JPS62111671A - 生コ−ヒ−豆からの食品用天然抗酸化剤の製造方法 - Google Patents
生コ−ヒ−豆からの食品用天然抗酸化剤の製造方法Info
- Publication number
- JPS62111671A JPS62111671A JP25229285A JP25229285A JPS62111671A JP S62111671 A JPS62111671 A JP S62111671A JP 25229285 A JP25229285 A JP 25229285A JP 25229285 A JP25229285 A JP 25229285A JP S62111671 A JPS62111671 A JP S62111671A
- Authority
- JP
- Japan
- Prior art keywords
- coffee beans
- green coffee
- antioxidant
- raw coffee
- pulverization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003963 antioxidant agent Substances 0.000 title claims abstract description 30
- 241000533293 Sesbania emerus Species 0.000 title claims abstract description 28
- 230000003078 antioxidant effect Effects 0.000 title claims abstract description 22
- 235000013305 food Nutrition 0.000 title claims abstract description 5
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- 238000000034 method Methods 0.000 claims abstract description 15
- 238000010298 pulverizing process Methods 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 4
- 239000002245 particle Substances 0.000 claims description 9
- 238000000227 grinding Methods 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 1
- 238000003809 water extraction Methods 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 4
- 239000007788 liquid Substances 0.000 abstract description 3
- 230000003064 anti-oxidating effect Effects 0.000 abstract 1
- 238000004108 freeze drying Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 10
- 108090000790 Enzymes Proteins 0.000 description 9
- 102000004190 Enzymes Human genes 0.000 description 9
- 229940088598 enzyme Drugs 0.000 description 9
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
- 238000000605 extraction Methods 0.000 description 8
- 239000007787 solid Substances 0.000 description 8
- 238000001914 filtration Methods 0.000 description 7
- QAIPRVGONGVQAS-DUXPYHPUSA-N trans-caffeic acid Chemical class OC(=O)\C=C\C1=CC=C(O)C(O)=C1 QAIPRVGONGVQAS-DUXPYHPUSA-N 0.000 description 7
- 239000012153 distilled water Substances 0.000 description 6
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 5
- 239000012085 test solution Substances 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 238000005238 degreasing Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000003208 petroleum Substances 0.000 description 4
- ACEAELOMUCBPJP-UHFFFAOYSA-N (E)-3,4,5-trihydroxycinnamic acid Natural products OC(=O)C=CC1=CC(O)=C(O)C(O)=C1 ACEAELOMUCBPJP-UHFFFAOYSA-N 0.000 description 3
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 235000004883 caffeic acid Nutrition 0.000 description 3
- 229940074360 caffeic acid Drugs 0.000 description 3
- QAIPRVGONGVQAS-UHFFFAOYSA-N cis-caffeic acid Natural products OC(=O)C=CC1=CC=C(O)C(O)=C1 QAIPRVGONGVQAS-UHFFFAOYSA-N 0.000 description 3
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 3
- 235000020778 linoleic acid Nutrition 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- CWVRJTMFETXNAD-FWCWNIRPSA-N 3-O-Caffeoylquinic acid Natural products O[C@H]1[C@@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-FWCWNIRPSA-N 0.000 description 2
- NGSWKAQJJWESNS-UHFFFAOYSA-N 4-coumaric acid Chemical compound OC(=O)C=CC1=CC=C(O)C=C1 NGSWKAQJJWESNS-UHFFFAOYSA-N 0.000 description 2
- PZIRUHCJZBGLDY-UHFFFAOYSA-N Caffeoylquinic acid Natural products CC(CCC(=O)C(C)C1C(=O)CC2C3CC(O)C4CC(O)CCC4(C)C3CCC12C)C(=O)O PZIRUHCJZBGLDY-UHFFFAOYSA-N 0.000 description 2
- CWVRJTMFETXNAD-KLZCAUPSSA-N Neochlorogenin-saeure Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O CWVRJTMFETXNAD-KLZCAUPSSA-N 0.000 description 2
- 238000002835 absorbance Methods 0.000 description 2
- 238000007605 air drying Methods 0.000 description 2
