KR101813898B1 - 에어로겔 재료의 제조방법 및 그 제조를 위한 전구체. - Google Patents
에어로겔 재료의 제조방법 및 그 제조를 위한 전구체. Download PDFInfo
- Publication number
- KR101813898B1 KR101813898B1 KR1020167003001A KR20167003001A KR101813898B1 KR 101813898 B1 KR101813898 B1 KR 101813898B1 KR 1020167003001 A KR1020167003001 A KR 1020167003001A KR 20167003001 A KR20167003001 A KR 20167003001A KR 101813898 B1 KR101813898 B1 KR 101813898B1
- Authority
- KR
- South Korea
- Prior art keywords
- gel
- sol
- hydrophobing
- agent
- catalyst
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04B—GENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
- E04B1/00—Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
- E04B1/62—Insulation or other protection; Elements or use of specified material therefor
- E04B1/74—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls
- E04B1/76—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls specifically with respect to heat only
- E04B1/78—Heat insulating elements
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/157—After-treatment of gels
- C01B33/158—Purification; Drying; Dehydrating
- C01B33/1585—Dehydration into aerogels
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/06—Halogens; Compounds thereof
- B01J27/08—Halides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
- B01J31/0231—Halogen-containing compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
- B01J31/0272—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing elements other than those covered by B01J31/0201 - B01J31/0255
- B01J31/0274—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing elements other than those covered by B01J31/0201 - B01J31/0255 containing silicon
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/145—Preparation of hydroorganosols, organosols or dispersions in an organic medium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/155—Preparation of hydroorganogels or organogels
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Architecture (AREA)
- Acoustics & Sound (AREA)
- Electromagnetism (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Silicon Compounds (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Thermal Insulation (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP13179185.7A EP2832690A1 (de) | 2013-08-02 | 2013-08-02 | Verfahren zur Herstellung eines Aerogelmaterials |
| EP13179185.7 | 2013-08-02 | ||
| PCT/EP2014/066213 WO2015014813A1 (de) | 2013-08-02 | 2014-07-28 | Verfahren zur herstellung eines aerogelmaterials |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20160054462A KR20160054462A (ko) | 2016-05-16 |
| KR101813898B1 true KR101813898B1 (ko) | 2018-01-02 |
Family
ID=48917409
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020167003001A Expired - Fee Related KR101813898B1 (ko) | 2013-08-02 | 2014-07-28 | 에어로겔 재료의 제조방법 및 그 제조를 위한 전구체. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20160258153A1 (enExample) |
| EP (2) | EP2832690A1 (enExample) |
| JP (1) | JP6449279B2 (enExample) |
| KR (1) | KR101813898B1 (enExample) |
| CN (2) | CN114408931A (enExample) |
| AU (1) | AU2014298538B2 (enExample) |
| BR (1) | BR112016002360A2 (enExample) |
| WO (1) | WO2015014813A1 (enExample) |
