-06-21 日商三菱化學股份有限公司 單體組成物、甲基丙烯酸系樹脂組成物及樹脂成形體

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2848499A (en) 1956-05-09 1958-08-19 Celanese Corp Preparation of unsaturated aldehydes
DE3106557A1 (de) 1981-02-21 1982-09-16 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von (alpha)-alkylacroleinen
JPS606635A (ja) * 1983-06-24 1985-01-14 Mitsubishi Petrochem Co Ltd 1,2−不飽和カルボン酸および/またはそのエステルの精製法
DE3740293A1 (de) 1987-11-27 1989-06-01 Hoechst Ag Verfahren zur herstellung von alpha-alkylacroleinen
JP3069420B2 (ja) 1991-11-05 2000-07-24 ダイセル化学工業株式会社 反応器および反応方法
US5468899A (en) * 1995-01-11 1995-11-21 Bauer, Jr.; William Process for purifying α,β-unsaturated esters
SG71815A1 (en) 1997-07-08 2000-04-18 Asahi Chemical Ind Method of producing methyl methacrylate
JP3792449B2 (ja) * 1999-09-01 2006-07-05 三菱レイヨン株式会社 メタクリル酸の精製法
DE10144490A1 (de) * 2001-09-10 2003-03-27 Basf Ag Verfahren zur Herstellung von (Meth)acrylsäureestern
JP4076227B2 (ja) 2001-12-21 2008-04-16 旭化成ケミカルズ株式会社 酸化物触媒組成物
JP4173757B2 (ja) 2003-03-26 2008-10-29 ジヤトコ株式会社 ロックアップクラッチの寿命判定方法及びスリップロックアップ領域設定方法並びに寿命判定装置
US7141702B2 (en) 2004-03-26 2006-11-28 Council Of Scientific And Industrial Research Process for the synthesis of α-substituted acroleins
CA2744402C (en) * 2008-12-18 2018-06-05 Lucite International Uk Limited Methyl methacrylate purification process
EP2986589B1 (de) 2013-04-19 2018-03-14 Evonik Röhm GmbH Verfahren zur herstellung von methylmethacrylat
JP6202037B2 (ja) * 2015-04-09 2017-09-27 ダイキン工業株式会社 組成物
TWI715627B (zh) 2015-09-16 2021-01-11 德商羅伊姆公司 含鈉鹽之mma-甲醇混合物的萃取後處理
EP3450422A1 (de) 2017-08-29 2019-03-06 Evonik Röhm GmbH Verfahren zur herstellung optischer formmassen

Also Published As

Publication number Publication date
WO2022238144A1 (de) 2022-11-17
CN117279885A (zh) 2023-12-22
JP2024518080A (ja) 2024-04-24
BR112023023281A2 (pt) 2024-01-23
EP4337633A1 (de) 2024-03-20
US20250282929A1 (en) 2025-09-11
TW202311223A (zh) 2023-03-16

Similar Documents

Publication Publication Date Title
TWI633082B (zh) 製備甲基丙烯醛及其調理/去水以進行直接氧化性酯化的方法
JP5666467B2 (ja) メチルメタクリレート精製方法
FR2934261A1 (fr) Procede de synthese d'esters de l'acide acrylique
JP6824253B2 (ja) メタクロレインをベースとするアルキルメタクリレートからのメタクリル酸の合成
US4828652A (en) Removal of aldehydes from α, β-olefinically unsaturated carboxylic acids
JP2020531673A (ja) 光学成形材料の製造方法
JP6779288B2 (ja) アクリル酸オリゴマーの合成方法
WO2010031949A1 (fr) Procede de fabrication d'acide acrylique bio-ressource de grade polymere a partir de glycerol
KR20180110007A (ko) 이성질체 혼합물로부터의 단량체 제조 방법
JP2015007142A (ja) エチレン性不飽和酸またはそのエステルの製造
DE10144490A1 (de) Verfahren zur Herstellung von (Meth)acrylsäureestern
KR20240006654A (ko) 황색도 지수 감소 및 안정화를 위한 불포화 에스테르 함유 첨가제
FR2957594A1 (fr) Procede de fabrication d'acide acrylique bio-ressource de grade polymere a partir de glycerol
CZ173395A3 (en) Process for preparing biacetyl free of methyl methacrylate
JP2002194022A (ja) (メタ)アクリル酸エステルの精製方法、(メタ)アクリル酸エステルおよび(メタ)アクリル樹脂
KR102362635B1 (ko) 변색 효과에 관하여 안정화된 n,n-디메틸아미노에틸 아크릴레이트 조성물
JP2007045803A (ja) 精製されたメタクリル酸メチルを得る方法
KR101860166B1 (ko) 감소된 비아세틸 함량을 갖는 메틸 메타크릴레이트의 제조 방법
JPH1036309A (ja) 水酸基含有ビニル化合物の安定化剤およびその使用方法

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902