- 239000013040 bath agent Substances 0.000 description 2
- 235000001368 chlorogenic acid Nutrition 0.000 description 2
- CWVRJTMFETXNAD-JUHZACGLSA-N chlorogenic acid Chemical compound O[C@@H]1[C@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-JUHZACGLSA-N 0.000 description 2
- 229940074393 chlorogenic acid Drugs 0.000 description 2
- FFQSDFBBSXGVKF-KHSQJDLVSA-N chlorogenic acid Natural products O[C@@H]1C[C@](O)(C[C@@H](CC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O FFQSDFBBSXGVKF-KHSQJDLVSA-N 0.000 description 2
- BMRSEYFENKXDIS-KLZCAUPSSA-N cis-3-O-p-coumaroylquinic acid Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)cc2)[C@@H]1O)C(=O)O BMRSEYFENKXDIS-KLZCAUPSSA-N 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000007710 freezing Methods 0.000 description 2
- 230000008014 freezing Effects 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 150000002978 peroxides Chemical class 0.000 description 2
- NJYFRQQXXXRJHK-UHFFFAOYSA-N (4-aminophenyl) thiocyanate Chemical compound NC1=CC=C(SC#N)C=C1 NJYFRQQXXXRJHK-UHFFFAOYSA-N 0.000 description 1
- KSEBMYQBYZTDHS-HWKANZROSA-M (E)-Ferulic acid Natural products COC1=CC(\C=C\C([O-])=O)=CC=C1O KSEBMYQBYZTDHS-HWKANZROSA-M 0.000 description 1
- NGSWKAQJJWESNS-ZZXKWVIFSA-M 4-Hydroxycinnamate Natural products OC1=CC=C(\C=C\C([O-])=O)C=C1 NGSWKAQJJWESNS-ZZXKWVIFSA-M 0.000 description 1
- DFYRUELUNQRZTB-UHFFFAOYSA-N Acetovanillone Natural products COC1=CC(C(C)=O)=CC=C1O DFYRUELUNQRZTB-UHFFFAOYSA-N 0.000 description 1
- 108091005508 Acid proteases Proteins 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- 108010059892 Cellulase Proteins 0.000 description 1
- 108091005804 Peptidases Proteins 0.000 description 1
- 239000004365 Protease Substances 0.000 description 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- SOIFLUNRINLCBN-UHFFFAOYSA-N ammonium thiocyanate Chemical compound [NH4+].[S-]C#N SOIFLUNRINLCBN-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 229940106157 cellulase Drugs 0.000 description 1
- -1 chlorogenic acid Chemical class 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 235000013365 dairy product Nutrition 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 229960002089 ferrous chloride Drugs 0.000 description 1
- 235000001785 ferulic acid Nutrition 0.000 description 1
- KSEBMYQBYZTDHS-HWKANZROSA-N ferulic acid Chemical compound COC1=CC(\C=C\C(O)=O)=CC=C1O KSEBMYQBYZTDHS-HWKANZROSA-N 0.000 description 1
- 229940114124 ferulic acid Drugs 0.000 description 1
- KSEBMYQBYZTDHS-UHFFFAOYSA-N ferulic acid Natural products COC1=CC(C=CC(O)=O)=CC=C1O KSEBMYQBYZTDHS-UHFFFAOYSA-N 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical compound Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- QURCVMIEKCOAJU-UHFFFAOYSA-N trans-isoferulic acid Natural products COC1=CC=C(C=CC(O)=O)C=C1O QURCVMIEKCOAJU-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
- Anti-Oxidant Or Stabilizer Compositions (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP25229285A JPS62111671A (ja) | 1985-11-11 | 1985-11-11 | 生コ−ヒ−豆からの食品用天然抗酸化剤の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP25229285A JPS62111671A (ja) | 1985-11-11 | 1985-11-11 | 生コ−ヒ−豆からの食品用天然抗酸化剤の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS62111671A true JPS62111671A (ja) | 1987-05-22 |
| JPH0559696B2 JPH0559696B2 (enExample) | 1993-08-31 |
Family
ID=17235227
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP25229285A Granted JPS62111671A (ja) | 1985-11-11 | 1985-11-11 | 生コ−ヒ−豆からの食品用天然抗酸化剤の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS62111671A (enExample) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05236918A (ja) * | 1992-02-27 | 1993-09-17 | Umezawa:Kk | 食用天然抗酸化保存剤の製造法 |
