JPWO2020012193A5 - - Google Patents
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- Publication number
- JPWO2020012193A5 JPWO2020012193A5 JP2021524125A JP2021524125A JPWO2020012193A5 JP WO2020012193 A5 JPWO2020012193 A5 JP WO2020012193A5 JP 2021524125 A JP2021524125 A JP 2021524125A JP 2021524125 A JP2021524125 A JP 2021524125A JP WO2020012193 A5 JPWO2020012193 A5 JP WO2020012193A5
- Authority
- JP
- Japan
- Prior art keywords
- precursor
- cations
- solution
- organic solvent
- item
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000000034 method Methods 0.000 claims description 59
- 150000001768 cations Chemical class 0.000 claims description 34
- 239000000243 solution Substances 0.000 claims description 29
- 239000002243 precursor Substances 0.000 claims description 26
- 150000001450 anions Chemical class 0.000 claims description 16
- 239000003960 organic solvent Substances 0.000 claims description 16
- 239000000463 material Substances 0.000 claims description 13
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000002244 precipitate Substances 0.000 claims description 12
- 150000001875 compounds Chemical class 0.000 claims description 11
- -1 metalloid cations Chemical class 0.000 claims description 9
- 239000010409 thin film Substances 0.000 claims description 8
- 239000007864 aqueous solution Substances 0.000 claims description 7
- 239000000758 substrate Substances 0.000 claims description 7
- 239000002184 metal Substances 0.000 claims description 5
- 229910052751 metal Inorganic materials 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 125000000217 alkyl group Chemical group 0.000 claims description 3
- 239000003125 aqueous solvent Substances 0.000 claims description 3
- 125000005913 (C3-C6) cycloalkyl group Chemical group 0.000 claims description 2
- WJYIASZWHGOTOU-UHFFFAOYSA-N Heptylamine Chemical compound CCCCCCCN WJYIASZWHGOTOU-UHFFFAOYSA-N 0.000 claims description 2
- BAVYZALUXZFZLV-UHFFFAOYSA-O Methylammonium ion Chemical compound [NH3+]C BAVYZALUXZFZLV-UHFFFAOYSA-O 0.000 claims description 2
- 150000003973 alkyl amines Chemical class 0.000 claims description 2
- 125000005210 alkyl ammonium group Chemical group 0.000 claims description 2
- 150000001412 amines Chemical class 0.000 claims description 2
- 125000003118 aryl group Chemical group 0.000 claims description 2
- HQABUPZFAYXKJW-UHFFFAOYSA-O butylazanium Chemical compound CCCC[NH3+] HQABUPZFAYXKJW-UHFFFAOYSA-O 0.000 claims description 2
- 238000000151 deposition Methods 0.000 claims description 2
- 238000001704 evaporation Methods 0.000 claims description 2
- 230000008020 evaporation Effects 0.000 claims description 2
- ZRALSGWEFCBTJO-UHFFFAOYSA-O guanidinium Chemical compound NC(N)=[NH2+] ZRALSGWEFCBTJO-UHFFFAOYSA-O 0.000 claims description 2
- BMVXCPBXGZKUPN-UHFFFAOYSA-O hexylazanium Chemical compound CCCCCC[NH3+] BMVXCPBXGZKUPN-UHFFFAOYSA-O 0.000 claims description 2
- 150000002466 imines Chemical class 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 229910052752 metalloid Inorganic materials 0.000 claims description 2
- IOQPZZOEVPZRBK-UHFFFAOYSA-O octylazanium Chemical compound CCCCCCCC[NH3+] IOQPZZOEVPZRBK-UHFFFAOYSA-O 0.000 claims description 2
- DPBLXKKOBLCELK-UHFFFAOYSA-O pentylazanium Chemical compound CCCCC[NH3+] DPBLXKKOBLCELK-UHFFFAOYSA-O 0.000 claims description 2
