JPS5838430B2 - パラフイン系炭化水素からスルホン酸を製造する方法及び装置 - Google Patents
パラフイン系炭化水素からスルホン酸を製造する方法及び装置Info
- Publication number
- JPS5838430B2 JPS5838430B2 JP49108689A JP10868974A JPS5838430B2 JP S5838430 B2 JPS5838430 B2 JP S5838430B2 JP 49108689 A JP49108689 A JP 49108689A JP 10868974 A JP10868974 A JP 10868974A JP S5838430 B2 JPS5838430 B2 JP S5838430B2
- Authority
- JP
- Japan
- Prior art keywords
- paraffin
- sulfonic acid
- reactor
- oxygen
- conduit
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000012188 paraffin wax Substances 0.000 title claims description 47
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 title claims description 24
- 238000000034 method Methods 0.000 title claims description 21
- 229930195733 hydrocarbon Natural products 0.000 title claims description 6
- 150000002430 hydrocarbons Chemical class 0.000 title claims description 6
- 239000007789 gas Substances 0.000 claims description 42
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 claims description 32
- 239000000203 mixture Substances 0.000 claims description 22
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 16
- 239000001301 oxygen Substances 0.000 claims description 16
- 229910052760 oxygen Inorganic materials 0.000 claims description 16
- 239000012530 fluid Substances 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 9
- 239000012429 reaction media Substances 0.000 claims description 8
- 239000011541 reaction mixture Substances 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 4
- 239000012295 chemical reaction liquid Substances 0.000 claims description 2
- 230000005855 radiation Effects 0.000 claims description 2
- 238000010924 continuous production Methods 0.000 claims 1
- 239000012071 phase Substances 0.000 description 19
- 238000006243 chemical reaction Methods 0.000 description 18
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 14
- 239000007791 liquid phase Substances 0.000 description 9
- 125000004432 carbon atom Chemical group C* 0.000 description 6
- 238000010586 diagram Methods 0.000 description 6
- 238000012546 transfer Methods 0.000 description 6
- 239000008346 aqueous phase Substances 0.000 description 5
- 238000002156 mixing Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 238000013019 agitation Methods 0.000 description 3
- 238000009792 diffusion process Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- 239000000376 reactant Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 2
- 229940057995 liquid paraffin Drugs 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000011437 continuous method Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000010908 decantation Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 239000008246 gaseous mixture Substances 0.000 description 1
- 239000007792 gaseous phase Substances 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000005381 potential energy Methods 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 238000006277 sulfonation reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
- B01J19/122—Incoherent waves
- B01J19/123—Ultraviolet light
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S204/00—Chemistry: electrical and wave energy
- Y10S204/902—Production of desired compound by wave energy in presence of a chemically designated nonreactant chemical treating agent, excluding water, chloroform, carbon tetrachloride, methylene chloride or benzene
- Y10S204/903—Inorganic chemical treating agent
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7333746 | 1973-09-20 | ||