| EP0714968A2 (en) | 1994-12-02 | 1996-06-05 | Ucc Ueshima Coffee Co., Ltd. | Natural antioxidant and method of preparing the same |
| JPH1042787A (ja) * | 1996-08-05 | 1998-02-17 | Ogawa Koryo Kk | フレーバー用熱劣化抑制剤 |
| WO2005032570A1 (ja) * | 2003-10-06 | 2005-04-14 | Oryza Oil & Fat Chemical Co., Ltd. | ダイエット用組成物 |
| JP2006335758A (ja) * | 2003-10-06 | 2006-12-14 | Oriza Yuka Kk | ダイエット用組成物 |
| KR100687546B1 (ko) * | 1999-05-13 | 2007-02-27 | 가부시키가이샤 도요학코 | Sod작용을 가진 조성물, 및 이를 함유하는 혈압억제제 |
| US7713566B2 (en) | 1999-12-21 | 2010-05-11 | Zapp Loretta M | Method for enhancing post-processing content of beneficial compounds in beverages |
| WO2012005293A1 (ja) | 2010-07-06 | 2012-01-12 | 花王株式会社 | 精製クロロゲン酸類含有製剤の製造方法 |
| GB2482032A (en) * | 2010-07-16 | 2012-01-18 | Kraft Foods R & D Inc | Coffee milling process |
| US9101648B2 (en) | 2009-03-26 | 2015-08-11 | Intercontinental Great Brands Llc | Pharmaceutical composition comprising mannooligosaccharides derived from coffee for treatment of lifestyle-related disease, and food useful for treatment of lifestyle-related disease |
| WO2018211845A1 (ja) | 2017-05-18 | 2018-11-22 | 花王株式会社 | 食品組成物 |
| WO2019069981A1 (ja) | 2017-10-03 | 2019-04-11 | 花王株式会社 | ホットフラッシュ改善剤 |
-
1985
- 1985-11-11 JP JP25229285A patent/JPS62111671A/ja active Granted
Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05236918A (ja) * | 1992-02-27 | 1993-09-17 | Umezawa:Kk | 食用天然抗酸化保存剤の製造法 |
| EP0714968A2 (en) | 1994-12-02 | 1996-06-05 | Ucc Ueshima Coffee Co., Ltd. | Natural antioxidant and method of preparing the same |
| JPH1042787A (ja) * | 1996-08-05 | 1998-02-17 | Ogawa Koryo Kk | フレーバー用熱劣化抑制剤 |
| KR100687546B1 (ko) * | 1999-05-13 | 2007-02-27 | 가부시키가이샤 도요학코 | Sod작용을 가진 조성물, 및 이를 함유하는 혈압억제제 |
| US8357419B2 (en) | 1999-12-21 | 2013-01-22 | Loretta Zapp | Method for enhancing post-processing content of beneficial compounds in beverages naturally containing same |
| US7713566B2 (en) | 1999-12-21 | 2010-05-11 | Zapp Loretta M | Method for enhancing post-processing content of beneficial compounds in beverages |
| WO2005032570A1 (ja) * | 2003-10-06 | 2005-04-14 | Oryza Oil & Fat Chemical Co., Ltd. | ダイエット用組成物 |
| JP2006335758A (ja) * | 2003-10-06 | 2006-12-14 | Oriza Yuka Kk | ダイエット用組成物 |
| JPWO2005032570A1 (ja) * | 2003-10-06 | 2007-11-15 | オリザ油化株式会社 | ダイエット用組成物 |
| CN1863543B (zh) | 2003-10-06 | 2010-06-16 | 奥力榨油化株式会社 | 减肥用组合物 |
| JP4499665B2 (ja) * | 2003-10-06 | 2010-07-07 | オリザ油化株式会社 | ダイエット用組成物 |
| US8802164B2 (en) | 2003-10-06 | 2014-08-12 | Oryza Oil & Fat Chemical Co., Ltd. | Method for promoting carnitine palmitoyltransferase activity using green coffee bean extract |
| US9101648B2 (en) | 2009-03-26 | 2015-08-11 | Intercontinental Great Brands Llc | Pharmaceutical composition comprising mannooligosaccharides derived from coffee for treatment of lifestyle-related disease, and food useful for treatment of lifestyle-related disease |
| WO2012005293A1 (ja) | 2010-07-06 | 2012-01-12 | 花王株式会社 | 精製クロロゲン酸類含有製剤の製造方法 |
| GB2482032B (en) * | 2010-07-16 | 2013-04-10 | Kraft Foods R & D Inc | Coffee products and related processes |
| GB2482032A (en) * | 2010-07-16 | 2012-01-18 | Kraft Foods R & D Inc | Coffee milling process |
| US9357791B2 (en) | 2010-07-16 | 2016-06-07 | Kraft Foods R & D, Inc. | Coffee products and related processes |
| US10194675B2 (en) | 2010-07-16 | 2019-02-05 | Kraft Foods R&D, Inc. | Coffee products and related processes |
| WO2018211845A1 (ja) | 2017-05-18 | 2018-11-22 | 花王株式会社 | 食品組成物 |
| WO2019069981A1 (ja) | 2017-10-03 | 2019-04-11 | 花王株式会社 | ホットフラッシュ改善剤 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0559696B2 (enExample) | 1993-08-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |