JPS6219544A - ２，３−ジクロル−１−プロパノ−ルの製法 - Google Patents
２，３−ジクロル−１−プロパノ−ルの製法Info
- Publication number
- JPS6219544A JPS6219544A JP15879085A JP15879085A JPS6219544A JP S6219544 A JPS6219544 A JP S6219544A JP 15879085 A JP15879085 A JP 15879085A JP 15879085 A JP15879085 A JP 15879085A JP S6219544 A JPS6219544 A JP S6219544A
- Authority
- JP
- Japan
- Prior art keywords
- hydrogen chloride
- allyl alcohol
- chlorine
- reaction
- propanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- ZXCYIJGIGSDJQQ-UHFFFAOYSA-N 2,3-dichloropropan-1-ol Chemical compound OCC(Cl)CCl ZXCYIJGIGSDJQQ-UHFFFAOYSA-N 0.000 title claims description 13
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 claims abstract description 50
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 33
- 238000006243 chemical reaction Methods 0.000 claims abstract description 24
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000000460 chlorine Substances 0.000 claims abstract description 17
- 229910052801 chlorine Inorganic materials 0.000 claims abstract description 17
- 239000002904 solvent Substances 0.000 claims abstract description 9
- 239000000243 solution Substances 0.000 abstract description 20
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract description 19
- 229910000041 hydrogen chloride Inorganic materials 0.000 abstract description 19
- 238000000034 method Methods 0.000 abstract description 14
- 239000007864 aqueous solution Substances 0.000 abstract description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 abstract description 5
- 150000001875 compounds Chemical class 0.000 abstract description 4
- 239000002994 raw material Substances 0.000 abstract description 4
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 abstract description 3
- CTKINSOISVBQLD-UHFFFAOYSA-N Glycidol Chemical compound OCC1CO1 CTKINSOISVBQLD-UHFFFAOYSA-N 0.000 abstract description 2
- 239000003822 epoxy resin Substances 0.000 abstract description 2
- 229920000647 polyepoxide Polymers 0.000 abstract description 2
- 229920003051 synthetic elastomer Polymers 0.000 abstract 1
- 239000005061 synthetic rubber Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 description 9
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 6
- 238000007086 side reaction Methods 0.000 description 5
- PUNGDGIPJMLONU-UHFFFAOYSA-N 3,3-dichloropropan-1-ol Chemical compound OCCC(Cl)Cl PUNGDGIPJMLONU-UHFFFAOYSA-N 0.000 description 4
- OSDWBNJEKMUWAV-UHFFFAOYSA-N Allyl chloride Chemical compound ClCC=C OSDWBNJEKMUWAV-UHFFFAOYSA-N 0.000 description 4
- 238000004817 gas chromatography Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- 229940044613 1-propanol Drugs 0.000 description 2
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 description 2
- 238000005660 chlorination reaction Methods 0.000 description 2
- IGJWHVUMEJASKV-UHFFFAOYSA-N chloronium Chemical compound [ClH2+] IGJWHVUMEJASKV-UHFFFAOYSA-N 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- -1 ether compound Chemical class 0.000 description 2
- 150000002170 ethers Chemical class 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 1
- QGJOPFRUJISHPQ-NJFSPNSNSA-N carbon disulfide-14c Chemical compound S=[14C]=S QGJOPFRUJISHPQ-NJFSPNSNSA-N 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- XPFVYQJUAUNWIW-UHFFFAOYSA-N furfuryl alcohol Chemical compound OCC1=CC=CO1 XPFVYQJUAUNWIW-UHFFFAOYSA-N 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP15879085A JPS6219544A (ja) | 1985-07-18 | 1985-07-18 | ２，３−ジクロル−１−プロパノ−ルの製法 |
| US07/083,190 US4788351A (en) | 1985-07-18 | 1987-08-10 | Process for the production of 2,3-dichloro-1-propanol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP15879085A JPS6219544A (ja) | 1985-07-18 | 1985-07-18 | ２，３−ジクロル−１−プロパノ−ルの製法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6219544A true JPS6219544A (ja) | 1987-01-28 |
| JPS646177B2 JPS646177B2 (enrdf_load_stackoverflow) | 1989-02-02 |
Family
ID=15679398
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP15879085A Granted JPS6219544A (ja) | 1985-07-18 | 1985-07-18 | ２，３−ジクロル−１−プロパノ−ルの製法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6219544A (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63290835A (ja) * | 1987-05-21 | 1988-11-28 | Showa Denko Kk | ２，３−ジクロロ−１−プロパノ−ルの製造法 |
| US4788351A (en) * | 1985-07-18 | 1988-11-29 | Osaka Soda Co., Ltd. | Process for the production of 2,3-dichloro-1-propanol |
-
1985
- 1985-07-18 JP JP15879085A patent/JPS6219544A/ja active Granted
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4788351A (en) * | 1985-07-18 | 1988-11-29 | Osaka Soda Co., Ltd. | Process for the production of 2,3-dichloro-1-propanol |
| JPS63290835A (ja) * | 1987-05-21 | 1988-11-28 | Showa Denko Kk | ２，３−ジクロロ−１−プロパノ−ルの製造法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS646177B2 (enrdf_load_stackoverflow) | 1989-02-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |