JPS5925820B2 - ３，３，３−トリフルオロ−２−トリフルオロメチルプロペン／ふつ化ビニリデン共重合体とポリテトラフルオロエチレンとの組成物 - Google Patents
３，３，３−トリフルオロ−２−トリフルオロメチルプロペン／ふつ化ビニリデン共重合体とポリテトラフルオロエチレンとの組成物Info
- Publication number
- JPS5925820B2 JPS5925820B2 JP50125990A JP12599075A JPS5925820B2 JP S5925820 B2 JPS5925820 B2 JP S5925820B2 JP 50125990 A JP50125990 A JP 50125990A JP 12599075 A JP12599075 A JP 12599075A JP S5925820 B2 JPS5925820 B2 JP S5925820B2
- Authority
- JP
- Japan
- Prior art keywords
- composition
- weight
- trifluoromethylpropene
- copolymer
- trifluoro
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000203 mixture Substances 0.000 title claims description 47
- 229920001577 copolymer Polymers 0.000 title claims description 32
- 229920001343 polytetrafluoroethylene Polymers 0.000 title claims description 18
- 239000004810 polytetrafluoroethylene Substances 0.000 title claims description 18
- -1 polytetrafluoroethylene Polymers 0.000 title claims description 6
- QMIWYOZFFSLIAK-UHFFFAOYSA-N 3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene Chemical group FC(F)(F)C(=C)C(F)(F)F QMIWYOZFFSLIAK-UHFFFAOYSA-N 0.000 title description 9
- 239000002245 particle Substances 0.000 claims description 16
- BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 claims description 9
- 239000000155 melt Substances 0.000 claims 1
- 239000011347 resin Substances 0.000 claims 1
- 229920005989 resin Polymers 0.000 claims 1
- 238000000576 coating method Methods 0.000 description 20
- 239000000758 substrate Substances 0.000 description 18
- 239000011248 coating agent Substances 0.000 description 13
- 238000000034 method Methods 0.000 description 10
- 239000000843 powder Substances 0.000 description 10
- 238000002844 melting Methods 0.000 description 6
- 230000008018 melting Effects 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 6
- 239000002184 metal Substances 0.000 description 6
- 239000007788 liquid Substances 0.000 description 5
- 239000003381 stabilizer Substances 0.000 description 5
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 4
- 238000005299 abrasion Methods 0.000 description 4
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 4
- 239000000292 calcium oxide Substances 0.000 description 4
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 4
- 239000004744 fabric Substances 0.000 description 4
- 239000003365 glass fiber Substances 0.000 description 4
- 229940098458 powder spray Drugs 0.000 description 4
- 238000009736 wetting Methods 0.000 description 4
- 239000000654 additive Substances 0.000 description 3
- 239000011152 fibreglass Substances 0.000 description 3
- 239000010410 layer Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 150000002739 metals Chemical class 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N Propene Chemical compound CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 description 2
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 2
- 238000007334 copolymerization reaction Methods 0.000 description 2
- 239000004205 dimethyl polysiloxane Substances 0.000 description 2
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 2
- 238000001125 extrusion Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 229920001296 polysiloxane Polymers 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- 230000005855 radiation Effects 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 239000011787 zinc oxide Substances 0.000 description 2
- ICTYZHTZZOUENE-UHFFFAOYSA-N 1,1,1-trifluorobut-2-ene Chemical compound CC=CC(F)(F)F ICTYZHTZZOUENE-UHFFFAOYSA-N 0.000 description 1
- GUTLYIVDDKVIGB-OUBTZVSYSA-N Cobalt-60 Chemical compound [60Co] GUTLYIVDDKVIGB-OUBTZVSYSA-N 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 239000010425 asbestos Substances 0.000 description 1
- CXKCTMHTOKXKQT-UHFFFAOYSA-N cadmium oxide Inorganic materials [Cd]=O CXKCTMHTOKXKQT-UHFFFAOYSA-N 0.000 description 1
- CFEAAQFZALKQPA-UHFFFAOYSA-N cadmium(2+);oxygen(2-) Chemical compound [O-2].[Cd+2] CFEAAQFZALKQPA-UHFFFAOYSA-N 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- UUAGAQFQZIEFAH-UHFFFAOYSA-N chlorotrifluoroethylene Chemical group FC(F)=C(F)Cl UUAGAQFQZIEFAH-UHFFFAOYSA-N 0.000 description 1
- 239000008199 coating composition Substances 0.000 description 1
