CA2345053C - Method for producing highly pure monoethylene glycol - Google Patents

Method for producing highly pure monoethylene glycol Download PDF

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Publication number
CA2345053C
CA2345053C CA002345053A CA2345053A CA2345053C CA 2345053 C CA2345053 C CA 2345053C CA 002345053 A CA002345053 A CA 002345053A CA 2345053 A CA2345053 A CA 2345053A CA 2345053 C CA2345053 C CA 2345053C
Authority
CA
Canada
Prior art keywords
column
monoethylene glycol
stream
degree
pressure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CA002345053A
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English (en)
French (fr)
Other versions
CA2345053A1 (en
Inventor
Gerhard Theis
Till Adrian
Bernd Bessling
Hans Hasse
Frans Vansant
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of CA2345053A1 publication Critical patent/CA2345053A1/en
Application granted granted Critical
Publication of CA2345053C publication Critical patent/CA2345053C/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/20—Power plant

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CA002345053A 1998-09-23 1999-09-21 Method for producing highly pure monoethylene glycol Expired - Lifetime CA2345053C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19843697.1 1998-09-23
DE19843697A DE19843697A1 (de) 1998-09-23 1998-09-23 Verfahren zur Herstellung von hochreinem Monoethylenglykol
PCT/EP1999/006968 WO2000017141A1 (de) 1998-09-23 1999-09-21 Verfahren zur herstellung von hochreinem monoethylenglykol

Publications (2)

Publication Number Publication Date
CA2345053A1 CA2345053A1 (en) 2000-03-30
CA2345053C true CA2345053C (en) 2008-07-15

Family

ID=7882020

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002345053A Expired - Lifetime CA2345053C (en) 1998-09-23 1999-09-21 Method for producing highly pure monoethylene glycol

Country Status (19)

