JPS59195576A - セラミツク原料粉末の製造方法 - Google Patents
セラミツク原料粉末の製造方法Info
- Publication number
- JPS59195576A JPS59195576A JP58071018A JP7101883A JPS59195576A JP S59195576 A JPS59195576 A JP S59195576A JP 58071018 A JP58071018 A JP 58071018A JP 7101883 A JP7101883 A JP 7101883A JP S59195576 A JPS59195576 A JP S59195576A
- Authority
- JP
- Japan
- Prior art keywords
- raw material
- ceramic raw
- material powder
- powder
- add
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002994 raw material Substances 0.000 title claims description 30
- 239000000843 powder Substances 0.000 title claims description 26
- 239000000919 ceramic Substances 0.000 title claims description 21
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 238000000034 method Methods 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000002002 slurry Substances 0.000 claims description 8
- 238000001354 calcination Methods 0.000 claims description 6
- 229910052718 tin Inorganic materials 0.000 claims description 6
- 229910052726 zirconium Inorganic materials 0.000 claims description 6
- 229910002651 NO3 Inorganic materials 0.000 claims description 5
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 5
- 229910052788 barium Inorganic materials 0.000 claims description 4
- 229910052791 calcium Inorganic materials 0.000 claims description 4
- 239000000470 constituent Substances 0.000 claims description 4
- 229910052745 lead Inorganic materials 0.000 claims description 4
- 229910052712 strontium Inorganic materials 0.000 claims description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 2
- 238000010298 pulverizing process Methods 0.000 claims description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims 1
- 238000003287 bathing Methods 0.000 claims 1
- 229910017604 nitric acid Inorganic materials 0.000 claims 1
- 229910052761 rare earth metal Inorganic materials 0.000 claims 1
- 229910052727 yttrium Inorganic materials 0.000 claims 1
- 229910052725 zinc Inorganic materials 0.000 claims 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 18
- 239000002244 precipitate Substances 0.000 description 14
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 12
- 239000007864 aqueous solution Substances 0.000 description 11
- 235000002639 sodium chloride Nutrition 0.000 description 10
- 239000003990 capacitor Substances 0.000 description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 235000015165 citric acid Nutrition 0.000 description 6
- 238000010304 firing Methods 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- -1 organic acid salt Chemical class 0.000 description 6
- 239000011575 calcium Substances 0.000 description 5
- 235000006408 oxalic acid Nutrition 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 229910052719 titanium Inorganic materials 0.000 description 5
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
- 239000011230 binding agent Substances 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000003381 stabilizer Substances 0.000 description 4
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 3
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 3
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 3
- 229910052783 alkali metal Inorganic materials 0.000 description 3
- 235000011114 ammonium hydroxide Nutrition 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000010419 fine particle Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 3
- 229910052573 porcelain Inorganic materials 0.000 description 3
- 239000011163 secondary particle Substances 0.000 description 3
- 235000002906 tartaric acid Nutrition 0.000 description 3
- 239000011975 tartaric acid Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical class N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000000908 ammonium hydroxide Substances 0.000 description 2
- 150000003863 ammonium salts Chemical class 0.000 description 2
- 229910052797 bismuth Inorganic materials 0.000 description 2
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 description 2
- 239000003518 caustics Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- 230000002194 synthesizing effect Effects 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241001474791 Proboscis Species 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 241000713311 Simian immunodeficiency virus Species 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- LEHOTFFKMJEONL-UHFFFAOYSA-N Uric Acid Chemical compound N1C(=O)NC(=O)C2=C1NC(=O)N2 LEHOTFFKMJEONL-UHFFFAOYSA-N 0.000 description 1
- TVWHNULVHGKJHS-UHFFFAOYSA-N Uric acid Natural products N1C(=O)NC(=O)C2NC(=O)NC21 TVWHNULVHGKJHS-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 150000004703 alkoxides Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- GXUARMXARIJAFV-UHFFFAOYSA-L barium oxalate Chemical compound [Ba+2].[O-]C(=O)C([O-])=O GXUARMXARIJAFV-UHFFFAOYSA-L 0.000 description 1
