KR102066682B1 - 말론산 이염, 및 말로닐 다이할라이드의 제조 방법 - Google Patents

말론산 이염, 및 말로닐 다이할라이드의 제조 방법 Download PDF

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KR102066682B1
KR102066682B1 KR1020147019199A KR20147019199A KR102066682B1 KR 102066682 B1 KR102066682 B1 KR 102066682B1 KR 1020147019199 A KR1020147019199 A KR 1020147019199A KR 20147019199 A KR20147019199 A KR 20147019199A KR 102066682 B1 KR102066682 B1 KR 102066682B1
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phenyl
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KR20140107420A (ko
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웬밍 장
게리 데이비드 애니스
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에프엠씨 코포레이션
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D471/00Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, at least one ring being a six-membered ring with one nitrogen atom, not provided for by groups C07D451/00 - C07D463/00
    • C07D471/02Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, at least one ring being a six-membered ring with one nitrogen atom, not provided for by groups C07D451/00 - C07D463/00 in which the condensed system contains two hetero rings
    • C07D471/04Ortho-condensed systems
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C55/00Saturated compounds having more than one carboxyl group bound to acyclic carbon atoms
    • C07C55/36Acyl halides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/30Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms containing six-membered aromatic rings
    • C07C57/34Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms containing six-membered aromatic rings containing more than one carboxyl group
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/30Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms containing six-membered aromatic rings
    • C07C57/34Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms containing six-membered aromatic rings containing more than one carboxyl group
    • C07C57/36Phenymalonic acid
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D213/00Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/24Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D213/54Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/55Acids; Esters
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/58Preparation of carboxylic acid halides
    • C07C51/60Preparation of carboxylic acid halides by conversion of carboxylic acids or their anhydrides or esters, lactones, salts into halides with the same carboxylic acid part
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/64Acyl halides
    • C07C57/72Acyl halides containing six-membered aromatic rings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Pyridine Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
KR1020147019199A 2011-12-15 2012-12-13 말론산 이염, 및 말로닐 다이할라이드의 제조 방법 Active KR102066682B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201161570962P 2011-12-15 2011-12-15
US61/570,962 2011-12-15
PCT/US2012/069468 WO2013090547A1 (en) 2011-12-15 2012-12-13 Malonic acid di-salts and a method for preparing malonyl dihalides

Publications (2)

Publication Number Publication Date
KR20140107420A KR20140107420A (ko) 2014-09-04
KR102066682B1 true KR102066682B1 (ko) 2020-01-16

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KR1020147019199A Active KR102066682B1 (ko) 2011-12-15 2012-12-13 말론산 이염, 및 말로닐 다이할라이드의 제조 방법

Country Status (17)

Country Link
US (1) US9108965B2 (https=)
EP (1) EP2791107B1 (https=)
JP (2) JP2015501841A (https=)
KR (1) KR102066682B1 (https=)
CN (1) CN104066713B (https=)
AR (1) AR089221A1 (https=)
AU (1) AU2012352256B2 (https=)
BR (1) BR112014014232B1 (https=)
CA (1) CA2857333A1 (https=)
CO (1) CO7121339A2 (https=)
HU (1) HUE044394T2 (https=)
IL (1) IL232632A (https=)
MX (1) MX352470B (https=)
RU (1) RU2636942C2 (https=)
TW (1) TWI572587B (https=)
WO (1) WO2013090547A1 (https=)
ZA (1) ZA201403383B (https=)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI528899B (zh) * 2010-12-29 2016-04-11 杜邦股份有限公司 中離子性殺蟲劑
RU2638137C2 (ru) 2012-06-21 2017-12-15 Е.И.Дюпон Де Немур Энд Компани Твердые формы внутренней соли пиридопиримидиния
CN105254515A (zh) * 2015-11-13 2016-01-20 浙江汇能生物股份有限公司 一种氯化琥珀胆碱的制备方法
TW201738229A (zh) 2016-04-26 2017-11-01 杜邦股份有限公司 製備n-[(5-嘧啶基)甲基]-2-吡啶胺之方法
US20200062710A1 (en) * 2016-12-06 2020-02-27 Nipppon Kayaku Kabushiki Kaisha Method For Producing 3-(Pyridyl-2-Amino)Propionitrile And Analogues Thereof
JP6916161B2 (ja) * 2018-02-20 2021-08-11 インディアン オイル コーポレーション リミテッド ポリオレフィンポリマー用添加剤および熱可塑性組成物
US12356988B2 (en) 2018-03-05 2025-07-15 Corteva Agriscience Llc Process and intermediates for the preparation of certain mesoionic pesticides
CN108373468B (zh) * 2018-05-18 2019-12-17 武汉工程大学 一种n-2-吡啶-5-嘧啶甲胺的制备方法
CN109020952A (zh) * 2018-11-01 2018-12-18 雅本化学股份有限公司 一种n-2-吡啶基-5-嘧啶甲胺的制备方法
US20250011301A1 (en) 2021-11-10 2025-01-09 Corteva Agriscience Llc Processes for the preparation of certain mesoionic pesticides
EP4573074A1 (en) 2022-08-18 2025-06-25 Corteva Agriscience LLC Process for the preparation and isolation of intermediates of certain mesoionic pesticides
CN116003253A (zh) * 2022-12-31 2023-04-25 上海试四化学品有限公司 一种三氟苯嘧啶中间体2-[3-(三氟甲基)苯基]丙二酸二甲酯的制备方法
CN118359606A (zh) * 2023-01-19 2024-07-19 华东理工大学 三氟苯嘧啶多晶型及其制备方法
CN116715573B (zh) * 2023-06-29 2025-08-19 河北华旭化工有限公司 一种2,2-二甲基丁酰氯的合成方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030153728A1 (en) * 2001-10-02 2003-08-14 Kolb Hartmuth C. Modified safe and efficient process for the environmentally friendly synthesis of lmidoesters
JP2005187368A (ja) * 2003-12-25 2005-07-14 Sumitomo Chemical Co Ltd カルボン酸クロリドの製造方法
WO2011017351A2 (en) * 2009-08-05 2011-02-10 E. I. Du Pont De Nemours And Company Mixtures of mesoionic pesticides