Families Citing this family (41)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106029760B (zh) * | 2014-02-26 | 2020-08-21 | 日立化成株式会社 | 气凝胶 |
| CH710694B1 (de) * | 2015-02-04 | 2019-05-15 | Rockwool Int | Verfahren zur Herstellung eines Aerogels resp. eines Aerogel-Verbundwerkstoffs, sowie Aerogel resp. Aerogel-Verbundwerkstoff erhältlich nach dem Verfahren. |
| KR101789371B1 (ko) | 2015-02-13 | 2017-10-23 | 주식회사 엘지화학 | 실리카 에어로겔 함유 블랑켓의 제조방법 및 이에 따라 제조된 실리카 에어로겔 함유 블랑켓 |
| GB201502613D0 (en) * | 2015-02-17 | 2015-04-01 | Univ Newcastle | Aerogels |
| DE102015211812A1 (de) | 2015-06-25 | 2016-12-29 | Wacker Chemie Ag | Wirtschaftliches Verfahren zur Herstellung von organisch modifizierten Lyo- oder Aerogelen |
| EP3124443A1 (de) * | 2015-07-28 | 2017-02-01 | D. Swarovski KG | Kontinuierliches sol-gel verfahren zur herstellung von quarzglas |
| KR101931569B1 (ko) | 2015-11-03 | 2018-12-21 | 주식회사 엘지화학 | 소수성의 산화금속-실리카 복합 에어로겔의 제조방법 및 이로부터 제조된 소수성의 산화금속-실리카 복합 에어로겔 |
| KR101774140B1 (ko) * | 2016-01-19 | 2017-09-01 | 주식회사 엘지화학 | 에어로겔 시트의 제조방법 및 장치 |
| KR101953371B1 (ko) | 2016-01-19 | 2019-02-28 | 주식회사 엘지화학 | 에어로겔 시트의 제조방법 및 장치 |
| KR101962207B1 (ko) | 2016-02-17 | 2019-03-27 | 주식회사 엘지화학 | 에어로겔 시트를 포함하는 복합시트 제조방법 및 제조장치 |
| KR101962206B1 (ko) | 2016-02-19 | 2019-03-27 | 주식회사 엘지화학 | 에어로겔 시트를 포함하는 복합시트 제조방법 및 제조장치 |
| KR101968648B1 (ko) * | 2016-02-19 | 2019-04-12 | 주식회사 엘지화학 | 에어로겔 시트의 제조방법 및 장치 |
| KR20170110993A (ko) | 2016-03-24 | 2017-10-12 | 주식회사 엘지화학 | 실리카 에어로겔 제조시스템 |
| FR3050013B1 (fr) * | 2016-04-11 | 2019-08-02 | Saint-Gobain Isover | Fours et produits d'isolation pour fours |
| CH712479A1 (de) * | 2016-05-20 | 2017-11-30 | Flumroc Ag | Anlage und Verfahren zur Herstellung eines Aerogel-Verbundwerkstoffs und Aerogel-Verbundwerkstoff. |
| FR3053263B1 (fr) * | 2016-07-04 | 2018-08-31 | Keey Aerogrl | Procede continu de fabrication d'un aerogel |
| PL3490954T3 (pl) | 2016-07-29 | 2020-06-29 | Evonik Operations Gmbh | Sposób wytwarzania hydrofobowego materiału termoizolacyjnego zawierającego krzemionkę pirogeniczną |
| EP3281920A1 (de) * | 2016-08-12 | 2018-02-14 | D. Swarovski KG | Kontinuierliches sol-gel-verfahren zur herstellung von silicathaltigen gläsern oder glaskeramiken |
| CN108602681B (zh) | 2016-09-12 | 2021-12-17 | 株式会社Lg化学 | 二氧化硅气凝胶的制备方法以及由其制备的二氧化硅气凝胶 |
| KR101942474B1 (ko) * | 2016-11-18 | 2019-01-25 | 주식회사 엘지화학 | 전가수분해된 알킬 폴리실리케이트의 합성방법 |
| WO2018134275A1 (de) | 2017-01-18 | 2018-07-26 | Evonik Degussa Gmbh | Granulares wärmedämmungsmaterial und verfahren zur dessen herstellung |
| CN106955650A (zh) * | 2017-04-01 | 2017-07-18 | 东华大学 | 一种三维多孔框架增强纤维气凝胶材料及其制备方法 |
| DE102017209782A1 (de) | 2017-06-09 | 2018-12-13 | Evonik Degussa Gmbh | Verfahren zur Wärmedämmung eines evakuierbaren Behälters |
| EP3498671A1 (en) * | 2017-12-15 | 2019-06-19 | EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt | Superinsulating silica aerogel with high stiffness and density |
| CN111818994A (zh) * | 2018-03-05 | 2020-10-23 | 赢创运营有限公司 | 生产气凝胶材料的方法 |
| US12030810B2 (en) | 2018-07-17 | 2024-07-09 | Evonik Operations Gmbh | Thermal insulating composition based on fumed silica granulates, processes for its preparation and uses thereof |
