KR100611284B1 - 고순도 모노에틸렌 글리콜의 제조 방법 - Google Patents

고순도 모노에틸렌 글리콜의 제조 방법 Download PDF

Info

Publication number
KR100611284B1
KR100611284B1 KR1020017003647A KR20017003647A KR100611284B1 KR 100611284 B1 KR100611284 B1 KR 100611284B1 KR 1020017003647 A KR1020017003647 A KR 1020017003647A KR 20017003647 A KR20017003647 A KR 20017003647A KR 100611284 B1 KR100611284 B1 KR 100611284B1
Authority
KR
South Korea
Prior art keywords
column
monoethylene glycol
stream
pressure
vacuum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
KR1020017003647A
Other languages
English (en)
Korean (ko)
Other versions
KR20010075276A (ko
Inventor
게르하르트 타이스
틸 아드리안
베른트 베쓸링
한스 하쎄
프란스 반샌트
Original Assignee
바스프 악티엔게젤샤프트
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 바스프 악티엔게젤샤프트 filed Critical 바스프 악티엔게젤샤프트
Publication of KR20010075276A publication Critical patent/KR20010075276A/ko
Application granted granted Critical
Publication of KR100611284B1 publication Critical patent/KR100611284B1/ko
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/20—Power plant

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020017003647A 1998-09-23 1999-09-21 고순도 모노에틸렌 글리콜의 제조 방법 Expired - Lifetime KR100611284B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19843697.1 1998-09-23
DE19843697A DE19843697A1 (de) 1998-09-23 1998-09-23 Verfahren zur Herstellung von hochreinem Monoethylenglykol

Publications (2)

Publication Number Publication Date
KR20010075276A KR20010075276A (ko) 2001-08-09
KR100611284B1 true KR100611284B1 (ko) 2006-08-10

Family

ID=7882020

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020017003647A Expired - Lifetime KR100611284B1 (ko) 1998-09-23 1999-09-21 고순도 모노에틸렌 글리콜의 제조 방법

Country Status (19)

Country Link
US (1) US6605192B1 (https=)
EP (1) EP1115682B1 (https=)
JP (1) JP4427190B2 (https=)
KR (1) KR100611284B1 (https=)
CN (1) CN1217898C (https=)
AR (1) AR020655A1 (https=)
AT (1) ATE255084T1 (https=)
AU (1) AU5980199A (https=)
BR (1) BR9913889B1 (https=)
CA (1) CA2345053C (https=)
DE (2) DE19843697A1 (https=)
ES (1) ES2212671T3 (https=)
MY (1) MY121383A (https=)
PL (1) PL195588B1 (https=)
RU (1) RU2235710C2 (https=)
SA (1) SA99200783B1 (https=)
TW (1) TW475925B (https=)
UA (1) UA60383C2 (https=)
WO (1) WO2000017141A1 (https=)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6372925B1 (en) 2000-06-09 2002-04-16 Shell Oil Company Process for operating the epoxidation of ethylene
US7095741B1 (en) * 2000-12-20 2006-08-22 Cisco Technology, Inc. Port isolation for restricting traffic flow on layer 2 switches
DE10321733A1 (de) * 2003-05-14 2004-12-02 Basf Ag Verfahren zur Herstellung von ameisensauren Formiaten
US8197645B2 (en) * 2005-12-29 2012-06-12 Basf Aktiengesellschaft Process for separating propylene glycol from aqueous compositions
RU2312696C1 (ru) * 2006-03-17 2007-12-20 Андрей Григорьевич Вендило Универсальная установка для очистки высококипящих растворителей вакуумной ректификацией и способы очистки вакуумной ректификацией на ней этиленгликоля, моноэтаноламина, метилцеллозольва, этилцеллозольва, бутилцеллозольва, n-метилпирролидона и бензилового спирта
WO2007144360A2 (en) * 2006-06-13 2007-12-21 Shell Internationale Research Maatschappij B.V. Glycol separation and purification
CA2739676A1 (en) * 2008-10-09 2010-04-15 Shell Internationale Research Maatschappij B.V. Process for the recovery of monoethylene glycol
CN106242945A (zh) * 2008-11-10 2016-12-21 陶氏技术投资有限公司 用于生产低色素二醇的方法
PL217778B1 (pl) 2011-06-20 2014-08-29 Piotr Medoń Sposób osuszania glikolu i układ do osuszania glikolu
CN103265401B (zh) * 2013-04-24 2014-12-17 河南朝歌日光新能源股份有限公司 一种煤制乙二醇工艺副产残液的回收方法
US9732019B1 (en) * 2016-04-01 2017-08-15 Cameron Solutions, Inc. System and method to remove organic acid from a rich MEG stream by stripping
GB201710508D0 (en) * 2017-06-30 2017-08-16 Johnson Matthey Davy Technologies Ltd Process
KR102663736B1 (ko) * 2017-11-23 2024-05-10 쉘 인터내셔날 리써취 마트샤피지 비.브이. 에틸렌 옥시드 및 에틸렌 글리콜 생산 방법
NL2025637B1 (en) * 2020-05-20 2021-12-07 Ioniqa Tech B V A separation method and reactor system for a glycol-water mixture
CN119868990B (zh) * 2025-03-12 2025-10-24 连云港石化有限公司 一种乙二醇预脱水塔装置及其使用方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2510548A (en) * 1947-06-20 1950-06-06 Lummus Co Multiple-effect distillation
DE1942094A1 (de) 1968-08-22 1970-02-26 Union Carbide Corp Verfahren zur Reinigung von verunreinigten Glykolen
IT972794B (it) * 1972-12-22 1974-05-31 Sir Soc Italiana Resine Spa Procedimento perfezionato per la produzione del glicole etilenico
US4182659A (en) * 1977-10-31 1980-01-08 Davy International Aktiengesellschaft Method of concentrating a water-containing glycol
DE3001727A1 (de) * 1980-01-18 1981-07-23 Hoechst Ag, 6000 Frankfurt Verfahren zur herstellung von hochreinem monoethylenglykol
DE3338488A1 (de) 1982-10-29 1984-05-03 Basf Ag, 6700 Ludwigshafen Verfahren zur gewinnung von temperaturempfindlichen produkten durch thermisch schonende destillation mittels eines mit einer destillationskolonne verbundenen duennschichtverdampfers und eine anordnung zur durchfuehrung des verfahrens
JPS6089439A (ja) 1983-10-24 1985-05-20 Mitsui Toatsu Chem Inc エチレングリコ−ルの製造方法
FR2564458B1 (fr) 1984-05-15 1986-09-12 Atochem Procede de separation de l'ethyleneglycol sous forme concentree dans un procede de fabrication d'oxyde d'ethylene
DE4306144A1 (de) * 1993-02-27 1994-09-01 Brown John Deutsche Eng Gmbh Verfahren und Polykondensationsanlage zur Aufbereitung von verunreinigtem Ethylenglykol
DE19602116A1 (de) 1996-01-22 1997-07-24 Basf Ag Verfahren zur Gewinnung von Glykolen mit niedrigem Aldehydgehalt
RU2111949C1 (ru) * 1996-08-19 1998-05-27 Акционерное общество "Нижнекамскнефтехим" Способ извлечения моно- и диэтиленгликолей из кубового остатка процесса выделения моноэтиленгликоля
US5738417A (en) * 1997-01-29 1998-04-14 Westinghouse Air Brake Company Brake pipe sensing unit

Also Published As

Publication number Publication date
MY121383A (en) 2006-01-28
CA2345053A1 (en) 2000-03-30
CN1319080A (zh) 2001-10-24
EP1115682B1 (de) 2003-11-26
ATE255084T1 (de) 2003-12-15
AR020655A1 (es) 2002-05-22
WO2000017141A1 (de) 2000-03-30
EP1115682A1 (de) 2001-07-18
UA60383C2 (uk) 2003-10-15
US6605192B1 (en) 2003-08-12
PL347580A1 (en) 2002-04-08
DE19843697A1 (de) 2000-03-30
AU5980199A (en) 2000-04-10
BR9913889B1 (pt) 2011-01-11
DE59907884D1 (de) 2004-01-08
JP2002526463A (ja) 2002-08-20
RU2235710C2 (ru) 2004-09-10
TW475925B (en) 2002-02-11
JP4427190B2 (ja) 2010-03-03
CN1217898C (zh) 2005-09-07
PL195588B1 (pl) 2007-10-31
BR9913889A (pt) 2001-07-03
ES2212671T3 (es) 2004-07-16
SA99200783B1 (ar) 2006-08-12
KR20010075276A (ko) 2001-08-09
CA2345053C (en) 2008-07-15