Country Link
US (1) US6605192B1 (https=)
EP (1) EP1115682B1 (https=)
JP (1) JP4427190B2 (https=)
KR (1) KR100611284B1 (https=)
CN (1) CN1217898C (https=)
AR (1) AR020655A1 (https=)
AT (1) ATE255084T1 (https=)
AU (1) AU5980199A (https=)
BR (1) BR9913889B1 (https=)
CA (1) CA2345053C (https=)
DE (2) DE19843697A1 (https=)
ES (1) ES2212671T3 (https=)
MY (1) MY121383A (https=)
PL (1) PL195588B1 (https=)
RU (1) RU2235710C2 (https=)
SA (1) SA99200783B1 (https=)
TW (1) TW475925B (https=)
UA (1) UA60383C2 (https=)
WO (1) WO2000017141A1 (https=)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6372925B1 (en) 2000-06-09 2002-04-16 Shell Oil Company Process for operating the epoxidation of ethylene
US7095741B1 (en) * 2000-12-20 2006-08-22 Cisco Technology, Inc. Port isolation for restricting traffic flow on layer 2 switches
DE10321733A1 (de) * 2003-05-14 2004-12-02 Basf Ag Verfahren zur Herstellung von ameisensauren Formiaten
US8197645B2 (en) * 2005-12-29 2012-06-12 Basf Aktiengesellschaft Process for separating propylene glycol from aqueous compositions
RU2312696C1 (ru) * 2006-03-17 2007-12-20 Андрей Григорьевич Вендило Универсальная установка для очистки высококипящих растворителей вакуумной ректификацией и способы очистки вакуумной ректификацией на ней этиленгликоля, моноэтаноламина, метилцеллозольва, этилцеллозольва, бутилцеллозольва, n-метилпирролидона и бензилового спирта
WO2007144360A2 (en) * 2006-06-13 2007-12-21 Shell Internationale Research Maatschappij B.V. Glycol separation and purification
CA2739676A1 (en) * 2008-10-09 2010-04-15 Shell Internationale Research Maatschappij B.V. Process for the recovery of monoethylene glycol
CN106242945A (zh) * 2008-11-10 2016-12-21 陶氏技术投资有限公司 用于生产低色素二醇的方法
PL217778B1 (pl) 2011-06-20 2014-08-29 Piotr Medoń Sposób osuszania glikolu i układ do osuszania glikolu
CN103265401B (zh) * 2013-04-24 2014-12-17 河南朝歌日光新能源股份有限公司 一种煤制乙二醇工艺副产残液的回收方法
US9732019B1 (en) * 2016-04-01 2017-08-15 Cameron Solutions, Inc. System and method to remove organic acid from a rich MEG stream by stripping
GB201710508D0 (en) * 2017-06-30 2017-08-16 Johnson Matthey Davy Technologies Ltd Process
KR102663736B1 (ko) * 2017-11-23 2024-05-10 쉘 인터내셔날 리써취 마트샤피지 비.브이. 에틸렌 옥시드 및 에틸렌 글리콜 생산 방법
NL2025637B1 (en) * 2020-05-20 2021-12-07 Ioniqa Tech B V A separation method and reactor system for a glycol-water mixture
CN119868990B (zh) * 2025-03-12 2025-10-24 连云港石化有限公司 一种乙二醇预脱水塔装置及其使用方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2510548A (en) * 1947-06-20 1950-06-06 Lummus Co Multiple-effect distillation
DE1942094A1 (de) 1968-08-22 1970-02-26 Union Carbide Corp Verfahren zur Reinigung von verunreinigten Glykolen
IT972794B (it) * 1972-12-22 1974-05-31 Sir Soc Italiana Resine Spa Procedimento perfezionato per la produzione del glicole etilenico
US4182659A (en) * 1977-10-31 1980-01-08 Davy International Aktiengesellschaft Method of concentrating a water-containing glycol
DE3001727A1 (de) * 1980-01-18 1981-07-23 Hoechst Ag, 6000 Frankfurt Verfahren zur herstellung von hochreinem monoethylenglykol
DE3338488A1 (de) 1982-10-29 1984-05-03 Basf Ag, 6700 Ludwigshafen Verfahren zur gewinnung von temperaturempfindlichen produkten durch thermisch schonende destillation mittels eines mit einer destillationskolonne verbundenen duennschichtverdampfers und eine anordnung zur durchfuehrung des verfahrens
JPS6089439A (ja) 1983-10-24 1985-05-20 Mitsui Toatsu Chem Inc エチレングリコ−ルの製造方法
FR2564458B1 (fr) 1984-05-15 1986-09-12 Atochem Procede de separation de l'ethyleneglycol sous forme concentree dans un procede de fabrication d'oxyde d'ethylene
DE4306144A1 (de) * 1993-02-27 1994-09-01 Brown John Deutsche Eng Gmbh Verfahren und Polykondensationsanlage zur Aufbereitung von verunreinigtem Ethylenglykol
DE19602116A1 (de) 1996-01-22 1997-07-24 Basf Ag Verfahren zur Gewinnung von Glykolen mit niedrigem Aldehydgehalt
RU2111949C1 (ru) * 1996-08-19 1998-05-27 Акционерное общество "Нижнекамскнефтехим" Способ извлечения моно- и диэтиленгликолей из кубового остатка процесса выделения моноэтиленгликоля
US5738417A (en) * 1997-01-29 1998-04-14 Westinghouse Air Brake Company Brake pipe sensing unit

Also Published As

Publication number Publication date
MY121383A (en) 2006-01-28
CA2345053A1 (en) 2000-03-30
KR100611284B1 (ko) 2006-08-10
CN1319080A (zh) 2001-10-24
EP1115682B1 (de) 2003-11-26
ATE255084T1 (de) 2003-12-15
AR020655A1 (es) 2002-05-22
WO2000017141A1 (de) 2000-03-30
EP1115682A1 (de) 2001-07-18
UA60383C2 (uk) 2003-10-15
US6605192B1 (en) 2003-08-12
PL347580A1 (en) 2002-04-08
DE19843697A1 (de) 2000-03-30
AU5980199A (en) 2000-04-10
BR9913889B1 (pt) 2011-01-11
DE59907884D1 (de) 2004-01-08
JP2002526463A (ja) 2002-08-20
RU2235710C2 (ru) 2004-09-10
TW475925B (en) 2002-02-11
JP4427190B2 (ja) 2010-03-03
CN1217898C (zh) 2005-09-07
PL195588B1 (pl) 2007-10-31
BR9913889A (pt) 2001-07-03
ES2212671T3 (es) 2004-07-16
SA99200783B1 (ar) 2006-08-12
KR20010075276A (ko) 2001-08-09

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Effective date: 20190923