- 239000003495 polar organic solvent Substances 0.000 claims description 2
- 239000002798 polar solvent Substances 0.000 claims description 2
- WGYKZJWCGVVSQN-UHFFFAOYSA-O propan-1-aminium Chemical compound CCC[NH3+] WGYKZJWCGVVSQN-UHFFFAOYSA-O 0.000 claims description 2
- 125000001424 substituent group Chemical group 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims 2
- 125000003342 alkenyl group Chemical group 0.000 claims 1
- 125000000753 cycloalkyl group Chemical group 0.000 claims 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 1
- 239000002904 solvent Substances 0.000 description 4
- 125000000882 C2-C6 alkenyl group Chemical group 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000002178 crystalline material Substances 0.000 description 1
- QUSNBJAOOMFDIB-UHFFFAOYSA-O ethylaminium Chemical compound CC[NH3+] QUSNBJAOOMFDIB-UHFFFAOYSA-O 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000004528 spin coating Methods 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2023142087A JP7601971B2 (ja) | 2018-07-13 | 2023-09-01 | Ａ／ｍ／ｘ材料の製作方法 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1811539.4 | 2018-07-13 | ||
| GBGB1811539.4A GB201811539D0 (en) | 2018-07-13 | 2018-07-13 | Fabrication process for a/m/x materials |
| PCT/GB2019/051961 WO2020012193A1 (en) | 2018-07-13 | 2019-07-12 | Fabrication process for a/m/x materials |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2023142087A Division JP7601971B2 (ja) | 2018-07-13 | 2023-09-01 | Ａ／ｍ／ｘ材料の製作方法 |
Publications (4)
| Publication Number | Publication Date |
|---|---|
| JP2021532603A JP2021532603A (ja) | 2021-11-25 |
| JP2021532603A5 JP2021532603A5 (https=) | 2022-07-11 |
| JPWO2020012193A5 true JPWO2020012193A5 (https=) | 2022-07-11 |
| JP7464595B2 JP7464595B2 (ja) | 2024-04-09 |
Family
ID=63272997
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2021524125A Active JP7464595B2 (ja) | 2018-07-13 | 2019-07-12 | Ａ／ｍ／ｘ材料の製作方法 |
| JP2023142087A Active JP7601971B2 (ja) | 2018-07-13 | 2023-09-01 | Ａ／ｍ／ｘ材料の製作方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2023142087A Active JP7601971B2 (ja) | 2018-07-13 | 2023-09-01 | Ａ／ｍ／ｘ材料の製作方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US11976227B2 (https=) |
| EP (2) | EP3820967B1 (https=) |
| JP (2) | JP7464595B2 (https=) |
| KR (2) | KR102786917B1 (https=) |
| CN (2) | CN112739798A (https=) |
| ES (1) | ES2969577T3 (https=) |
| GB (1) | GB201811539D0 (https=) |
| WO (1) | WO2020012193A1 (https=) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102581137B1 (ko) * | 2018-08-29 | 2023-09-22 | 삼성디스플레이 주식회사 | 표시 장치 |
| CN113380910B (zh) * | 2020-03-09 | 2023-01-24 | 中国科学院大连化学物理研究所 | 一种铌卤化物材料与制备及应用 |
| KR102899242B1 (ko) * | 2020-03-30 | 2025-12-11 | 삼성디스플레이 주식회사 | 유기 금속 할라이드 화합물, 이를 포함한 광학 부재, 발광 소자 및 장치 |
| CN111944525B (zh) * | 2020-08-25 | 2022-05-10 | 深圳大学 | 零维铯铅溴无机钙钛矿材料及其制备方法 |
| KR102524997B1 (ko) * | 2020-09-18 | 2023-04-26 | 한국세라믹기술원 | Ｃｓ4ＰｂＢｒ6 페로브스카이트 나노결정 및 ＷＡＳＳＲ(Water-assisted Solid State Reaction Method)을 이용한 제작방법 |
| JP7440777B2 (ja) * | 2021-09-27 | 2024-02-29 | 日亜化学工業株式会社 | 発光材料、波長変換部材、発光装置及び発光材料の製造方法 |
| CN115896951B (zh) * | 2021-09-30 | 2024-10-29 | 闽都创新实验室 | 一种混合卤素醋酸铅二阶非线性光学晶体及其制备方法和应用 |
| CN114517088B (zh) * | 2021-12-29 | 2024-07-09 | 华东理工大学 | 一种卤化物钙钛矿纳米材料及其制备方法 |
| CN115385939A (zh) * | 2022-08-22 | 2022-11-25 | 重庆大学 | 一种铜基卤化物红光材料及其制备方法和应用 |