Similar Documents

Publication Publication Date Title
KR100670881B1 (ko) 고순도 모노에틸렌 글리콜의 제조 방법
KR100611284B1 (ko) 고순도 모노에틸렌 글리콜의 제조 방법
RU2639872C2 (ru) Способ очистки пропиленоксида
US6780289B2 (en) Process for the purification and recovery of acetonitrile
EP1888194B1 (en) New stripper configuration for the production of ethylene oxide
US8389776B2 (en) Treatment of phenol
KR102011715B1 (ko) 페놀 정제 방법
JP2002526462A5 (https=)
BG51039A3 (bg) Метод за пречистване на етиленгликол получен от етиленкарбонат
KR100551461B1 (ko) 미정제 액상 비닐 아세테이트의 후처리방법
JP2002526463A5 (https=)
CN1267276A (zh) 甲醇物流的提纯
JP2001031600A (ja) 高純度モノエチレングリコールの製法
CN113398618A (zh) 一种提高蒸馏分离效果的方法及蒸馏系统
KR20040027905A (ko) 아크릴로니트릴 제조에서 헤드 컬럼의 개선된 조작
MXPA01002968A (en) Method for producing highly pure monoethylene glycol
KR100707831B1 (ko) 노말 부틸아세테이트를 제조하는 방법 및 그 제조 장치
MXPA01002578A (en) Method for producing highly pure monoethylene glycol
KR20230029779A (ko) 아세톤 회수 및 정제
JP2013082709A (ja) プロピレンオキサイドの取得方法

Legal Events

Date Code Title Description
PA0105 International application

Patent event date: 20010322

Patent event code: PA01051R01D

Comment text: International Patent Application

PG1501 Laying open of application
A201 Request for examination
PA0201 Request for examination

Patent event code: PA02012R01D

Patent event date: 20040920

Comment text: Request for Examination of Application

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

Comment text: Notification of reason for refusal

Patent event date: 20060425

Patent event code: PE09021S01D

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

Patent event code: PE07011S01D

Comment text: Decision to Grant Registration

Patent event date: 20060630

GRNT Written decision to grant
PR0701 Registration of establishment

Comment text: Registration of Establishment

Patent event date: 20060803

Patent event code: PR07011E01D

PR1002 Payment of registration fee

Payment date: 20060804

End annual number: 3

Start annual number: 1

PG1601 Publication of registration
PR1001 Payment of annual fee

Payment date: 20090623

Start annual number: 4

End annual number: 4

PR1001 Payment of annual fee

Payment date: 20100628

Start annual number: 5

End annual number: 5

PR1001 Payment of annual fee

Payment date: 20110623

Start annual number: 6

End annual number: 6

FPAY Annual fee payment

Payment date: 20120725

Year of fee payment: 7

PR1001 Payment of annual fee

Payment date: 20120725

Start annual number: 7

End annual number: 7

FPAY Annual fee payment

Payment date: 20130723

Year of fee payment: 8

PR1001 Payment of annual fee

Payment date: 20130723

Start annual number: 8

End annual number: 8

FPAY Annual fee payment

Payment date: 20140724

Year of fee payment: 9

PR1001 Payment of annual fee

Payment date: 20140724

Start annual number: 9

End annual number: 9

FPAY Annual fee payment

Payment date: 20150723

Year of fee payment: 10

PR1001 Payment of annual fee

Payment date: 20150723

Start annual number: 10

End annual number: 10

FPAY Annual fee payment

Payment date: 20160801

Year of fee payment: 11

PR1001 Payment of annual fee

Payment date: 20160801

Start annual number: 11

End annual number: 11

FPAY Annual fee payment

Payment date: 20180717

Year of fee payment: 13

PR1001 Payment of annual fee

Payment date: 20180717

Start annual number: 13

End annual number: 13

FPAY Annual fee payment

Payment date: 20190806

Year of fee payment: 14

PR1001 Payment of annual fee

Payment date: 20190806

Start annual number: 14

End annual number: 14

PC1801 Expiration of term

Termination date: 20200321

Termination category: Expiration of duration