| EP3597615A1 (en) | 2018-07-17 | 2020-01-22 | Evonik Operations GmbH | Granular mixed oxide material and thermal insulating composition on its basis |
| CN112424144B (zh) | 2018-07-18 | 2023-02-17 | 赢创运营有限公司 | 在环境压力下使基于二氧化硅的成型隔绝材料体疏水化的方法 |
| CN111039583B (zh) * | 2018-10-11 | 2022-10-11 | 卢孟磊 | 一种低成本快速制备微纳结构气凝胶膨胀珍珠岩的方法 |
| DE102018128410A1 (de) * | 2018-11-13 | 2020-05-14 | Fraunhofer Gesellschaft zur Förderung der angewandten Forschung e.V. | Verfahren zur Herstellung von Aerogelen und mit diesem erhältliche Aerogele |
| WO2020125956A1 (de) | 2018-12-18 | 2020-06-25 | Wacker Chemie Ag | Verfahren zur herstellung abgerundeter gelpartikel |
| FR3094975B1 (fr) * | 2019-04-10 | 2022-11-18 | Keey Aerogel | Procédé de synthèse d’un aérogel de silice hydrophobique de type « one pot » à partir d’un précurseur de silice |
| EP3896035A1 (en) * | 2020-04-15 | 2021-10-20 | EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt | Silica aerogels and silica aerogel blankets |
| WO2021204815A1 (en) * | 2020-04-06 | 2021-10-14 | Empa Eidgenössische Materialprüfungs- Und Forschungsanstalt | Silica aerogels |
| CN113563012B (zh) * | 2020-04-29 | 2022-11-04 | 台湾气凝胶科技材料开发股份有限公司 | 御寒、隔热的疏水性气凝胶复合胶状物的制备方法及其相关产物 |
| JP7577757B2 (ja) * | 2020-04-30 | 2024-11-05 | エボニック オペレーションズ ゲーエムベーハー | アルカリ安定性の上昇したシリカエアロゲル |
| CH717558A1 (de) | 2020-06-22 | 2021-12-30 | Rockwool Int | Aerogel-Verbundwerkstoffen, sowie Wärmedämmelement. |
| EP4177231A1 (de) | 2021-11-03 | 2023-05-10 | Evonik Operations GmbH | Wärmedämmsysteme mit verbesserter kosteneffizienz |
| CN117510181B (zh) * | 2023-11-07 | 2024-04-16 | 武汉中科先进材料科技有限公司 | 一种超疏水、增强型二氧化硅气凝胶毡及其制备方法 |
| CN117658589A (zh) * | 2023-12-07 | 2024-03-08 | 翌江新材(江苏)有限公司 | 一种制备气凝胶材料的新型方法 |
| CN118561286A (zh) * | 2024-04-15 | 2024-08-30 | 湖南尚成新材料科技有限责任公司 | 采用醇混合溶液的亚临界态流体制备疏水气凝胶的方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013053951A1 (en) * | 2011-10-14 | 2013-04-18 | Enersens | Process for manufacturing xerogels |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2659155B2 (ja) * | 1992-02-03 | 1997-09-30 | 松下電工株式会社 | 疎水性エアロゲルの製造方法 |
| EP0585456B1 (en) * | 1992-02-18 | 1997-05-07 | Matsushita Electric Works Ltd | Process for producing hydrophobic aerogel |
| US5565142A (en) | 1992-04-01 | 1996-10-15 | Deshpande; Ravindra | Preparation of high porosity xerogels by chemical surface modification. |
| JP3712410B2 (ja) | 1993-08-31 | 2005-11-02 | ビーエーエスエフ アクチェンゲゼルシャフト | 疎水性ケイ酸エアロゲル |
| DE19631267C1 (de) | 1996-08-02 | 1998-04-30 | Hoechst Ag | Verfahren zur Herstellung von organisch modifizierten Aerogelen |
| DE19648798C2 (de) * | 1996-11-26 | 1998-11-19 | Hoechst Ag | Verfahren zur Herstellung von organisch modifizierten Aerogelen durch Oberflächenmodifikation des wäßrigen Gels (ohne vorherigen Lösungsmitteltausch) und anschließender Trocknung |
| JP3954842B2 (ja) * | 2001-08-02 | 2007-08-08 | 株式会社アルバック | 疎水性多孔質材料の製造方法 |
| FR2849444B1 (fr) * | 2002-12-30 | 2006-07-28 | Rhodia Chimie Sa | Procede de preparation d'un suspension de silice dans une matiere silicone eventuellement reticulable |
| EP1714195A2 (en) * | 2004-01-06 | 2006-10-25 | Aspen Aerogels Inc. | Ormosil aerogels containing silicon bonded polymethacrylate |
