KR100352680B1 - 플루오르화수소의 제거 방법 - Google Patents

플루오르화수소의 제거 방법 Download PDF

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Publication number
KR100352680B1
KR100352680B1 KR1020017015229A KR20017015229A KR100352680B1 KR 100352680 B1 KR100352680 B1 KR 100352680B1 KR 1020017015229 A KR1020017015229 A KR 1020017015229A KR 20017015229 A KR20017015229 A KR 20017015229A KR 100352680 B1 KR100352680 B1 KR 100352680B1
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South Korea
Prior art keywords
mixture
liquid phase
hydrogen fluoride
temperature
molar ratio
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Expired - Fee Related
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KR1020017015229A
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English (en)
Korean (ko)
Inventor
쓰다다께히데
마쓰모또다께오
다나까요시노리
고마쓰사또시
고야마사또시
Original Assignee
다이낑 고오교 가부시키가이샤
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Application filed by 다이낑 고오교 가부시키가이샤 filed Critical 다이낑 고오교 가부시키가이샤
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Publication of KR100352680B1 publication Critical patent/KR100352680B1/ko
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
    • C07C19/10—Acyclic saturated compounds containing halogen atoms containing fluorine and chlorine
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/19—Fluorine; Hydrogen fluoride
    • C01B7/191—Hydrogen fluoride
    • C01B7/195—Separation; Purification
    • C01B7/196—Separation; Purification by distillation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/19—Fluorine; Hydrogen fluoride
    • C01B7/191—Hydrogen fluoride
    • C01B7/195—Separation; Purification

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
KR1020017015229A 1992-04-13 1993-04-09 플루오르화수소의 제거 방법 Expired - Fee Related KR100352680B1 (ko)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JPJP-P-1992-00092667 1992-04-13
JP9266792 1992-04-13
JPJP-P-1992-00107656 1992-04-27
JP10765692 1992-04-27

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
KR10-1998-0702434A Division KR100338277B1 (ko) 1992-04-13 1993-04-09 플루오르화수소의제거방법

Publications (1)

Publication Number Publication Date
KR100352680B1 true KR100352680B1 (ko) 2002-09-16

Family

ID=26434051

Family Applications (3)

Application Number Title Priority Date Filing Date
KR1020017015229A Expired - Fee Related KR100352680B1 (ko) 1992-04-13 1993-04-09 플루오르화수소의 제거 방법
KR1019930703863A Expired - Fee Related KR100295306B1 (ko) 1992-04-13 1993-04-09 플루오르화수소의제거방법
KR10-1998-0702434A Expired - Fee Related KR100338277B1 (ko) 1992-04-13 1993-04-09 플루오르화수소의제거방법

Family Applications After (2)

Application Number Title Priority Date Filing Date
KR1019930703863A Expired - Fee Related KR100295306B1 (ko) 1992-04-13 1993-04-09 플루오르화수소의제거방법
KR10-1998-0702434A Expired - Fee Related KR100338277B1 (ko) 1992-04-13 1993-04-09 플루오르화수소의제거방법

Country Status (13)

Country Link
US (2) US5523015A (https=)
EP (1) EP0606482B1 (https=)
JP (1) JP3147380B2 (https=)
KR (3) KR100352680B1 (https=)
CN (1) CN1039313C (https=)
AU (1) AU663586B2 (https=)
BR (1) BR9305484A (https=)
CA (1) CA2111007C (https=)
DE (1) DE69319711T2 (https=)
ES (1) ES2118949T3 (https=)
RU (1) RU2118635C1 (https=)
TW (1) TW283659B (https=)
WO (1) WO1993021140A1 (https=)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3163831B2 (ja) * 1993-04-06 2001-05-08 ダイキン工業株式会社 １，１−ジフルオロエタンとフッ化水素の共沸混合物および１，１−ジフルオロエタンまたはフッ化水素の回収方法
GB9407257D0 (en) * 1993-04-22 1994-06-08 Ici Plc Vaporisation of liquids
US6274781B1 (en) * 1993-11-01 2001-08-14 E. I. Du Pont De Nemours And Company Production of dihalomethanes containing fluorine and azeotropes of dihalomethanes containing chlorine with HF
DE69500938T2 (de) * 1994-02-28 1998-04-30 Atochem Elf Sa Verfahren zur Trennung von Fluorwasserstoff und Difluormethan
US5718807A (en) * 1994-09-20 1998-02-17 E. I. Du Pont De Nemours And Company Purification process for hexafluoroethane products
US5789633A (en) * 1995-06-06 1998-08-04 E. I. Du Pont De Nemours And Company Azeotropic or azeotrope-like compositions of hydrofluoric acid with dihaloethanes
US5714650A (en) * 1995-06-07 1998-02-03 E. I. Du Pont De Nemours And Company Continuous manufacture of 1,1-difluoroethane
US5672788A (en) * 1995-06-07 1997-09-30 E. I. Du Pont De Nemours And Company Two-step process for manufacturing 1,1-difluoroethane
US5763708A (en) * 1995-09-20 1998-06-09 Allied Signal Inc. Process for the production of difluoromethane
US5785822A (en) * 1996-05-23 1998-07-28 Alliedsignal Inc. Process for separating difluoromethane
WO1998000379A1 (en) * 1996-07-03 1998-01-08 Alliedsignal Inc. Water extraction of hydrogen fluoride from a halocarbon/hydrogen fluoride azeotropic mixture
CA2264686A1 (en) * 1996-08-27 1998-03-05 Daikin Industries, Ltd. Process for producing difluoromethane
DE69708137T2 (de) * 1996-08-27 2002-06-20 Daikin Industries, Ltd. Verfahren zur herstellung von difluormethan
US5800682A (en) * 1996-10-08 1998-09-01 Alliedsignal Inc. Process for the production of difluoromethane
FR2768717B1 (fr) * 1997-09-24 1999-11-12 Solvay Procede de separation de fluorure d'hydrogene de ses melanges avec un hydrofluoroalcane contenant de 3 a 6 atomes de carbone
US6488817B1 (en) * 1998-03-31 2002-12-03 Alliedsignal Inc. Purification of hydrofluorocarbons
US6521803B1 (en) * 1998-12-18 2003-02-18 Solvay (Societe Anonyme) Method for separating a mixture comprising at least an hydrofluoroalkane and hydrogen fluoride, methods for preparing a hydrofluoroalkane and azeotropic compositions
RU2174999C1 (ru) * 2000-05-12 2001-10-20 Общество с ограниченной ответственностью "Учебно-научно-производственная фирма "Липиды" Способ рафинации труднорафинируемых растительных масел
US6500795B2 (en) * 2001-01-24 2002-12-31 Honeywell International Inc. Azeotrope-like composition of 1-chloro-1,3,3,3-tetrafluoropropane and hydrogen fluoride
US6605193B2 (en) 2001-04-25 2003-08-12 Atofina Chemicals, Inc. Recovery of HFC-32
CN101270029A (zh) * 2001-06-01 2008-09-24 霍尼韦尔国际公司 1,1,1,3,3-五氟丁烷与氟化氢的类共沸组合物的应用
JP5439177B2 (ja) * 2006-08-24 2014-03-12 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 共沸蒸留によってフッ化水素からフルオロオレフィンを分離する方法
CN103626626B (zh) * 2013-11-01 2015-06-24 西安近代化学研究所 氟化氢和2-氯-1,1,1,2-四氟丙烷混合物的分离方法
GB2636765A (en) * 2023-12-21 2025-07-02 Mexichem Uk Ltd Compositions

