BR112016002360A2 - processo para a produção de um material de aerogel - Google Patents

processo para a produção de um material de aerogel

Info

Publication number
BR112016002360A2
BR112016002360A2 BR112016002360A BR112016002360A BR112016002360A2 BR 112016002360 A2 BR112016002360 A2 BR 112016002360A2 BR 112016002360 A BR112016002360 A BR 112016002360A BR 112016002360 A BR112016002360 A BR 112016002360A BR 112016002360 A2 BR112016002360 A2 BR 112016002360A2
Authority
BR
Brazil
Prior art keywords
hydrophobation
airgel material
gel
colloidal solution
producing
Prior art date
Application number
BR112016002360A
Other languages
English (en)
Inventor
Simmen Caroline
Koebel Matthias
Brunner Samuel
Zhao Shanyu
Original Assignee
Empa Eidgenoessische Mat & Forschungsanstalt
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Empa Eidgenoessische Mat & Forschungsanstalt filed Critical Empa Eidgenoessische Mat & Forschungsanstalt
Publication of BR112016002360A2 publication Critical patent/BR112016002360A2/pt

Links

Classifications

    • E—FIXED CONSTRUCTIONS
    • E04—BUILDING
    • E04B—GENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
    • E04B1/00—Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
    • E04B1/62—Insulation or other protection; Elements or use of specified material therefor
    • E04B1/74—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls
    • E04B1/76—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls specifically with respect to heat only
    • E04B1/78—Heat insulating elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/145—Preparation of hydroorganosols, organosols or dispersions in an organic medium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/155—Preparation of hydroorganogels or organogels
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/157—After-treatment of gels
    • C01B33/158—Purification; Drying; Dehydrating
    • C01B33/1585—Dehydration into aerogels

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Architecture (AREA)
  • Physics & Mathematics (AREA)
  • Acoustics & Sound (AREA)
  • Electromagnetism (AREA)
  • Civil Engineering (AREA)
  • Structural Engineering (AREA)
  • Silicon Compounds (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Thermal Insulation (AREA)

Abstract

resumo de patente de invenção para: "processo para a produção de um material de aerogel". processo para a produção de um material de aerogel, compreende as seguintes etapas: a) preparação de uma solução coloidal de óxido de silício em uma mistura alcoólica de solventes; b) desencadeamento da gelificação da solução coloidal através da adição de base, resultando um gel e opcionalmente envelhecimento do gel; c) hidrofobação do gel opcionalmente envelhecido; d) remoção da mistura de solventes através de secagem subcrítica, formando-se o material de aerogel. a solução coloidal de óxido de silício formada na etapa a) contém pelo menos um agente de hidrofobação que pode ser ativado cataliticamente com ácido, sendo que a proporção volumétrica do agente de hidrofobação na solução coloidal perfaz de 5 a 60 %. a hidrofobação na etapa c) é iniciada através da libertação ou adição de pelo menos um catalisador de hidrofobação que interage com o agente de hidrofobação.
BR112016002360A 2013-08-02 2014-07-28 processo para a produção de um material de aerogel BR112016002360A2 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP13179185.7A EP2832690A1 (de) 2013-08-02 2013-08-02 Verfahren zur Herstellung eines Aerogelmaterials
PCT/EP2014/066213 WO2015014813A1 (de) 2013-08-02 2014-07-28 Verfahren zur herstellung eines aerogelmaterials

Publications (1)

Publication Number Publication Date
BR112016002360A2 true BR112016002360A2 (pt) 2017-08-01

Family

ID=48917409

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112016002360A BR112016002360A2 (pt) 2013-08-02 2014-07-28 processo para a produção de um material de aerogel

Country Status (8)

Country Link
US (1) US20160258153A1 (pt)
EP (2) EP2832690A1 (pt)
JP (1) JP6449279B2 (pt)
KR (1) KR101813898B1 (pt)
CN (2) CN114408931A (pt)
AU (1) AU2014298538B2 (pt)
BR (1) BR112016002360A2 (pt)
WO (1) WO2015014813A1 (pt)

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EP3281920A1 (de) * 2016-08-12 2018-02-14 D. Swarovski KG Kontinuierliches sol-gel-verfahren zur herstellung von silicathaltigen gläsern oder glaskeramiken
US11279622B2 (en) 2016-09-12 2022-03-22 Lg Chem, Ltd. Method for producing silica aerogel and silica aerogel produced thereby
KR101942474B1 (ko) * 2016-11-18 2019-01-25 주식회사 엘지화학 전가수분해된 알킬 폴리실리케이트의 합성방법
EP3571173A1 (de) 2017-01-18 2019-11-27 Evonik Degussa GmbH Granulares wärmedämmungsmaterial und verfahren zur dessen herstellung
CN106955650A (zh) * 2017-04-01 2017-07-18 东华大学 一种三维多孔框架增强纤维气凝胶材料及其制备方法
DE102017209782A1 (de) 2017-06-09 2018-12-13 Evonik Degussa Gmbh Verfahren zur Wärmedämmung eines evakuierbaren Behälters
US20210039954A1 (en) * 2018-03-05 2021-02-11 Evonik Operations Gmbh Method for producing an aerogel material
EP3597615A1 (en) 2018-07-17 2020-01-22 Evonik Operations GmbH Granular mixed oxide material and thermal insulating composition on its basis
US11987528B2 (en) 2018-07-18 2024-05-21 Kingspan Insulation Limited Process for hydrophobizing shaped insulation-material bodies based on silica at ambient pressure
CN111039583B (zh) * 2018-10-11 2022-10-11 卢孟磊 一种低成本快速制备微纳结构气凝胶膨胀珍珠岩的方法
DE102018128410A1 (de) * 2018-11-13 2020-05-14 Fraunhofer Gesellschaft zur Förderung der angewandten Forschung e.V. Verfahren zur Herstellung von Aerogelen und mit diesem erhältliche Aerogele
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FR3094975B1 (fr) * 2019-04-10 2022-11-18 Keey Aerogel Procédé de synthèse d’un aérogel de silice hydrophobique de type « one pot » à partir d’un précurseur de silice
EP3896035A1 (en) * 2020-04-15 2021-10-20 EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt Silica aerogels and silica aerogel blankets
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Also Published As

Publication number Publication date
AU2014298538B2 (en) 2018-02-22
JP2016530199A (ja) 2016-09-29
AU2014298538A1 (en) 2016-02-25
US20160258153A1 (en) 2016-09-08
EP2832690A1 (de) 2015-02-04
CN105555710A (zh) 2016-05-04
KR20160054462A (ko) 2016-05-16
CN114408931A (zh) 2022-04-29
KR101813898B1 (ko) 2018-01-02
EP3027558A1 (de) 2016-06-08
JP6449279B2 (ja) 2019-01-09
WO2015014813A1 (de) 2015-02-05

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Legal Events

Date Code Title Description
B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]
B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]

Free format text: EM VIRTUDE DO ARQUIVAMENTO PUBLICADO NA RPI 2472 DE 22-05-2018 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDO O ARQUIVAMENTO DO PEDIDO DE PATENTE, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.