- 229940094800 barium oxalate Drugs 0.000 description 1
- HQYOWPDUMCBSLQ-UHFFFAOYSA-L barium(2+);2,3-dihydroxybutanedioate Chemical compound [Ba+2].[O-]C(=O)C(O)C(O)C([O-])=O HQYOWPDUMCBSLQ-UHFFFAOYSA-L 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 235000011116 calcium hydroxide Nutrition 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- QXDMQSPYEZFLGF-UHFFFAOYSA-L calcium oxalate Chemical compound [Ca+2].[O-]C(=O)C([O-])=O QXDMQSPYEZFLGF-UHFFFAOYSA-L 0.000 description 1
- PBUBJNYXWIDFMU-UHFFFAOYSA-L calcium;butanedioate Chemical compound [Ca+2].[O-]C(=O)CCC([O-])=O PBUBJNYXWIDFMU-UHFFFAOYSA-L 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000033444 hydroxylation Effects 0.000 description 1
- 238000005805 hydroxylation reaction Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910000000 metal hydroxide Inorganic materials 0.000 description 1
- 150000004692 metal hydroxides Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 150000002913 oxalic acids Chemical class 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000011164 primary particle Substances 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- ORXDFZVXVSSTPU-UHFFFAOYSA-J tetrapotassium tetrachloride Chemical compound [Cl-].[Cl-].[Cl-].[Cl-].[K+].[K+].[K+].[K+] ORXDFZVXVSSTPU-UHFFFAOYSA-J 0.000 description 1
- 229940116269 uric acid Drugs 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Inorganic Insulating Materials (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58071018A JPS59195576A (ja) | 1983-04-21 | 1983-04-21 | セラミツク原料粉末の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58071018A JPS59195576A (ja) | 1983-04-21 | 1983-04-21 | セラミツク原料粉末の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS59195576A true JPS59195576A (ja) | 1984-11-06 |
| JPH0210091B2 JPH0210091B2 (en, 2012) | 1990-03-06 |
Family
ID=13448350
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58071018A Granted JPS59195576A (ja) | 1983-04-21 | 1983-04-21 | セラミツク原料粉末の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59195576A (en, 2012) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63141206A (ja) * | 1986-12-04 | 1988-06-13 | 太陽誘電株式会社 | 粒界絶縁型半導体磁器 |
| JPS63233035A (ja) * | 1987-03-23 | 1988-09-28 | 科学技術庁無機材質研究所長 | 多成分セラミツクスの製造方法 |
| JPH02107552A (ja) * | 1988-10-13 | 1990-04-19 | Sumitomo Special Metals Co Ltd | 電子デバイス用誘電体磁器組成物 |
| US5032559A (en) * | 1989-05-05 | 1991-07-16 | Gte Products Corporation | Method of preparing barium, titanium, zirconium oxide ferroelectric ceramic compositions |
| CN102503407A (zh) * | 2011-09-30 | 2012-06-20 | 天津大学 | 新型无铅x8r型多层陶瓷电容器介质及其制备方法 |
| JP2020083672A (ja) * | 2018-11-16 | 2020-06-04 | 堺化学工業株式会社 | チタン酸バリウムの製造方法 |
-
1983
- 1983-04-21 JP JP58071018A patent/JPS59195576A/ja active Granted
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63141206A (ja) * | 1986-12-04 | 1988-06-13 | 太陽誘電株式会社 | 粒界絶縁型半導体磁器 |
| JPS63233035A (ja) * | 1987-03-23 | 1988-09-28 | 科学技術庁無機材質研究所長 | 多成分セラミツクスの製造方法 |
| JPH02107552A (ja) * | 1988-10-13 | 1990-04-19 | Sumitomo Special Metals Co Ltd | 電子デバイス用誘電体磁器組成物 |
| US5032559A (en) * | 1989-05-05 | 1991-07-16 | Gte Products Corporation | Method of preparing barium, titanium, zirconium oxide ferroelectric ceramic compositions |
| CN102503407A (zh) * | 2011-09-30 | 2012-06-20 | 天津大学 | 新型无铅x8r型多层陶瓷电容器介质及其制备方法 |
| JP2020083672A (ja) * | 2018-11-16 | 2020-06-04 | 堺化学工業株式会社 | チタン酸バリウムの製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0210091B2 (en, 2012) | 1990-03-06 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4061583A (en) | Preparation of titanates | |
| JPH0459261B2 (en, 2012) | ||
| KR100845216B1 (ko) | 구형의 정방정계 티탄산바륨 입자 및 그의 제조방법 | |
| JP2004517795A (ja) | 被覆されたチタン酸バリウム系粒子および製法 | |
| JPS6153114A (ja) | 易焼結性ペロブスカイト固溶体の原料粉末の製造方法 | |
| JPH03153557A (ja) | 鉛系ペロブスカイト型セラミックスの原料粉末の製造方法 | |
| JPS59195576A (ja) | セラミツク原料粉末の製造方法 | |
| KR101556678B1 (ko) | 결정성 티탄산 스트론튬 분말 및 그의 제조 방법 | |
| JPS63141204A (ja) | 電子部品用磁器の製造方法 | |
| JPH0246531B2 (en, 2012) | ||
| JPS59195574A (ja) | セラミツク原料粉末の製造方法 | |
| JPS61242903A (ja) | 複合酸化物セラミツク粉末の製造方法 | |
| JP3163649B2 (ja) | セラミック原料粉末の製造方法 | |
| JPS6153113A (ja) | 湿式法による易焼結性ペロブスカイト及びその固溶体の原料粉末の製造方法 | |
| JPS61111957A (ja) | セラミック誘電体の製造方法 | |
| JP2764111B2 (ja) | ペロブスカイト系セラミック粉末の製造方法 | |
| JPH0210090B2 (en, 2012) | ||
| JPS59128263A (ja) | セラミツク原料粉末の製造方法 | |
| KR100395218B1 (ko) | ＢａＴｉＯ3계 분말 제조 방법 | |
| JP2767584B2 (ja) | ペロブスカイト型セラミックス微粉末の製造方法 | |
| JPH0769645A (ja) | 鉛含有複合酸化物の製造方法 | |
| JPH013019A (ja) | ペロブスカイト型セラミックス微粉末の製造方法 | |
| CN1027634C (zh) | 正温度系数热敏电阻陶瓷超细粉的制造方法 | |
| JPS61163118A (ja) | 粉末分散湿式法による易焼結性ペロブスカイト原料粉末の製造法 | |
| JPS61251515A (ja) | 複合酸化物セラミツク粉末の製造方法 |