KR101673591B1 - 기체상에서의 이소시아네이트의 제조 방법 - Google Patents

기체상에서의 이소시아네이트의 제조 방법 Download PDF

Info

Publication number
KR101673591B1
KR101673591B1 KR1020090122317A KR20090122317A KR101673591B1 KR 101673591 B1 KR101673591 B1 KR 101673591B1 KR 1020090122317 A KR1020090122317 A KR 1020090122317A KR 20090122317 A KR20090122317 A KR 20090122317A KR 101673591 B1 KR101673591 B1 KR 101673591B1
Authority
KR
South Korea
Prior art keywords
reaction space
amine
reaction
cross
reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
KR1020090122317A
Other languages
English (en)
Korean (ko)
Other versions
KR20100067626A (ko
Inventor
클라우스 비스쿠프
라이너 브룬즈
볼프강 로렌츠
프릿츠 폴
프리드헬름 스테펜즈
폴케르 미헬레
Original Assignee
코베스트로 도이칠란드 아게
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 코베스트로 도이칠란드 아게 filed Critical 코베스트로 도이칠란드 아게
Publication of KR20100067626A publication Critical patent/KR20100067626A/ko
Application granted granted Critical
Publication of KR101673591B1 publication Critical patent/KR101673591B1/ko
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00Preparation of derivatives of isocyanic acid
    • C07C263/10Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/07Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by halogen atoms
    • C07C205/11Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by halogen atoms having nitro groups bound to carbon atoms of six-membered aromatic rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/27Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by etherified hydroxy groups
    • C07C205/35Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by etherified hydroxy groups having nitro groups and etherified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C205/36Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by etherified hydroxy groups having nitro groups and etherified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton to carbon atoms of the same non-condensed six-membered aromatic ring or to carbon atoms of six-membered aromatic rings being part of the same condensed ring system
    • C07C205/37Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by etherified hydroxy groups having nitro groups and etherified hydroxy groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton to carbon atoms of the same non-condensed six-membered aromatic ring or to carbon atoms of six-membered aromatic rings being part of the same condensed ring system the oxygen atom of at least one of the etherified hydroxy groups being further bound to an acyclic carbon atom
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C239/00Compounds containing nitrogen-to-halogen bonds; Hydroxylamino compounds or ethers or esters thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C265/00Derivatives of isocyanic acid
    • C07C265/12Derivatives of isocyanic acid having isocyanate groups bound to carbon atoms of six-membered aromatic rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020090122317A 2008-12-11 2009-12-10 기체상에서의 이소시아네이트의 제조 방법 Active KR101673591B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102008061686A DE102008061686A1 (de) 2008-12-11 2008-12-11 Verfahren zur Herstellung von Isocyanaten in der Gasphase
DE102008061686.9 2008-12-11

Publications (2)

Publication Number Publication Date
KR20100067626A KR20100067626A (ko) 2010-06-21
KR101673591B1 true KR101673591B1 (ko) 2016-11-07

Family

ID=41693159

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020090122317A Active KR101673591B1 (ko) 2008-12-11 2009-12-10 기체상에서의 이소시아네이트의 제조 방법

Country Status (10)

