JPS6212746A - アセトアセチル化ポリブタジエン系オリゴマーの製造方法 - Google Patents
アセトアセチル化ポリブタジエン系オリゴマーの製造方法Info
- Publication number
- JPS6212746A JPS6212746A JP15274485A JP15274485A JPS6212746A JP S6212746 A JPS6212746 A JP S6212746A JP 15274485 A JP15274485 A JP 15274485A JP 15274485 A JP15274485 A JP 15274485A JP S6212746 A JPS6212746 A JP S6212746A
- Authority
- JP
- Japan
- Prior art keywords
- oligomer
- acetoacetylated
- diketene
- volume
- liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- WASQWSOJHCZDFK-UHFFFAOYSA-N diketene Chemical compound C=C1CC(=O)O1 WASQWSOJHCZDFK-UHFFFAOYSA-N 0.000 claims abstract description 15
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims abstract description 12
- 239000003054 catalyst Substances 0.000 claims abstract description 4
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 abstract description 15
- 150000001875 compounds Chemical class 0.000 abstract description 8
- 238000006243 chemical reaction Methods 0.000 abstract description 7
- 239000000853 adhesive Substances 0.000 abstract description 5
- 230000001070 adhesive effect Effects 0.000 abstract description 5
- 239000003431 cross linking reagent Substances 0.000 abstract description 5
- 229920000642 polymer Polymers 0.000 abstract description 5
- 239000004372 Polyvinyl alcohol Substances 0.000 abstract description 4
- 229920002451 polyvinyl alcohol Polymers 0.000 abstract description 4
- 239000007787 solid Substances 0.000 abstract description 3
- 239000002904 solvent Substances 0.000 abstract description 2
- 239000011345 viscous material Substances 0.000 abstract description 2
- 239000011344 liquid material Substances 0.000 abstract 1
- 239000007788 liquid Substances 0.000 description 16
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Substances CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 12
- 239000005062 Polybutadiene Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 229920002589 poly(vinylethylene) polymer Polymers 0.000 description 4
- 229920002857 polybutadiene Polymers 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 229910001873 dinitrogen Inorganic materials 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 238000010926 purge Methods 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical class OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 229920000459 Nitrile rubber Polymers 0.000 description 2
- 229920002873 Polyethylenimine Polymers 0.000 description 2
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 239000000539 dimer Substances 0.000 description 2
- 238000011038 discontinuous diafiltration by volume reduction Methods 0.000 description 2
- 239000003822 epoxy resin Substances 0.000 description 2
- 229920000647 polyepoxide Polymers 0.000 description 2
- 239000001632 sodium acetate Substances 0.000 description 2
- 235000017281 sodium acetate Nutrition 0.000 description 2
- QDRKDTQENPPHOJ-UHFFFAOYSA-N sodium ethoxide Chemical compound [Na+].CC[O-] QDRKDTQENPPHOJ-UHFFFAOYSA-N 0.000 description 2
- 229910014033 C-OH Inorganic materials 0.000 description 1
- 229910014570 C—OH Inorganic materials 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 229920003006 Polybutadiene acrylonitrile Polymers 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 150000001993 dienes Chemical class 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 238000007720 emulsion polymerization reaction Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 238000010550 living polymerization reaction Methods 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920001084 poly(chloroprene) Polymers 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920000768 polyamine Polymers 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- -1 polyoxyethylene Polymers 0.000 description 1
- 229920001451 polypropylene glycol Polymers 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- FDRCDNZGSXJAFP-UHFFFAOYSA-M sodium chloroacetate Chemical compound [Na+].[O-]C(=O)CCl FDRCDNZGSXJAFP-UHFFFAOYSA-M 0.000 description 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyethers (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP15274485A JPS6212746A (ja) | 1985-07-11 | 1985-07-11 | アセトアセチル化ポリブタジエン系オリゴマーの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP15274485A JPS6212746A (ja) | 1985-07-11 | 1985-07-11 | アセトアセチル化ポリブタジエン系オリゴマーの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6212746A true JPS6212746A (ja) | 1987-01-21 |
| JPH0513142B2 JPH0513142B2 (OSRAM) | 1993-02-19 |
Family
ID=15547208
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP15274485A Granted JPS6212746A (ja) | 1985-07-11 | 1985-07-11 | アセトアセチル化ポリブタジエン系オリゴマーの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6212746A (OSRAM) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR19990059023A (ko) * | 1997-12-30 | 1999-07-26 | 안용찬 | 2-분지쇄-3-히드록시지방산 및 그 염의 제조방법 |
| CN104045558A (zh) * | 2013-03-15 | 2014-09-17 | 江苏天成生化制品有限公司 | 一种乙酰乙酸甲酯生产传质工艺 |
| JP2019501265A (ja) * | 2016-01-06 | 2019-01-17 | フィナ テクノロジー，インコーポレイティド | 硬化可能なポリファルネセンベース組成物 |
| US11466118B2 (en) | 2019-11-22 | 2022-10-11 | Fina Technology, Inc. | Chain end hydroxyl functionalized branched polyfarnesenes obtained by radical polymerization |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS49116020A (OSRAM) * | 1973-03-16 | 1974-11-06 | ||
| JPS55113723A (en) * | 1979-02-26 | 1980-09-02 | Ko Kamata | Drug composition to be absorbed in digestive canal |
| JPS5615243A (en) * | 1979-07-11 | 1981-02-14 | Hoechst Ag | Acetylacetoxyalkyllarylether* its manufacture and its use |
-
1985
- 1985-07-11 JP JP15274485A patent/JPS6212746A/ja active Granted
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS49116020A (OSRAM) * | 1973-03-16 | 1974-11-06 | ||
| JPS55113723A (en) * | 1979-02-26 | 1980-09-02 | Ko Kamata | Drug composition to be absorbed in digestive canal |
| JPS5615243A (en) * | 1979-07-11 | 1981-02-14 | Hoechst Ag | Acetylacetoxyalkyllarylether* its manufacture and its use |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR19990059023A (ko) * | 1997-12-30 | 1999-07-26 | 안용찬 | 2-분지쇄-3-히드록시지방산 및 그 염의 제조방법 |
| CN104045558A (zh) * | 2013-03-15 | 2014-09-17 | 江苏天成生化制品有限公司 | 一种乙酰乙酸甲酯生产传质工艺 |
| JP2019501265A (ja) * | 2016-01-06 | 2019-01-17 | フィナ テクノロジー，インコーポレイティド | 硬化可能なポリファルネセンベース組成物 |
| US11634531B2 (en) | 2016-01-06 | 2023-04-25 | Fina Technology, Inc. | Curable polyfarnesene-based compositions |
| US11466118B2 (en) | 2019-11-22 | 2022-10-11 | Fina Technology, Inc. | Chain end hydroxyl functionalized branched polyfarnesenes obtained by radical polymerization |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0513142B2 (OSRAM) | 1993-02-19 |
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