- 239000011247 coating layer Substances 0.000 description 1
- 239000007822 coupling agent Substances 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000001746 injection moulding Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910000464 lead oxide Inorganic materials 0.000 description 1
- HTUMBQDCCIXGCV-UHFFFAOYSA-N lead oxide Chemical compound [O-2].[Pb+2] HTUMBQDCCIXGCV-UHFFFAOYSA-N 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000007750 plasma spraying Methods 0.000 description 1
- 239000003505 polymerization initiator Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 239000012744 reinforcing agent Substances 0.000 description 1
- 230000003252 repetitive effect Effects 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000005488 sandblasting Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 229920001187 thermosetting polymer Polymers 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L27/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers
- C08L27/02—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L27/12—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
- C08L27/16—Homopolymers or copolymers or vinylidene fluoride
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L27/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers
- C08L27/02—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L27/12—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
- C08L27/18—Homopolymers or copolymers or tetrafluoroethene
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S525/00—Synthetic resins or natural rubbers -- part of the class 520 series
- Y10S525/934—Powdered coating composition
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/3154—Of fluorinated addition polymer from unsaturated monomers
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/516,712 US3962373A (en) | 1974-10-21 | 1974-10-21 | Compositions of 3,3,3-trifluoro-2-trifluoromethyl propene/vinylidene fluoride copolymer and polytetrafluoroethylene |
| US516712 | 1974-10-21 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5165157A JPS5165157A (en) | 1976-06-05 |
| JPS5925820B2 true JPS5925820B2 (ja) | 1984-06-21 |
Family
ID=24056790
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP50125990A Expired JPS5925820B2 (ja) | 1974-10-21 | 1975-10-21 | ３，３，３−トリフルオロ−２−トリフルオロメチルプロペン／ふつ化ビニリデン共重合体とポリテトラフルオロエチレンとの組成物 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US3962373A (enExample) |
| JP (1) | JPS5925820B2 (enExample) |
| CA (1) | CA1056093A (enExample) |
| DE (1) | DE2545897C2 (enExample) |
| FR (1) | FR2288763A1 (enExample) |
| GB (1) | GB1487028A (enExample) |
| IT (1) | IT1048240B (enExample) |
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4110186A (en) * | 1975-05-13 | 1978-08-29 | Beatrice Foods Co. | Fluorinated ethylene-propylene copolymer powders having improved adhesion to substrates and method |
| JPS53149881A (en) * | 1977-06-03 | 1978-12-27 | Asahi Glass Co Ltd | Strengthened cation exchange resin membrane and production thereof |
| FR2395289A1 (fr) * | 1977-06-24 | 1979-01-19 | Ugine Kuhlmann | Compositions thermoplastiques lubrifiees a base de poly(fluorure de vinylidene) |
| US4351882A (en) * | 1981-01-13 | 1982-09-28 | E. I. Du Pont De Nemours And Company | Article coated with fluoropolymer finish with improved durability |
| US5025131A (en) * | 1981-09-09 | 1991-06-18 | Raychem Corporation | Method of heating diesel fuel utilizing conductive polymer heating elements |
| US5093898A (en) * | 1981-09-09 | 1992-03-03 | Raychem Corporation | Electrical device utilizing conductive polymer composition |
| JPS5941350A (ja) * | 1982-08-31 | 1984-03-07 | Daikin Ind Ltd | 改良された含フツ素熱可塑性ゴム組成物 |
| US4504528A (en) * | 1983-07-11 | 1985-03-12 | Rm Industrial Products Company, Inc. | Process for coating aqueous fluoropolymer coating on porous substrate |
| US4988566A (en) * | 1983-11-07 | 1991-01-29 | Glaister Frank J | Fluorocarbon polymer compositions and articles shaped therefrom |
| GB2185046A (en) * | 1985-11-29 | 1987-07-08 | Square Grip Ltd | Concrete reinforcing elements allowing for relative movement between concrete and element |
| US4655945A (en) * | 1986-01-28 | 1987-04-07 | Peter J. Balsells | Bearing seal and method of manufacture |