| FR7333746A FR2244734B1 (OSRAM) | 1973-09-20 | 1973-09-20 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5076024A JPS5076024A (OSRAM) | 1975-06-21 |
| JPS5838430B2 true JPS5838430B2 (ja) | 1983-08-23 |
Family
ID=9125318
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP49108689A Expired JPS5838430B2 (ja) | 1973-09-20 | 1974-09-20 | パラフイン系炭化水素からスルホン酸を製造する方法及び装置 |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US4000049A (OSRAM) |
| JP (1) | JPS5838430B2 (OSRAM) |
| BE (1) | BE820095A (OSRAM) |
| CA (1) | CA1047438A (OSRAM) |
| CH (1) | CH599139A5 (OSRAM) |
| DE (1) | DE2444895C2 (OSRAM) |
| ES (1) | ES430254A1 (OSRAM) |
| FR (1) | FR2244734B1 (OSRAM) |
| GB (1) | GB1459881A (OSRAM) |
| IT (1) | IT1022141B (OSRAM) |
| LU (1) | LU70948A1 (OSRAM) |
| NL (1) | NL7412491A (OSRAM) |
| NO (1) | NO139385C (OSRAM) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4517063A (en) * | 1984-02-13 | 1985-05-14 | The Standard Oil Company | Photochemical reactor and method for carrying out photochemical reactions therein |
| US8512809B2 (en) * | 2010-03-31 | 2013-08-20 | General Electric Company | Method of processing multilayer film |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US449687A (en) * | 1891-04-07 | maxim | ||
| BE515328A (OSRAM) * | 1951-11-06 | 1900-01-01 | ||
| US3111538A (en) * | 1957-02-07 | 1963-11-19 | Hercules Powder Co Ltd | Continuous manufacture of explosive liquid nitric acid esters |
| GB1039804A (en) * | 1963-02-11 | 1966-08-24 | Exxon Research Engineering Co | Sulfoxidation process |
| GB1089137A (en) * | 1964-06-12 | 1967-11-01 | British Hydrocarbon Chem Ltd | Improvements relating to the production of sulphonic acids |
| FR1474522A (fr) * | 1965-04-03 | 1967-03-24 | Hoechst Ag | Procédé de traitement complémentaire d'acides sulfoniques de paraffine |
| US3658671A (en) * | 1968-09-20 | 1972-04-25 | Lion Fat Oil Co Ltd | Sulfoxidation of paraffin |
| US3682803A (en) * | 1969-04-23 | 1972-08-08 | Kao Corp | Process for the photochemical sulfoxidation of n-paraffin |
-
1973
- 1973-09-20 FR FR7333746A patent/FR2244734B1/fr not_active Expired
-
1974
- 1974-09-18 GB GB4069674A patent/GB1459881A/en not_active Expired
- 1974-09-18 US US05/507,081 patent/US4000049A/en not_active Expired - Lifetime
- 1974-09-19 NO NO743379A patent/NO139385C/no unknown
- 1974-09-19 BE BE148683A patent/BE820095A/xx not_active IP Right Cessation
- 1974-09-19 LU LU70948A patent/LU70948A1/xx unknown
- 1974-09-19 CH CH1268674A patent/CH599139A5/xx not_active IP Right Cessation
- 1974-09-19 CA CA209,608A patent/CA1047438A/fr not_active Expired
- 1974-09-19 DE DE2444895A patent/DE2444895C2/de not_active Expired
- 1974-09-20 ES ES430254A patent/ES430254A1/es not_active Expired
- 1974-09-20 JP JP49108689A patent/JPS5838430B2/ja not_active Expired
- 1974-09-20 NL NL7412491A patent/NL7412491A/xx not_active Application Discontinuation
- 1974-09-20 IT IT27501/74A patent/IT1022141B/it active
Also Published As
| Publication number | Publication date |
|---|---|
| NL7412491A (nl) | 1975-03-24 |
| NO743379L (OSRAM) | 1975-04-14 |
| FR2244734B1 (OSRAM) | 1976-11-19 |
| ES430254A1 (es) | 1977-02-16 |
| DE2444895A1 (de) | 1975-04-03 |
| IT1022141B (it) | 1978-03-20 |
| LU70948A1 (OSRAM) | 1975-03-06 |
| JPS5076024A (OSRAM) | 1975-06-21 |
| FR2244734A1 (OSRAM) | 1975-04-18 |
| CA1047438A (fr) | 1979-01-30 |
| BE820095A (fr) | 1975-01-16 |
| CH599139A5 (OSRAM) | 1978-05-12 |
| NO139385B (no) | 1978-11-20 |
| NO139385C (no) | 1979-02-28 |
| US4000049A (en) | 1976-12-28 |
| GB1459881A (en) | 1976-12-31 |
| DE2444895C2 (de) | 1985-05-15 |
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