| IL297568B2 (en) * | 2022-10-23 | 2024-06-01 | Green Capsula Solution Ltd | Optically Concentrated Thermally Stabilized Photovoltaic System And Method |
| CN115558489B (zh) * | 2022-10-24 | 2023-07-18 | 吉林大学 | 一种高荧光效率零维镓掺杂金属卤化物及其制备方法 |
| WO2024130481A1 (en) * | 2022-12-19 | 2024-06-27 | Dic Corporation | Method for producing metal halide compound |
| KR102872383B1 (ko) * | 2023-06-05 | 2025-10-22 | 서울대학교산학협력단 | 페로브스카이트 분말, 발광소자용 발광층 및 이의 제조방법 |
| GB202318485D0 (en) | 2023-12-04 | 2024-01-17 | Univ Oxford Innovation Ltd | Passivation |
| KR102927200B1 (ko) * | 2025-05-08 | 2026-02-11 | 단국대학교 천안캠퍼스 산학협력단 | 무수 pedot을 포함하는 정공 수송층, 이를 포함하는 루도르파이트 광전소자의 제조방법 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10388897B2 (en) | 2012-05-18 | 2019-08-20 | Oxford University Innovation Limited | Optoelectronic device comprising porous scaffold material and perovskites |
| EP3010054B1 (en) | 2012-05-18 | 2019-02-20 | Oxford University Innovation Limited | Optoelectronic device |
| GB201208793D0 (en) | 2012-05-18 | 2012-07-04 | Isis Innovation | Optoelectronic device |
| ES2707296T3 (es) | 2012-09-18 | 2019-04-03 | Univ Oxford Innovation Ltd | Dispositivo optoelectrónico |
| ES2776161T3 (es) | 2013-12-17 | 2020-07-29 | Univ Oxford Innovation Ltd | Dispositivo fotovoltaico que comprende una perovskita de haluro metálico y un agente pasivante |
| US9334443B1 (en) * | 2014-10-31 | 2016-05-10 | Sun Harmonics, Ltd. | Synthesis of CsSnI3 by a solution based method |
| CN104505462A (zh) | 2014-12-19 | 2015-04-08 | 深圳大学 | 一种有机金属卤化物薄膜及其制备方法与应用 |
| CN104861958B (zh) * | 2015-05-14 | 2017-02-15 | 北京理工大学 | 一种钙钛矿/聚合物复合发光材料及其制备方法 |
| GB201513272D0 (en) | 2015-07-28 | 2015-09-09 | Isis Innovation | Luminescent material |
| AU2016316984B2 (en) | 2015-09-02 | 2021-11-25 | Oxford Photovoltaics Limited | Double perovskite |
| GB201520972D0 (en) | 2015-11-27 | 2016-01-13 | Isis Innovation | Mixed cation perovskite |
| KR101804173B1 (ko) | 2016-04-04 | 2017-12-05 | 한국화학연구원 | BaSnO3 박막 및 이의 저온 제조 방법 |
| KR101967029B1 (ko) * | 2016-12-22 | 2019-04-08 | 아주대학교산학협력단 | 페로브스카이트 발광 구조체 및 이의 제조 방법 |
| US9880458B1 (en) | 2017-04-17 | 2018-01-30 | Hee Solar, L.L.C. | Hybrid perovskite material processing |
| CN107099290A (zh) * | 2017-07-05 | 2017-08-29 | 向爱双 | 制备核壳结构钙钛矿量子点的方法 |
| CN107887510A (zh) | 2017-10-25 | 2018-04-06 | 深圳大学 | 一种二维层状钙钛矿薄膜、太阳能电池及其制备方法 |
-
2018
- 2018-07-13 GB GBGB1811539.4A patent/GB201811539D0/en not_active Ceased
-
2019
- 2019-07-12 EP EP19744819.4A patent/EP3820967B1/en active Active
- 2019-07-12 KR KR1020237031696A patent/KR102786917B1/ko active Active
- 2019-07-12 CN CN201980060141.3A patent/CN112739798A/zh active Pending
- 2019-07-12 ES ES21195937T patent/ES2969577T3/es active Active
- 2019-07-12 EP EP21195937.4A patent/EP3974498B1/en active Active
- 2019-07-12 WO PCT/GB2019/051961 patent/WO2020012193A1/en not_active Ceased
- 2019-07-12 US US17/259,712 patent/US11976227B2/en active Active
- 2019-07-12 JP JP2021524125A patent/JP7464595B2/ja active Active
- 2019-07-12 KR KR1020217004317A patent/KR20210032444A/ko not_active Ceased
- 2019-07-12 CN CN202310501365.1A patent/CN116716104A/zh active Pending
-
2023
- 2023-05-16 US US18/318,700 patent/US20230348782A1/en active Pending
- 2023-09-01 JP JP2023142087A patent/JP7601971B2/ja active Active
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