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2450414A (en) * 1946-11-14 1948-10-05 Kinetic Chemicals Inc Distillation process for separating products of chloroform fluorination
US3490739A (en) * 1965-09-16 1970-01-20 Walter R Buckman Azeotropic composition containing hexafluoroacetone,hydrogen fluoride,and trichlorotrifluoroethane
DE1546079B2 (de) * 1965-12-22 1971-06-09 Allied Chemical Corp.. New York, N Y (V St.A ) Azeotropes loesungsmittelgemisch insbesondere zur entfernung eines harzflussmittels von gedruckten schaltungen
US3728268A (en) * 1970-12-11 1973-04-17 Du Pont Mixtures of 1,1,2-trichloro-1,2,2-trifluoroethane,ethanol and acetone and a ternary azeotrope thereof
US3789004A (en) * 1971-06-28 1974-01-29 Ici Ltd Solvent compositions
US3947558A (en) 1973-08-16 1976-03-30 Dow Chemical (Nederland) B.V. Method of recovering HF from mixtures containing C1 -C3 halocarbon compounds
US4020112A (en) * 1975-02-06 1977-04-26 E. I. Du Pont De Nemours And Company Oxidative fluorination of phenols
US4169807A (en) * 1978-03-20 1979-10-02 Rca Corporation Novel solvent drying agent
JPS59225131A (ja) 1983-06-06 1984-12-18 Showa Denko Kk ジフルオロメタンの製造方法
JPS6013726A (ja) 1983-07-04 1985-01-24 Showa Denko Kk フルオロメタンの製造方法
US4911792A (en) * 1988-08-01 1990-03-27 E. I. Du Pont De Nemours And Company Process for the separation of HF via phase separation and distillation
US4950364A (en) * 1989-05-04 1990-08-21 Pennwalt Corporation Process for the separation of 1,1-dichloro-1-fluoroethane and 1,1,1,3,3-pentafluorobutane
US4975156A (en) * 1989-05-04 1990-12-04 Atochem North America, Inc. Process for the separation of hydrogen fluoride, 1,1-dichloro-1-fluoroethane and 1-chloro-1,1-difluoroethane from liquid mixtures thereof
US5036036A (en) 1989-06-13 1991-07-30 E. I. Du Pont De Nemours And Company Chromium oxide catalyst composition
JPH05500672A (ja) 1989-10-04 1993-02-12 イー・アイ・デユポン・ドウ・ヌムール・アンド・カンパニー フルオロカーボン精製方法
GB9105407D0 (en) * 1991-03-14 1991-05-01 Ici Plc Separation process
US5196616A (en) * 1991-10-18 1993-03-23 E. I. Du Pont De Nemours And Company Process for separating and recovering fluorocarbons and hydrogen fluoride from mixtures thereof
US6274781B1 (en) 1993-11-01 2001-08-14 E. I. Du Pont De Nemours And Company Production of dihalomethanes containing fluorine and azeotropes of dihalomethanes containing chlorine with HF
DE69500938T2 (de) * 1994-02-28 1998-04-30 Atochem Elf Sa Verfahren zur Trennung von Fluorwasserstoff und Difluormethan

Also Published As

Publication number Publication date
AU3904093A (en) 1993-11-18
TW283659B (https=) 1996-08-21
EP0606482A4 (en) 1994-03-23
CN1088195A (zh) 1994-06-22
KR100295306B1 (ko) 2001-09-17
JP3147380B2 (ja) 2001-03-19
US5523015A (en) 1996-06-04
DE69319711T2 (de) 1999-01-07
AU663586B2 (en) 1995-10-12
BR9305484A (pt) 1995-04-11
US6311515B1 (en) 2001-11-06
DE69319711D1 (de) 1998-08-20
KR940701373A (ko) 1994-05-28
EP0606482B1 (en) 1998-07-15
EP0606482A1 (en) 1994-07-20
CN1039313C (zh) 1998-07-29
KR100338277B1 (ko) 2003-02-20
RU2118635C1 (ru) 1998-09-10
ES2118949T3 (es) 1998-10-01
WO1993021140A1 (fr) 1993-10-28
CA2111007A1 (en) 1993-10-28
CA2111007C (en) 2004-08-03

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