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2290412A1 (fr) * 1974-11-09 1976-06-04 Gema Sa Procede pour la preparation de chlorures d'acide a partir d'esters silyliques
US5358924A (en) 1991-03-21 1994-10-25 Bayer Aktiengesellschaft 3-hydroxy-4-aryl-5-oxo-pyrozoline derivatives, compositions and use
CN1215390A (zh) 1996-04-02 1999-04-28 拜尔公司 取代的苯基酮烯醇杀虫剂及除草剂
DE19649665A1 (de) * 1996-04-02 1997-10-09 Bayer Ag Neue substituierte Phenylketoenole
US6297400B1 (en) * 1999-07-02 2001-10-02 The Clorox Company Synthesis of a tetraamido macrocycle ligand from a novel diamidodiol
JP3824483B2 (ja) * 2000-10-31 2006-09-20 住友ベークライト株式会社 芳香族カルボン酸とその酸塩化物、および合成法
JP4644957B2 (ja) * 2001-03-09 2011-03-09 住友ベークライト株式会社 芳香族カルボン酸及びその酸塩化物誘導体、並びにそれらの合成法
US7060818B2 (en) * 2003-02-21 2006-06-13 Carnegie Mellon University Synthesis of macrocyclic tetraamido compounds and new metal insertion process
JP2004292393A (ja) * 2003-03-27 2004-10-21 Sumitomo Bakelite Co Ltd 芳香族カルボン酸及びその酸塩化物誘導体の合成法
CN100402520C (zh) 2006-07-28 2008-07-16 马启明 2-取代丙二酸钙盐的制备方法及钙盐的用途
RU2373182C2 (ru) * 2007-12-19 2009-11-20 Государственное образовательное учреждение высшего профессионального образования "Курский государственный технический университет" (КурскГТУ) Способ получения малоната и сукцината марганца (ii)
TWI468407B (zh) 2008-02-06 2015-01-11 Du Pont 中離子農藥
UA110924C2 (uk) 2009-08-05 2016-03-10 Е. І. Дю Пон Де Немур Енд Компані Мезоіонні пестициди
US20120122680A1 (en) 2009-08-05 2012-05-17 E.I. Du Pont De Nemours And Company Mesoionic pesticides
KR20120050467A (ko) * 2009-08-05 2012-05-18 이 아이 듀폰 디 네모아 앤드 캄파니 메소이온성 살충제
WO2011091532A1 (en) * 2010-01-28 2011-08-04 Boehringer Ingelheim International Gmbh Hepatitis c inhibitor compounds
TWI528899B (zh) 2010-12-29 2016-04-11 杜邦股份有限公司 中離子性殺蟲劑
WO2012106495A1 (en) 2011-02-03 2012-08-09 E. I. Du Pont De Nemours And Company Mesoionic pesticides

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030153728A1 (en) * 2001-10-02 2003-08-14 Kolb Hartmuth C. Modified safe and efficient process for the environmentally friendly synthesis of lmidoesters
JP2005187368A (ja) * 2003-12-25 2005-07-14 Sumitomo Chemical Co Ltd カルボン酸クロリドの製造方法
WO2011017351A2 (en) * 2009-08-05 2011-02-10 E. I. Du Pont De Nemours And Company Mixtures of mesoionic pesticides

Also Published As

Publication number Publication date
EP2791107A1 (en) 2014-10-22
MX2014006992A (es) 2014-08-01
CA2857333A1 (en) 2013-06-20
MX352470B (es) 2017-11-27
TWI572587B (zh) 2017-03-01
US9108965B2 (en) 2015-08-18
US20140343284A1 (en) 2014-11-20
JP2015501841A (ja) 2015-01-19
HUE044394T2 (hu) 2019-10-28
AR089221A1 (es) 2014-08-06
TW201329037A (zh) 2013-07-16
JP2018058840A (ja) 2018-04-12
AU2012352256A1 (en) 2014-05-29
RU2636942C2 (ru) 2017-11-29
IL232632A0 (en) 2014-06-30
BR112014014232A2 (pt) 2018-05-22
WO2013090547A1 (en) 2013-06-20
AU2012352256B2 (en) 2017-05-25
IL232632A (en) 2017-04-30
ZA201403383B (en) 2015-12-23
RU2014128826A (ru) 2016-02-10
BR112014014232B1 (pt) 2020-01-28
KR20140107420A (ko) 2014-09-04
JP6579399B2 (ja) 2019-09-25
CN104066713B (zh) 2016-08-24
CN104066713A (zh) 2014-09-24
EP2791107B1 (en) 2019-03-13
CO7121339A2 (es) 2014-11-20

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