Country Link
US (1) US9024057B2 (enExample)
EP (1) EP2196455B1 (enExample)
JP (1) JP5574684B2 (enExample)
KR (1) KR101673591B1 (enExample)
CN (1) CN101747230B (enExample)
DE (1) DE102008061686A1 (enExample)
ES (1) ES2394133T3 (enExample)
PL (1) PL2196455T3 (enExample)
RU (1) RU2528382C2 (enExample)
TW (1) TWI501944B (enExample)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013139703A1 (de) * 2012-03-19 2013-09-26 Bayer Intellectual Property Gmbh Verfahren zur herstellung von isocyanaten
HUE034207T2 (hu) 2013-02-08 2018-01-29 Covestro Deutschland Ag Eljárás primer amin foszfogenálásával gázfázisban elõállított izocianát elválasztására a foszfogenálás gáz halmazállapotú nyerstermékétõl
EP2829533A1 (de) 2013-07-26 2015-01-28 Bayer MaterialScience AG Verfahren zur herstellung von isocyanaten
WO2015024859A1 (de) 2013-08-19 2015-02-26 Bayer Materialscience Ag Verfahren zur gewinnung von organischen isocyanaten aus destillationsrückständen der isocyanatherstellung
HUE060286T2 (hu) 2014-06-24 2023-02-28 Covestro Intellectual Property Gmbh & Co Kg Eljárás kémiai termékek elõállítására az eljárás megszakítása mellett
EP3307708B1 (de) 2015-06-12 2021-12-01 Covestro Intellectual Property GmbH & Co. KG Verfahren zur herstellung von diisocyanaten in der gasphase
JP6804512B2 (ja) 2015-07-16 2020-12-23 コベストロ、ドイチュラント、アクチエンゲゼルシャフトCovestro Deutschland Ag イソシアネートの製造方法
JP6913083B2 (ja) 2015-09-30 2021-08-04 コベストロ、ドイチュラント、アクチエンゲゼルシャフトCovestro Deutschland Ag イソシアネートの製造方法
KR20190039518A (ko) 2016-08-17 2019-04-12 코베스트로 도이칠란트 아게 통합 생산으로 이소시아네이트 및 적어도 1종의 추가의 화학 생성물을 제조하는 방법
US10364214B1 (en) 2016-09-01 2019-07-30 Covestro Deutschland Ag Method for producing isocyanates
CN110382100B (zh) * 2017-03-06 2022-05-24 陶氏环球技术有限责任公司 制备异氰酸酯的方法
EP3634947B1 (de) 2017-06-08 2022-09-07 Covestro Intellectual Property GmbH & Co. KG Verfahren zur herstellung von isocyanaten in der gasphase
CN110914236B (zh) 2017-06-08 2023-01-31 科思创德国股份有限公司 制备异氰酸酯的方法
US11365172B2 (en) 2017-07-03 2022-06-21 Covestro Deutschland Ag Production plant for producing a chemical product by reacting H-functional reactants with phosgene, and method for operating same with an interruption to production
US10626084B2 (en) 2018-08-03 2020-04-21 Covestro Llc Method for producing two isocyanates
US10851048B2 (en) * 2018-11-13 2020-12-01 Covestro Deutschland Ag Process for preparing an isocyanate by partly adiabatically operated phosgenation of the corresponding amine

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100209992B1 (ko) * 1992-10-16 1999-07-15 들로 다니엘 기체상에서의 방향족 이소시아네이트형 화합물의 제조방법
WO2007028715A1 (de) * 2005-09-06 2007-03-15 Basf Se Verfahren zur herstellung von isocyanaten

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ATA50084A (de) 1984-02-15 1986-06-15 Lift Verkaufsgeraete Gmbh Karteikastenartige vorrichtung zur aufnahme von steifen, flachen gegenstaenden
DE3780438T2 (de) 1986-11-27 1993-01-28 Beecham Group Plc N-substituierte cyclische amine, ihre herstellung sowie pharmazeutische zusammensetzungen die sie enthalten.
DE3714439A1 (de) 1987-04-30 1988-11-10 Bayer Ag Verfahren zur herstellung von (cyclo)aliphatischen diisocyanaten
DE4034840A1 (de) 1990-11-02 1992-05-07 Henkel Kgaa Enzymatisches fluessigwaschmittel
DE4217019A1 (de) * 1992-05-22 1993-11-25 Bayer Ag Verfahren zur Herstellung von aromatischen Diisocyanaten
FR2723585B1 (fr) * 1994-08-12 1996-09-27 Rhone Poulenc Chimie Procede de preparation de composes du type polyisocyanates aromatiques en phase gazeuse.
DE19523385A1 (de) 1995-06-23 1997-01-09 Bayer Ag Verfahren zur Herstellung von Triisocyanaten
DE10133729A1 (de) * 2001-07-11 2003-01-23 Bayer Ag Verfahren zur Herstellung von (cyclo)aliphatischen Diisocyanaten
DE10133728A1 (de) * 2001-07-11 2003-01-23 Bayer Ag Verfahren zur Herstellung von (cyclo)aliphatischen Diisocyanaten
DE10222023A1 (de) 2002-05-17 2003-11-27 Bayer Ag Verfahren zur Herstellung von Isocyanaten in der Gasphase
DE10245704A1 (de) 2002-09-30 2004-04-01 Bayer Ag Verfahren zum Quenchen eines gasförmigen Reaktionsgemisches bei der Gasphasenphosgenierung von Diaminen
DE10307141A1 (de) 2003-02-20 2004-09-02 Bayer Ag Verfahren zur Herstellung von (Poly)isocyanaten in der Gasphase
DE10349504A1 (de) 2003-10-23 2005-05-25 Bayer Technology Services Gmbh Verfahren zur Herstellung von Isocyanaten in der Gasphase
DE10359627A1 (de) 2003-12-18 2005-07-21 Bayer Materialscience Ag Verfahren zur Herstellung von Diisocyanaten
DE102005036870A1 (de) 2005-08-02 2007-02-08 Bayer Materialscience Ag Verfahren zur Gasphasenphosgenierung
US20070049482A1 (en) 2005-08-11 2007-03-01 Shin-Etsu Chemical Co., Ltd. Synthetic quartz glass substrate for excimer lasers and making method
DE102005042604A1 (de) 2005-09-07 2007-03-08 Basf Ag Neutralisationsverfahren
EP2079685A1 (de) * 2006-11-07 2009-07-22 Basf Se Verfahren zur herstellung von isocyanaten
WO2008055898A1 (de) 2006-11-07 2008-05-15 Basf Se Verfahren zur herstellung von isocyanaten
JP2010508374A (ja) * 2006-11-07 2010-03-18 ビーエーエスエフ ソシエタス・ヨーロピア イソシアネートの製造方法
DE102006058634A1 (de) 2006-12-13 2008-06-19 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten in der Gasphase
DE102006058633A1 (de) * 2006-12-13 2008-06-19 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten in der Gasphase

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100209992B1 (ko) * 1992-10-16 1999-07-15 들로 다니엘 기체상에서의 방향족 이소시아네이트형 화합물의 제조방법
WO2007028715A1 (de) * 2005-09-06 2007-03-15 Basf Se Verfahren zur herstellung von isocyanaten

Also Published As

Publication number Publication date
RU2009145797A (ru) 2011-06-20
EP2196455B1 (de) 2012-09-26
CN101747230A (zh) 2010-06-23
DE102008061686A1 (de) 2010-06-17
US9024057B2 (en) 2015-05-05
TW201035022A (en) 2010-10-01
CN101747230B (zh) 2014-04-09
RU2528382C2 (ru) 2014-09-20
JP5574684B2 (ja) 2014-08-20
KR20100067626A (ko) 2010-06-21
ES2394133T3 (es) 2013-01-22
JP2010138171A (ja) 2010-06-24
PL2196455T3 (pl) 2013-02-28
TWI501944B (zh) 2015-10-01
US20100152484A1 (en) 2010-06-17
EP2196455A1 (de) 2010-06-16

Similar Documents

Publication Publication Date Title
KR101673591B1 (ko) 기체상에서의 이소시아네이트의 제조 방법
JP5361178B2 (ja) 気相中でのイソシアネートの製造方法
US7488842B2 (en) Method for producing isocyanates
KR101436181B1 (ko) 이소시아네이트 생산 방법
US8168818B2 (en) Method for producing isocyanates
US8212069B2 (en) Process for preparing isocyanates
TWI464139B (zh) 氣相中製備異氰酸酯之方法
US20100056822A1 (en) Method for producing isocyanates
US8399702B2 (en) Process for the production of aromatic diisocyanates in the gas
KR20170058927A (ko) 이소시아네이트의 기체 상 제조 방법
KR20120038436A (ko) 이소시아네이트를 기체 상으로 제조하는 방법
HK1122792A (en) Process for the preparation of isocyanates in the gas phase
HK1130766A (en) Process for the production of aromatic diisocyanates in the gas phase

Legal Events

Date Code Title Description
PA0109 Patent application

St.27 status event code: A-0-1-A10-A12-nap-PA0109

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

P22-X000 Classification modified

St.27 status event code: A-2-2-P10-P22-nap-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U11-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

P22-X000 Classification modified

St.27 status event code: A-4-4-P10-P22-nap-X000

R17-X000 Change to representative recorded

St.27 status event code: A-5-5-R10-R17-oth-X000

FPAY Annual fee payment

Payment date: 20191029

Year of fee payment: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 8

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 9

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 10