| FR2873677B1 (fr) * | 2004-07-29 | 2007-08-17 | Armines Ass Pour La Rech Et Le | Procede d'elaboration de serogels de silice hydrophobes |
| JP2007134420A (ja) * | 2005-11-09 | 2007-05-31 | Ulvac Japan Ltd | 疎水性多孔質シリカ材料による構造物内部の埋め込み方法 |
| US7999026B2 (en) * | 2007-02-02 | 2011-08-16 | Nissan Chemical Industries, Ltd. | Reactive monomer-dispersed silica sol and production method thereof, and curable composition and cured article thereof |
| KR100848856B1 (ko) * | 2007-03-27 | 2008-07-29 | 주식회사 넵 | 영구적 소수성을 갖는 에어로겔의 제조 방법 및 이로부터제조된 영구적 소수성을 갖는 에어로겔 |
| KR100924781B1 (ko) * | 2007-09-19 | 2009-11-03 | 주식회사 넵 | 영구적인 소수성을 갖는 고투광성 입상형 에어로겔제조방법 및 이로부터 제조된 입상형 에어로겔 |
| CN101372337B (zh) * | 2008-09-28 | 2010-12-08 | 厦门大学 | 共前驱体法常压干燥制备透明二氧化硅气凝胶的方法 |
| CN101691227B (zh) * | 2009-10-13 | 2011-10-12 | 厦门大学 | 二氧化硅气凝胶材料的制备方法 |
| KR101187568B1 (ko) | 2010-09-29 | 2012-10-04 | 한국에너지기술연구원 | 실리카 에어로겔 과립의 제조방법 |
| JP5669617B2 (ja) * | 2011-02-21 | 2015-02-12 | 株式会社トクヤマ | エアロゲル及び該エアロゲルを用いた断熱材 |
| CN102951650B (zh) * | 2012-08-31 | 2015-05-20 | 卢斌 | 一种快速制备SiO2气凝胶的常压干燥方法 |
| KR102172825B1 (ko) * | 2013-06-10 | 2020-11-02 | 닛산 가가쿠 가부시키가이샤 | 실리카 함유 수지 조성물 및 그 제조 방법 그리고 실리카 함유 수지 조성물의 성형품 |
-
2013
- 2013-08-02 EP EP13179185.7A patent/EP2832690A1/de not_active Ceased
-
2014
- 2014-07-28 EP EP14744131.5A patent/EP3027558A1/de not_active Withdrawn
- 2014-07-28 KR KR1020167003001A patent/KR101813898B1/ko not_active Expired - Fee Related
- 2014-07-28 AU AU2014298538A patent/AU2014298538B2/en not_active Ceased
- 2014-07-28 WO PCT/EP2014/066213 patent/WO2015014813A1/de not_active Ceased
- 2014-07-28 CN CN202111139256.7A patent/CN114408931A/zh active Pending
- 2014-07-28 JP JP2016530481A patent/JP6449279B2/ja not_active Expired - Fee Related
- 2014-07-28 BR BR112016002360A patent/BR112016002360A2/pt not_active IP Right Cessation
- 2014-07-28 US US14/908,601 patent/US20160258153A1/en not_active Abandoned
- 2014-07-28 CN CN201480050734.9A patent/CN105555710A/zh active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013053951A1 (en) * | 2011-10-14 | 2013-04-18 | Enersens | Process for manufacturing xerogels |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20160054462A (ko) | 2016-05-16 |
| JP6449279B2 (ja) | 2019-01-09 |
| AU2014298538A1 (en) | 2016-02-25 |
| WO2015014813A1 (de) | 2015-02-05 |
| EP3027558A1 (de) | 2016-06-08 |
| JP2016530199A (ja) | 2016-09-29 |
| BR112016002360A2 (pt) | 2017-08-01 |
| CN114408931A (zh) | 2022-04-29 |
| EP2832690A1 (de) | 2015-02-04 |
| AU2014298538B2 (en) | 2018-02-22 |
| US20160258153A1 (en) | 2016-09-08 |
| CN105555710A (zh) | 2016-05-04 |
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| PA0105 | International application |
St.27 status event code: A-0-1-A10-A15-nap-PA0105 |
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| PA0201 | Request for examination |
St.27 status event code: A-1-2-D10-D11-exm-PA0201 |
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| P11-X000 | Amendment of application requested |
St.27 status event code: A-2-2-P10-P11-nap-X000 |
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| P13-X000 | Application amended |
St.27 status event code: A-2-2-P10-P13-nap-X000 |
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