JPS6143286B2 - - Google Patents
Info
- Publication number
- JPS6143286B2 JPS6143286B2 JP56177694A JP17769481A JPS6143286B2 JP S6143286 B2 JPS6143286 B2 JP S6143286B2 JP 56177694 A JP56177694 A JP 56177694A JP 17769481 A JP17769481 A JP 17769481A JP S6143286 B2 JPS6143286 B2 JP S6143286B2
- Authority
- JP
- Japan
- Prior art keywords
- zirconia
- solution
- hydrogen peroxide
- monoclinic
- particles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 100
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 50
- 239000000243 solution Substances 0.000 claims description 27
- 238000004519 manufacturing process Methods 0.000 claims description 21
- 239000002245 particle Substances 0.000 claims description 21
- 238000000034 method Methods 0.000 claims description 17
- 239000007864 aqueous solution Substances 0.000 claims description 15
- 150000003754 zirconium Chemical class 0.000 claims description 12
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 6
- 229910052726 zirconium Inorganic materials 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 description 14
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 12
- 238000009835 boiling Methods 0.000 description 10
- IPCAPQRVQMIMAN-UHFFFAOYSA-L zirconyl chloride Chemical compound Cl[Zr](Cl)=O IPCAPQRVQMIMAN-UHFFFAOYSA-L 0.000 description 10
- 230000000694 effects Effects 0.000 description 9
- 239000010419 fine particle Substances 0.000 description 9
- 239000000843 powder Substances 0.000 description 8
- 239000011882 ultra-fine particle Substances 0.000 description 8
- 239000013078 crystal Substances 0.000 description 7
- 238000007796 conventional method Methods 0.000 description 6
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 5
- 235000011114 ammonium hydroxide Nutrition 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 238000010992 reflux Methods 0.000 description 5
- 239000012266 salt solution Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- 229910021529 ammonia Inorganic materials 0.000 description 4
- 239000003957 anion exchange resin Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 230000001737 promoting effect Effects 0.000 description 4
- 238000006460 hydrolysis reaction Methods 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 230000006911 nucleation Effects 0.000 description 2
- 238000010899 nucleation Methods 0.000 description 2
- 238000000634 powder X-ray diffraction Methods 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000011163 secondary particle Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- SPAGIJMPHSUYSE-UHFFFAOYSA-N Magnesium peroxide Chemical compound [Mg+2].[O-][O-] SPAGIJMPHSUYSE-UHFFFAOYSA-N 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 229920001429 chelating resin Polymers 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000007731 hot pressing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000009766 low-temperature sintering Methods 0.000 description 1
- 229960004995 magnesium peroxide Drugs 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000006224 matting agent Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- PFUVRDFDKPNGAV-UHFFFAOYSA-N sodium peroxide Chemical compound [Na+].[Na+].[O-][O-] PFUVRDFDKPNGAV-UHFFFAOYSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP17769481A JPS5879818A (ja) | 1981-11-05 | 1981-11-05 | 結晶質ジルコニアのコロイドゾル及びその製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP17769481A JPS5879818A (ja) | 1981-11-05 | 1981-11-05 | 結晶質ジルコニアのコロイドゾル及びその製造方法 |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60266830A Division JPH0764563B2 (ja) | 1985-11-27 | 1985-11-27 | 結晶質ジルコニアの微粉末及びその製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5879818A JPS5879818A (ja) | 1983-05-13 |
| JPS6143286B2 true JPS6143286B2 (ko) | 1986-09-26 |
Family
ID=16035467
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP17769481A Granted JPS5879818A (ja) | 1981-11-05 | 1981-11-05 | 結晶質ジルコニアのコロイドゾル及びその製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5879818A (ko) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9902655B2 (en) | 2013-10-18 | 2018-02-27 | Daiichi Kigenso Kagaku Kogyo Co., Ltd. | Zirconium oxide-titanium oxide composite sol and production method thereof |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2578241B1 (fr) * | 1985-03-01 | 1990-03-30 | Rhone Poulenc Spec Chim | Zircone stabilisee, son procede de preparation et son application dans des compositions ceramiques |
| JPS61201623A (ja) * | 1985-03-04 | 1986-09-06 | Etsuro Kato | ジルコニア超微結晶の球状凝集粒子の製造方法 |
| JPH0651568B2 (ja) * | 1985-11-29 | 1994-07-06 | 電気化学工業株式会社 | 酸化ジルコニウム系微粉末の製法 |
| JPH0712930B2 (ja) * | 1985-12-10 | 1995-02-15 | 悦朗 加藤 | 単斜ジルコニア超微結晶の繊維束状配向凝集粒子および製造方法 |
| JP2550547B2 (ja) * | 1986-12-19 | 1996-11-06 | 日産化学工業株式会社 | セラミツクス成型物の改質法 |
| US5223176A (en) * | 1988-09-30 | 1993-06-29 | Nissan Chemical Industries, Ltd. | Zirconia sol and method for making the same |
| US5037579A (en) * | 1990-02-12 | 1991-08-06 | Nalco Chemical Company | Hydrothermal process for producing zirconia sol |
| JP4106037B2 (ja) | 2004-03-01 | 2008-06-25 | 富士フイルム株式会社 | インクジェット記録媒体 |
| CN101160263B (zh) | 2005-04-18 | 2011-05-11 | 日产化学工业株式会社 | 酸性氧化锆溶胶和其制备方法 |
| JP4582789B2 (ja) * | 2005-07-25 | 2010-11-17 | 多木化学株式会社 | セリア−ジルコニア固溶体ゾル及びその製造方法 |
| JP5253095B2 (ja) * | 2007-12-20 | 2013-07-31 | 日揮触媒化成株式会社 | ジルコニアゾルの製造方法 |
-
1981
- 1981-11-05 JP JP17769481A patent/JPS5879818A/ja active Granted
Non-Patent Citations (1)
| Title |
|---|
| POWDER TECHNOLOGY=1980 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9902655B2 (en) | 2013-10-18 | 2018-02-27 | Daiichi Kigenso Kagaku Kogyo Co., Ltd. | Zirconium oxide-titanium oxide composite sol and production method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5879818A (ja) | 1983-05-13 |
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