| JP2591664B2 (ja) * | 1988-08-09 | 1997-03-19 | 大日精化工業株式会社 | 粉体塗料組成物 |
| JP2876375B2 (ja) * | 1993-02-22 | 1999-03-31 | 株式会社 金陽社 | ロール |
| US5695197A (en) * | 1996-12-06 | 1997-12-09 | Farley; Michael L. | Seal ring method of sealing and molding composition comprising blend of PTFE copolymer, polyamide and carbon fiber therefor |
| US6117508A (en) * | 1997-06-27 | 2000-09-12 | Dyneon Llc | Composite articles including a fluoropolymer blend |
| US6308392B1 (en) * | 1999-07-12 | 2001-10-30 | U.S. Welding International, Ltd. | Brittle wire manufacturing method and apparatus |
| DK1313611T3 (da) | 2000-08-17 | 2009-10-05 | Whitford Corp | Enkeltovertrukket, ikke-klæbende overtrækssystem og genstande overtrukket hermed |
| US6846570B2 (en) * | 2000-08-17 | 2005-01-25 | Whitford Corporation | Multiple coat non-stick coating system and articles coated with same |
| PL209218B1 (pl) * | 2002-04-23 | 2011-08-31 | Laurel Products | Sposób obróbki perfluoropolimeru i kompozycja na bazie perfluoropolimeru |
| EP1661947B1 (en) * | 2003-08-25 | 2016-05-11 | Daikin Industries, Ltd. | Product for high-frequency signal transmission, process for producing the same and high-frequency transmission cable |
| FR2864465B1 (fr) * | 2003-12-31 | 2007-10-19 | Arkema | Plaques de polymere fluore renforcees, procedes de fabrication, reacteurs contenant ces plaques resistants a la corrosion, leurs procedes de fabrication, et procedes de fluoration mis en oeuvre dans ces reacteurs |
| WO2006000035A1 (en) * | 2004-06-25 | 2006-01-05 | Orica Australia Pty. Ltd. | Construction material and powder coating composition |
| JP2008519132A (ja) * | 2004-11-02 | 2008-06-05 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | テロマー含有フルオロポリマーコーティング |
| JP4533115B2 (ja) * | 2004-12-03 | 2010-09-01 | 三井・デュポンフロロケミカル株式会社 | フッ素樹脂成形方法及びフッ素樹脂成形品 |
| US7969267B2 (en) * | 2004-12-09 | 2011-06-28 | Arkema | Reinforced fluoropolymer plates, production methods thereof, corrosion-resistant reactors containing said plates, production methods of same and fluorination methods performed in said reactors |
| WO2009052163A2 (en) * | 2007-10-15 | 2009-04-23 | Advanced Flexible Composites, Inc. | Crosslinkable fluoropolymer composition and uses thereof |
| JP5541176B2 (ja) * | 2011-01-24 | 2014-07-09 | ダイキン工業株式会社 | フッ素樹脂組成物及び該フッ素樹脂組成物の製造方法 |
| EP2714789B1 (en) | 2011-05-25 | 2016-02-03 | Arkema, Inc. | Irradiated fluoropolymer articles having low leachable fluoride ions |
| WO2014010509A1 (ja) * | 2012-07-09 | 2014-01-16 | 住友電気工業株式会社 | 耐熱難燃性樹脂組成物及び絶縁電線、チューブ |
| US20170004946A1 (en) * | 2015-06-30 | 2017-01-05 | Tyco Electronics Corporation | Conductive Composite and Circuit Protection Device Including a Conductive Composite |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3019206A (en) * | 1958-09-24 | 1962-01-30 | Minnesota Mining & Mfg | Polyblends of a thermoplastic tetrafluoroethylene polymer latex and an elastomeric fluorocarbon polymer latex and article coated therewith |
| US3030260A (en) * | 1958-12-15 | 1962-04-17 | North American Aviation Inc | Thermoplastic adhesive sealants |
| DE1947556A1 (de) * | 1968-09-25 | 1970-04-02 | Pennwalt Corp | Polyvinylidenfluorid-Zubereitungen |
| US3706723A (en) * | 1970-04-29 | 1972-12-19 | Allied Chem | Copolymer of 3,3,3 - trifluoro-2-trifluoromethyl propene and vinylidene fluoride |
-
1974
- 1974-10-21 US US05/516,712 patent/US3962373A/en not_active Expired - Lifetime
-
1975
- 1975-09-26 CA CA236,485A patent/CA1056093A/en not_active Expired
- 1975-10-14 DE DE2545897A patent/DE2545897C2/de not_active Expired
- 1975-10-16 IT IT6958575A patent/IT1048240B/it active
- 1975-10-20 GB GB4299775A patent/GB1487028A/en not_active Expired
- 1975-10-21 FR FR7532178A patent/FR2288763A1/fr active Granted
- 1975-10-21 JP JP50125990A patent/JPS5925820B2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CA1056093A (en) | 1979-06-05 |
| DE2545897A1 (de) | 1976-04-29 |
| FR2288763A1 (fr) | 1976-05-21 |
| JPS5165157A (en) | 1976-06-05 |
| US3962373A (en) | 1976-06-08 |
| IT1048240B (it) | 1980-11-20 |
| DE2545897C2 (de) | 1984-02-23 |
| FR2288763B1 (enExample) | 1979-01-05 |
| GB1487028A (en) | 1977-09-28 |
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